• BS EN 15621:2017

    Current The latest, up-to-date edition.

    Animal feeding stuffs: Methods of sampling and analysis. Determination of calcium, sodium, phosphorus, magnesium, potassium, sulphur, iron, zinc, copper, manganese and cobalt after pressure digestion by ICP-AES

    Available format(s):  Hardcopy, PDF

    Language(s):  English

    Published date:  23-08-2017

    Publisher:  British Standards Institution

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    Table of Contents - (Show below) - (Hide below)

    European foreword
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Principle
    5 Reagents
    6 Apparatus
    7 Sampling
    8 Preparation of the test sample
    9 Procedure
    10 Calculation and expression of the results
    11 Precision
    12 Test report
    Annex A (informative) - Results of the inter-laboratory test
    Annex B (informative) - Notes on the detection technique,
            interferences and quantification, pressure digestion
    Bibliography

    Abstract - (Show below) - (Hide below)

    Defines a method for the determination of the elements calcium, sodium, phosphorus, magnesium, potassium, sulphur, iron, zinc, copper, manganese and cobalt in animal feeding stuffs by inductively coupled plasma atomic emission spectrometry (ICP-AES) after pressure digestion.

    Scope - (Show below) - (Hide below)

    This European Standard specifies a method for the determination of the elements calcium, sodium, phosphorus, magnesium, potassium, sulphur, iron, zinc, copper, manganese and cobalt in animal feeding stuffs by inductively coupled plasma atomic emission spectrometry (ICP-AES) after pressure digestion. The method was fully statistically tested and evaluated for the elements calcium, sodium, phosphorus, magnesium, potassium, sulphur, iron, zinc, copper, manganese and cobalt within the following 11 animal feeds: 2 complete feeds (pig feed, sheep feed), 3 complementary feeds (3 mineral feeds), 1 mineral premixture, 3 feed materials (MgO, phosphate, CaCO3) and 2 feed additives (CuSO4, bentonite). For potassium and sulphur the HORRAT values were mostly higher than 2. Therefore, for these elements the method is more applicable as a screening method and not for confirmatory purposes. Other elements like molybdenum, lead, cadmium, arsenic were not fully statistically tested and evaluated within 11 animal feeding stuff samples because these elements did not occur in concentrations higher than the limit of quantification in most of these samples. A single laboratory validation is therefore necessary for the use of this multi element method for these elements. For the determination of extractable lead in minerals and feeds, containing phyllosilicates (e.g. kaolinite clay) wet digestion with nitric acid should be used. The method limit of quantification for each element is dependent on the sample matrix as well as on the instrument. The method is not applicable for determination of low concentrations of elements. A limit of quantification of 1 mg/kg should normally be obtained. NOTE 1 This method can also be used for the determination in products with high content (> 5 %) of the element to be measured, but for this purpose the accuracy of the method has to be checked individually. NOTE 2 Results of this European Standard EN 15621 may be higher than of EN 15510 because EN 15621 is using pressure digestion mode.

    General Product Information - (Show below) - (Hide below)

    Committee AW/10
    Development Note Supersedes DD CEN/TS 15621. (02/2012) Supersedes 16/30342879 DC. (09/2017)
    Document Type Standard
    Publisher British Standards Institution
    Status Current
    Supersedes

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 5725-1:1994 Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions
    ISO 6497:2002 Animal feeding stuffs Sampling
    EN ISO 6498:2012 Animal feeding stuffs - Guidelines for sample preparation (ISO 6498:2012)
    EN 13805:2014 Foodstuffs - Determination of trace elements - Pressure digestion
    EN ISO 6497 : 2005 ANIMAL FEEDING STUFFS - SAMPLING
    ISO 6498:2012 Animal feeding stuffs — Guidelines for sample preparation
    ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
    EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
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