• ASTM D 202 : 2017 : REDLINE

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

    Standard Test Methods for Sampling and Testing Untreated Paper Used for Electrical Insulation

    Available format(s):  PDF

    Superseded date:  09-06-2023

    Language(s):  English

    Published date:  22-02-2017

    Publisher:  American Society for Testing and Materials

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    Abstract - (Show below) - (Hide below)

    CONTAINED IN VOL. 10.01, 2017 Defines procedures for sampling and testing untreated paper to be used as an electrical insulator or as a constituent of a composite material used for electrical insulating purposes.

    Scope - (Show below) - (Hide below)

    1.1These test methods cover procedures for sampling and testing untreated paper to be used as an electrical insulator or as a constituent of a composite material used for electrical insulating purposes.

    1.1.1Untreated papers are thin, fibrous sheets normally laid down from a water suspension of pulped fibers (usually cellulosic) with or without various amounts of nonfibrous ingredients, and which are calendared, if required, to obtain desired thickness and density. Nevertheless, these test methods are applicable, generally although not invariably, to papers formed by other means, to papers modified (during or after formation) by additions, and to papers given subsequent mechanical treatments such as creping.

    1.1.2As an electrical insulating and dielectric material, paper is considered “untreated” until it is subjected to a manufacturing process such as drying, impregnation, or varnish treatment.

    1.1.3The test methods given herein were developed specifically for papers having a thickness of 0.75 mm (0.030 in.) or less. A number of these test methods are also suitable for use on other materials such as pulps or boards. Refer to Test Methods D3376 or D3394 to determine which tests are applicable to pulps or electrical insulating boards. In the paper industry, some products in thicknesses of less than 0.75 mm are termed “paperboard”. Such products are included within the scope of these methods.

    1.1.4These test methods are applicable to flexible fibrous-mat materials formed from suspensions of fiber in fluids other than water. Thicknesses of these mats approach 2 mm, and the fibers contained are possibly natural, synthetic, organic, or inorganic; fillers that are natural, synthetic, organic, or inorganic; and flexible polymeric binder materials.

    1.2The procedures appear in the following sections:

    Procedure

    Sections

    ASTM or TAPPI Reference
    (Modified)

    Absorption (Rise of Water)

    78 to 83

    . . .

    Acidity-Alkalinity-pH

    45 to 54

    E70

    Air Resistance

    98 to 101

    D726

    Aqueous Extract Conductivity

    55 to 64

    . . .

    Ash Content

    40 to 44

    D586

    Bursting Strength

    102 to 107

    D774/D774M

    Chlorides (Water-Extractable)

    165 to 183

    . . .

    Conditioning

    15

    D6054

    Conducting Paths

    138 to 151

    . . .

    Density, Apparent

    29 to 33

    . . .

    Dielectric Strength

    152 to 157

    D149

    Dimensions of Sheet, Rolls and Cores

    16 to 24

    D374

    Dissipation Factor and Permittivity

    158 to 164

    D150

    Edge-Tearing Resistance

    126 to 130

    D827

    Fiber Analysis

    74 to 77

    D1030

    Folding Endurance

    108 to 110

    T 423 and D2176

    Grammage

    25 to 28

    D646

    Permittivity

    158 to 164

    D150

    Heat Stability in Air

    131 to 137

    D827

    Impregnation Time

    84 to 91

    . . .

    Internal-Tearing Resistance

    121 to 125

    D689 or T 414

    Moisture Content

    34 to 39

    D644 and D3277

    Particulate Copper

    193 to 202

    . . .

    Particulate Iron

    184 to 192

    . . .

    Reagents

    4

    D1193

    Reports

    14

    E29

    Sampling

    6 to 13

    D3636

    Silver Tarnishing by Paper and Paperboard

    203 to 206

    T 444

    Solvent-Soluble Matter

    65 to 73

    . . .

    Surface Friction

    92 to 97

    D528 and T 455

    Tensile Properties

    111 to 120

    D76, E4

    Thickness (see Dimensions)

    16 to 24

    D374

    1.3The tests for Holes and Felt Hair Inclusions and the Stain Test for Fine Pores, have been removed from this compilation of test methods. These test methods were specific to grades of capacitor paper formerly covered by Specification D1930, which has been withdrawn.

    Note 1:This compilation of test methods is closely related to IEC Publication 60554-2. Not all of the individual methods included herein are included in IEC 60554-2, nor are all of the methods in IEC 60554-2 included in this standard. The individual procedures as described in the two standards are in general sufficiently close to each other that it is reasonable to expect that test results obtained by most of the procedures specified in either standard will not differ significantly. However, before assuming that a procedure in these test methods is exactly equivalent to an IEC 60554-2 procedure, the written procedures must be compared closely, and if it seems advisable, test results by the two procedures are compared.

    1.4The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.

    1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See 43.2.1, 71.1, 143.1, 148.1 and 156.1 for specific hazards.

    General Product Information - (Show below) - (Hide below)

    Committee D 09
    Document Type Redline
    Publisher American Society for Testing and Materials
    Status Superseded
    Superseded By

    Standards Referenced By This Book - (Show below) - (Hide below)

    MIL S 55620 : 0 SUBSTRATES, CERAMIC, FOR DEPOSITION OF THIN FILM MICROCIRCUITS
    TAPPI T 252 : 2002 : R2012 PH AND ELECTRICAL CONDUCTIVITY OF HOT WATER EXTRACTS OF PULP, PAPER, AND PAPERBOARD
    MIL-P-47271 Revision A:1983 PAPER, INSULATING, ELECTRICAL
    ASTM D 360 : 2012 Standard Specification for Shellac Varnishes
    ASTM D 778 : 1997 : R2002 Standard Test Methods for Hydrogen Ion Concentration (pH) of Paper Extracts (Hot- Extraction and Cold-Extraction Procedures)
    ASTM D 776 : 1992 : R1996 Standard Test Method for Determination of Effect of Dry Heat on Properties of Paper and Board
    ASTM D 619 : 2014 Standard Test Methods for Vulcanized Fibre Used for Electrical Insulation
    ASTM D 778 : 1997 Standard Test Methods for Hydrogen Ion Concentration (pH) of Paper Extracts (Hot- Extraction and Cold-Extraction Procedures)
    ASTM D 645/D645M : 1997 : R2007 Standard Test Method for Thickness of Paper and Paperboard (Withdrawn 2010)
    MIL-I-24683 Revision A:1990 INSULATION ELECTRICAL, HIGH TEMPERATURE INORGANIC PAPER
    DOD I 24683 : 1987 INSULATION ELECTRICAL, HIGH TEMPERATURE INORGANIC PAPER
    ASTM D 1677 : 2017 : REDLINE Standard Methods for Sampling and Testing Untreated Mica Paper Used for Electrical Insulation
    ASTM D 360 : 2012 : R2019 Standard Specification for Shellac Varnishes
    ASTM D 1304 : 1999 : R2005 Standard Test Methods for Adhesives Relative to Their Use as Electrical Insulation
    ASTM D 1458 : 2013-12 TEST METHODS FOR FULLY CURED SILICONE RUBBER-COATED GLASS FABRIC AND TAPES FOR ELECTRICAL INSULATION
    ASTM D 4714 : 1996 Standard Test Method for Determination of Effect of Moist Heat (50% Relative Humidity and 90°C) on Properties of Paper and Board
    ASTM D 1304 : 1999 : R2012 Standard Test Methods for Adhesives Relative to Their Use as Electrical Insulation
    ASTM D 778 : 1997 : R2007 Standard Test Methods for Hydrogen Ion Concentration (pH) of Paper Extracts (Hot-Extraction and Cold-Extraction Procedures) (Withdrawn 2010)
    ASTM D 1305 : 2016 : REDLINE Standard Specification for Electrical Insulating Paper and Paperboard—Sulfate (Kraft) Layer Type
    ASTM D 1304 : 1999 Standard Test Methods for Adhesives Relative to Their Use as Electrical Insulation
    ASTM D 645/D645M : 1997 Standard Test Method for Thickness of Paper and Paperboard
    SAE AMS 3803 : 2016 WIPES, COTTON, LOOSELY WOVEN
    ASTM D 645/D645M : 1997 : R2002 Standard Test Method for Thickness of Paper and Paperboard
    ASTM D 3664 : 2016 : REDLINE Standard Specification for Biaxially Oriented Polymeric Resin Film for Capacitors in Electrical Equipment
    ASTM D 4714 : 1996 : R2007 Standard Test Method for Determination of Effect of Moist Heat (50 % Relative Humidity and 90C) on Properties of Paper and Board (Withdrawn 2010)
    ASTM D 115 : 2017 : REDLINE Standard Test Methods for Testing Solvent Containing Varnishes Used for Electrical Insulation
    TAPPI T 252 : 2002 PH AND ELECTRICAL CONDUCTIVITY OF HOT WATER EXTRACTS OF PULP, PAPER, AND PAPERBOARD
    ASTM D 2753 : 1989 Specification for Electrolytic Capacitor Paper (Withdrawn 1993)
    ASTM D 4714 : 1996 : R2001 Standard Test Method for Determination of Effect of Moist Heat (50% Relative Humidity and 90°C) on Properties of Paper and Board
    ASTM D 2413 : 2016 : REDLINE Standard Practice for Preparation of Insulating Paper and Board Impregnated with a Liquid Dielectric
    MIL-I-545 Revision B:1976 INSULATION SHEET, ELECTRICAL, PAPER, PRESSBOARD
    MIL-F-10336 Revision E:1977 FIBER SHEET, VULCANIZED
    TAPPI T 252 : 2002 : R2007 PH AND ELECTRICAL CONDUCTIVITY OF HOT WATER EXTRACTS OF PULP, PAPER, AND PAPERBOARD
    ASTM D 3394 : 2016 : REDLINE Standard Test Methods for Sampling and Testing Electrical Insulating Board
    ASTM D 7812 : 2016 Standard Test Method for Tensile Testing of Aramid Paper
    ASTM D 776 : 1992 : R2001 Standard Test Method for Determination of Effect of Dry Heat on Properties of Paper and Board (Withdrawn 2009)

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM D 689 : 2017 Standard Test Method for Internal Tearing Resistance of Paper
    ASTM D 644 : 1999 Standard Test Method for Moisture Content of Paper and Paperboard by Oven Drying
    ASTM D 646 : 2013 Standard Test Method for Mass Per Unit Area of Paper and Paperboard of Aramid Papers (Basis Weight) (Withdrawn 2022)
    TAPPI T 460 : 2011 AIR RESISTANCE OF PAPER (GURLEY METHOD)
    TAPPI T 455 : 2014 IDENTIFICATION OF WIRE SIDE OF PAPER
    TAPPI T 470 : OM 89 EDGE TEARING RESISTANCE OF PAPER (EDGE-TEAR STIRRUP METHOD)
    ASTM D 1711 : 2015 : REDLINE Standard Terminology Relating to Electrical Insulation
    TAPPI T 423 : 2007 FOLDING ENDURANCE OF PAPER (SCHOPPER TYPE TESTER)
    ASTM D 2176 : 2016 Standard Test Method for Folding Endurance of Paper and Plastics Film by the M.I.T. Tester
    ASTM D 76 : 1999 Standard Specification for Tensile Testing Machines for Textiles
    ASTM E 70 TEST METHOD FOR PH OF AQUEOUS SOLUTIONS WITH THE GLASS ELECTRODE
    IEC 60554-2:2001 Cellulosic papers for electrical purposes - Part 2: Methods of test
    TAPPI T 536 : 2012 RESISTANCE OF PAPER TO PASSAGE OF AIR (HIGH-PRESSURE GURLEY METHOD)
    ASTM D 2865 : 2001 Standard Practice for Calibration of Standards and Equipment for Electrical Insulating Materials Testing
    ASTM D 3394 : 2016 : REDLINE Standard Test Methods for Sampling and Testing Electrical Insulating Board
    ASTM D 827 : 1967 : R1971 Method of Test for Edge Tearing Strength of Paper (Withdrawn 1980)
    ASTM D 2413 : 2016 : REDLINE Standard Practice for Preparation of Insulating Paper and Board Impregnated with a Liquid Dielectric
    ASTM D 528 : 1997 Standard Test Method for Machine Direction of Paper and Paperboard
    TAPPI T 444 : 2012 SILVER TARNISHING BY PAPER AND PAPERBOARD
    ASTM D 374 : 1999 Standard Test Methods for Thickness of Solid Electrical Insulation
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