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  • BS ISO 16000-14:2009

    Current The latest, up-to-date edition.

    Indoor air Determination of total (gas and particle-phase) polychlorinated dioxin-like biphenyls (PCBs) and polychlorinated dibenzo-p-dioxins/dibenzofurans (PCDDs/PCDFs). Extraction, clean-up and analysis by high-resolution gas chromatography and mass spectrometry

    Available format(s):  Hardcopy, PDF

    Language(s):  English

    Published date:  31-05-2009

    Publisher:  British Standards Institution

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    Introduction
    1 Scope
    2 Normative references
    3 Terms, definitions and abbreviated terms
    4 Principle
    5 Apparatus and materials
    6 Analysis
    7 Minimum requirements for extraction and clean-up
    8 Identification and quantification
    9 Quality assurance criteria for the procedure blanks
    10 Recovery
    11 Calculation and presentation of results
    12 Safety measures
    13 Performance characteristics
    14 Interferences
    Annex A (informative) - Structure, toxicity and calculation
            of toxic equivalents
    Annex B (informative) - Example for the clean-up of
            PCBs/PCDDs/PCDFs and the separation of PCBs
            from PCDDs/PCDFs
    Annex C (informative) - GC/MS analysis
    Annex D (informative) - Masses of the ions for PCDDs/PCDFs
            and PCBs
    Annex E (informative) - Interferences
    Annex F (normative) Calibration solutions for GC/MS calibration
    Annex G (informative) - Standard deviations, detection limits
            and indoor air concentrations for PCBs
    Bibliography

    Abstract - (Show below) - (Hide below)

    Defines extraction, clean-up, and analysis procedures for the determination of polychlorinated biphenyls (PCBs), polychlorinated dibenzo-p-dioxins (PCDDs) and polychlorinated dibenzofurans (PCDFs) collected from indoor air on particle filters backed by polyurethane foam (PUF).

    General Product Information - (Show below) - (Hide below)

    Committee EH/2/5
    Development Note Supersedes 07/30146333 DC. (06/2009)
    Document Type Standard
    Publisher British Standards Institution
    Status Current
    Supersedes

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 4793:1980 Laboratory sintered (fritted) filters — Porosity grading, classification and designation
    CEN/TS 1948-4:2007 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 4: Sampling and analysis of dioxin-like PCBs
    ISO 16000-13:2008 Indoor air — Part 13: Determination of total (gas and particle-phase) polychlorinated dioxin-like biphenyls (PCBs) and polychlorinated dibenzo-p-dioxins/dibenzofurans (PCDDs/PCDFs) — Collection on sorbent-backed filters
    EN 1948-2:2006 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 2: Extraction and clean-up of PCDDs/PCDFs
    VDI 3498 Blatt 2:2002-07 Ambient air measurement - Indoor air measurement - Measurement of polychlorinated dibenzo-p-dioxins and dibenzofurans; Method using small filters
    ISO 16017-1:2000 Indoor, ambient and workplace air — Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography — Part 1: Pumped sampling
    ISO 16017-2:2003 Indoor, ambient and workplace air — Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography — Part 2: Diffusive sampling
    EN 1948-3:2006 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 3: Identification and quantification of PCDDs/PCDFs
    ISO 16000-12:2008 Indoor air Part 12: Sampling strategy for polychlorinated biphenyls (PCBs), polychlorinated dibenzo-p-dioxins (PCDDs), polychlorinated dibenzofurans (PCDFs) and polycyclic aromatic hydrocarbons (PAHs)
    ISO 12219-1:2012 Interior air of road vehicles Part 1: Whole vehicle test chamber Specification and method for the determination of volatile organic compounds in cabin interiors
    ISO 9169:2006 Air quality Definition and determination of performance characteristics of an automatic measuring system
    VDI 3498 Blatt 1:2002-07 Ambient air measurement - Indoor air measurement - Measurement of polychlorinated dibenzo-p-dioxins and dibenzofurans; Method using large filters
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