ASTM E 2594 : 2009 : R2014

Superseded

Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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Standard Test Method for Analysis of Nickel Alloys by Inductively Coupled Plasma Atomic Emission Spectrometry (Performance-Based Method)

Available format(s): Hardcopy, PDF

Superseded date: 02-03-2020

Language(s): English

Published date: 24-06-2014

Publisher: American Society for Testing and Materials

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CONTAINED IN VOL. 03.05, 2014 Specifies the inductively coupled plasma atomic emission spectrometric analysis of nickel alloys.

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1.1This test method describes the inductively coupled plasma atomic emission spectrometric analysis of nickel alloys, such as specified by Committee B02, and having chemical compositions within the following limits:

Element	Application Range (%)
Aluminum	0.01–1.00
Boron	0.001–0.050
Calcium	0.001–0.05
Carbon	0.10–0.20
Chromium	0.01–33.0
Cobalt	0.10–20.0
Copper	0.01–3.00
Iron	0.01–50.0
Lead	0.001–0.01
Magnesium	0.0001–0.100
Manganese	0.01–3.0
Molybdenum	0.01–30.0
Niobium	0.01–6.0
Nickel	25.0–80.0
Nitrogen	0.001–0.20
Oxygen	0.0001–0.003
Phosphorous	0.001–0.030
Sulfur	0.0001–0.010
Silicon	0.01–1.50
Tantalum	0.005–0.10
Tin	0.001–0.020
Titanium	0.001–6.0
Tungsten	0.01–5.0
Vanadium	0.01–1.0
Zirconium	0.01–0.10

1.2The following elements may be determined using this test method. The test method user should carefully evaluate the precision and bias statements of this test method to determine applicability of the test method for the intended use.

Element	Quantification Range (%)
Aluminum	0.060–1.40
Boron	0.002–0.020
Calcium	0.001–0.003
Copper	0.010–0.52
Magnesium	0.001–0.10
Manganese	0.002–0.65
Niobium	0.020–5.5
Phosphorous	0.004–0.030
Tantalum	0.010–0.050
Tin	0.002–0.018
Titanium	0.020–3.1
Tungsten	0.007–0.11
Vanadium	0.010–0.50
Zirconium	0.002–0.10

1.3This test method has only been interlaboratory tested for the elements and ranges specified. It may be possible to extend this test method to other elements or different concentration ranges provided that method validation is performed that includes evaluation of method sensitivity, precision, and bias as described in this document. Additionally, the validation study must evaluate the acceptability of sample preparation methodology using reference materials or spike recoveries, or both. The user is cautioned to carefully evaluate the validation data against the laboratory’s data quality objectives. Method validation of scope extensions is also a requirement of ISO/IEC 17025.

1.4The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given in 8.2.6.3 and safety hazard statements are given in Section 9.

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Committee	E 01
Document Type	Test Method
ISBN
Pages
Product Note	Reconfirmed 2014
Published
Publisher	American Society for Testing and Materials
Status	Superseded
Superseded By	ASTM E 2594 : 2020
Supersedes	ASTM E 2594 : 2009

Standards Referenced By This Book - (Show below) - (Hide below)

ASTM E 1473 : 2016	Standard Test Methods for Chemical Analysis of Nickel, Cobalt and High-Temperature Alloys
ASTM F 3049 : 2014	Standard Guide for Characterizing Properties of Metal Powders Used for Additive Manufacturing Processes

Standards Referencing This Book - (Show below) - (Hide below)

ASTM E 2027 : 2017 : EDT 1	Standard Practice for Conducting Proficiency Tests in the Chemical Analysis of Metals, Ores, and Related Materials (Withdrawn 2022)
ISO/IEC 17025:2005	General requirements for the competence of testing and calibration laboratories
ASTM E 1479 : 2016	Standard Practice for Describing and Specifying Inductively Coupled Plasma Atomic Emission Spectrometers
ASTM E 1479 : 1999 : R2005	Standard Practice for Describing and Specifying Inductively-Coupled Plasma Atomic Emission Spectrometers
ASTM D 1193 : 1977 : R1983 : EDT 1	Standard Specification for Reagent Water
ASTM E 50 : 2017 : REDLINE	Standard Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials
ASTM E 1329 : 2000 : R2005	Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis
ASTM E 2027 : 2009	Standard Practice for Conducting Proficiency Tests in the Chemical Analysis of Metals, Ores, and Related Materials
ASTM E 2027 : 2017	Standard Practice for Conducting Proficiency Tests in the Chemical Analysis of Metals, Ores, and Related Materials
ASTM E 1479 : 2016 : REDLINE	Standard Practice for Describing and Specifying Inductively Coupled Plasma Atomic Emission Spectrometers
ASTM D 1193 : 2006 : R2011	Standard Specification for Reagent Water
ASTM E 1601 : 2019	Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
ASTM E 1601 : 1998	Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
ASTM E 1601 : 2010	Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
ASTM E 1329 : 2010	Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis (Withdrawn 2019)
ASTM E 1479 : 1999 : R2011	Standard Practice for Describing and Specifying Inductively-Coupled Plasma Atomic Emission Spectrometers
ASTM E 1329 : 2000	Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis
ASTM E 1601 : 2012 : REDLINE	Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
ASTM D 1193 : 1991	Standard Specification for Reagent Water
ASTM E 1601 : 2012	Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
ASTM E 2027 : 1999	Standard Practice for Conducting Proficiency Tests in the Chemical Analysis of Metals, Ores, and Related Materials
ASTM E 2027 : 2005	Standard Practice for Conducting Proficiency Tests in the Chemical Analysis of Metals, Ores, and Related Materials
ASTM D 1193 : 1970	Standard Specification For Reagent Water
ASTM D 1193 : 2006	Standard Specification for Reagent Water
ASTM D 1193 : 1999	Standard Specification for Reagent Water
ISO Guide 31:2015	Reference materials — Contents of certificates, labels and accompanying documentation
ASTM D 1193 : 2006 : R2018	Standard Specification for Reagent Water
ISO Guide 34:2009	General requirements for the competence of reference material producers
ASTM E 1479 : 1999	Standard Practice for Describing and Specifying Inductively-Coupled Plasma Atomic Emission Spectrometers
ISO/IEC Guide 98-3:2008	Uncertainty of measurement — Part 3: Guide to the expression of uncertainty in measurement (GUM:1995)

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