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TESTING OF CERAMIC RAW AND BASIC MATERIALS - DETERMINATION OF SULFUR IN POWDERS AND GRANULES OF NON-OXIDIC CERAMIC RAW AND BASIC MATERIALS - PART 2: INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRY (ICP/OES) OR ION CHROMATOGRAPHY AFTER BURNING IN AN OXYGEN FLOW
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Published date: 10-04-2013
Publisher: Ente Nazionale Italiano di Unificazione (UNI)
Foreword1 Scope2 Normative references3 Terms and definitions4 Principle5 Interferences6 Apparatus7 Reagents8 Sampling and sample preparation9 Preparation10 Calibration11 Performance12 Calculation and report of the results13 Precision14 Test reportAnnex A (informative) - Example of a combustion deviceAnnex B (informative) - Example for suitable operating parameters for the determination of sulfur by ion chromatographyAnnex C (informative) - Example for suitable operating parameters for the determination of sulfur by inductively coupled plasma optical emission spectroscopyAnnex D (informative) - Results of the round-robin testAnnex E (informative) - Information regarding the validation of the uncertainty of the mean valueAnnex F (informative) - Commercial Certified Reference Materials (CRM)Bibliography
Describes a method for the determination of sulfur in powdered and granular non-oxidic ceramic raw materials and materials, which are completely oxidized at a higher temperature in an oxygen atmosphere, e.g. carbon and graphite materials.
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