• ASTM D 7202 : 2015

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

    Standard Test Method for Determination of Beryllium in the Workplace by Extraction and Optical Fluorescence Detection

    Available format(s):  Hardcopy, PDF

    Superseded date:  17-06-2022

    Language(s):  English

    Published date:  13-11-2015

    Publisher:  American Society for Testing and Materials

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    1.1This test method is intended for use in the determination of beryllium by sampling workplace air and surface dust.

    1.2This test method assumes that air and surface samples are collected using appropriate and applicable ASTM International standard practices for sampling of workplace air and surface dust. These samples are typically collected using air filter sampling, vacuum sampling or wiping techniques. See Guide E1370 for guidance on air sampling strategies, and Guide D7659 for guidance on selection of surface sampling techniques.

    1.3Determination of beryllium in soil is not within the scope of this test method. See Test Method D7458 for determination of beryllium in soil samples.

    1.4This test method includes a procedure for extraction (dissolution) of beryllium in weakly acidic medium (pH of 1 % aqueous ammonium bifluoride is 4.8), followed by field analysis of aliquots of the extract solution using a beryllium-specific-optically fluorescent dye.

    1.5The procedure is suitable for on-site use in the field for occupational and environmental hygiene monitoring purposes. The method is also applicable for use in fixed-site laboratories.

    1.6No detailed operating instructions are provided because of differences among various makes and models of suitable fluorometric instruments. Instead, the analyst shall follow the instructions provided by the manufacturer of the particular instrument. This test method does not address comparative accuracy of different devices or the precision between instruments of the same make and model.

    1.7The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.8This test method contains notes that are explanatory and not part of mandatory requirements of the standard.

    1.9This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

    General Product Information - (Show below) - (Hide below)

    Committee D 22
    Document Type Test Method
    Publisher American Society for Testing and Materials
    Status Superseded
    Superseded By
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM D 7659 : 2010 : R2015 Standard Guide for Strategies for Surface Sampling of Metals and Metalloids for Worker Protection
    ASTM D 7707 : 2011 : R2016 Standard Specification for Wipe Sampling Materials for Beryllium in Surface Dust
    ASTM D 8208 : 2019 Standard Practice for Collection of Non-Fibrous Nanoparticles Using a Nanoparticle Respiratory Deposition (NRD) Sampler
    ASTM D 7035 : 2016 Standard Test Method for Determination of Metals and Metalloids in Airborne Particulate Matter by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
    ASTM D 8344 : 2020 Standard Practice for Ammonium Bifluoride and Nitric Acid Digestion of Airborne Dust and Dust-Wipe Samples for the Determination of Metals and Metalloids
    ASTM D 7439 : 2021 Standard Test Method for Determination of Elements in Airborne Particulate Matter by Inductively Coupled Plasma–Mass Spectrometry
    ASTM D 7707 : 2021 Standard Specification for Wipe Sampling Materials for Beryllium in Surface Dust
    ASTM D 7035 : 2021 Standard Test Method for Determination of Metals and Metalloids in Airborne Particulate Matter by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
    ASTM D 8404 : 2021 Standard Practice for Preparation of Soil Samples by Ammonium Bifluoride-Nitric Acid Digestion for Subsequent Analysis for Metals and Metalloids
    ASTM D 7659 : 2021 Standard Guide for Strategies for Surface Sampling of Metals and Metalloids for Worker Protection
    ASTM D 7458 : 2014 Standard Test Method for Determination of Beryllium in Soil, Rock, Sediment, and Fly Ash Using Ammonium Bifluoride Extraction and Fluorescence Detection
    ASTM D 7439 : 2014 Standard Test Method for Determination of Elements in Airborne Particulate Matter by Inductively Coupled Plasma–Mass Spectrometry

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM E 1792 : 2003 Standard Specification for Wipe Sampling Materials for Lead in Surface Dust
    ASTM D 7144 : 2021 Standard Practice for Collection of Surface Dust by Micro-vacuum Sampling for Subsequent Determination of Metals and Metalloids
    ASTM D 4840 : 1999 : R2018 : EDT 1 Standard Guide for Sample Chain-of-Custody Procedures
    ASTM E 1792 : 2003 : R2011 Standard Specification for Wipe Sampling Materials for Lead in Surface Dust
    ASTM E 1792 : 2001 Standard Specification for Wipe Sampling Materials for Lead in Surface Dust
    ASTM E 1792 : 2003 : R2016 Standard Specification for Wipe Sampling Materials for Lead in Surface Dust
    ASTM E 177 : 1990 : REV A : R1996 Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
    ASTM D 4840 : 1999 Standard Guide for Sampling Chain-of-Custody Procedures
    ASTM D 7035 : 2016 Standard Test Method for Determination of Metals and Metalloids in Airborne Particulate Matter by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
    ASTM D 7659 : 2021 Standard Guide for Strategies for Surface Sampling of Metals and Metalloids for Worker Protection
    ASTM D 7296 : 2012 Standard Practice for Collection of Settled Dust Samples Using Dry Wipe Sampling Methods for Subsequent Determination of Beryllium and Compounds
    ASTM D 1356 : 2015 Standard Terminology Relating to Sampling and Analysis of Atmospheres
    ASTM D 6966 : 2018 Standard Practice for Collection of Settled Dust Samples Using Wipe Sampling Methods for Subsequent Determination of Metals
    ASTM E 1370 : 1996 Standard Guide for Air Sampling Strategies for Worker and Workplace Protection
    ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
    ASTM D 7707 : 2021 Standard Specification for Wipe Sampling Materials for Beryllium in Surface Dust
    ASTM D 1356 : 2017 Standard Terminology Relating to Sampling and Analysis of Atmospheres
    ASTM D 7144 : 2005 : REV A : R2011 Standard Practice for Collection of Surface Dust by Micro-vacuum Sampling for Subsequent Metals Determination
    ASTM D 7035 : 2010 Standard Test Method for Determination of Metals and Metalloids in Airborne Particulate Matter by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
    ASTM E 691 : 2020 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM E 1370 : 1996 : R2002 Standard Guide for Air Sampling Strategies for Worker and Workplace Protection
    ASTM D 6966 : 2008 Standard Practice for Collection of Settled Dust Samples Using Wipe Sampling Methods for Subsequent Determination of Metals
    ASTM D 1356 : 2015 : REV B Standard Terminology Relating to Sampling and Analysis of Atmospheres
    ASTM D 7458 : 2008 Standard Test Method for Determination of Beryllium in Soil, Rock, Sediment, and Fly Ash Using Ammonium Bifluoride Extraction and Fluorescence Detection
    ASTM E 691 : 2019 : EDT 1 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM D 7035 : 2021 Standard Test Method for Determination of Metals and Metalloids in Airborne Particulate Matter by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
    ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
    ASTM D 7296 : 2006 Standard Practice for Collection of Settled Dust Samples Using Dry Wipe Sampling Methods for Subsequent Determination of Beryllium and Compounds
    ASTM D 7458 : 2014 Standard Test Method for Determination of Beryllium in Soil, Rock, Sediment, and Fly Ash Using Ammonium Bifluoride Extraction and Fluorescence Detection
    ASTM D 5337 : 2011 : R2016 Standard Practice for Flow Rate Adjustment of Personal Sampling Pumps
    ASTM D 1356 : 2014 : REV A Standard Terminology Relating to Sampling and Analysis of Atmospheres
    ASTM E 1370 : 2014 Standard Guide for Air Sampling Strategies for Worker and Workplace Protection
    ASTM E 1792 : 2002 Standard Specification for Wipe Sampling Materials for Lead in Surface Dust
    ASTM D 7296 : 2018 Standard Practice for Collection of Settled Dust Samples Using Dry Wipe Sampling Methods for Subsequent Determination of Beryllium and Compounds
    ASTM E 691 : 2009 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM D 1193 : 1991 Standard Specification for Reagent Water
    ASTM D 5337 : 1997 Standard Practice for Flow Rate for Calibration of Personal Sampling Pumps
    ASTM D 1356 : 2015 : REV A Standard Terminology Relating to Sampling and Analysis of Atmospheres
    ASTM D 1356 : 2005 : R2010 Standard Terminology Relating to Sampling and Analysis of Atmospheres
    ASTM D 6966 : 2003 Standard Practice for Collection of Settled Dust Samples Using Wipe Sampling Methods for Subsequent Determination of Metals
    ASTM D 7659 : 2010 Standard Guide for Strategies for Surface Sampling of Metals and Metalloids for Worker Protection
    ASTM E 691 : 2021 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM D 1356 : 2020 Standard Terminology Relating to Sampling and Analysis of Atmospheres
    ASTM E 1792 : 2001 : EDT 1 Standard Specification for Wipe Sampling Materials for Lead in Surface Dust
    ASTM D 1356 : 2000 : REV A Standard Terminology Relating to Sampling and Analysis of Atmospheres
    ASTM D 7659 : 2010 : R2015 Standard Guide for Strategies for Surface Sampling of Metals and Metalloids for Worker Protection
    ASTM D 5337 : 2011 Standard Practice for Flow Rate for Calibration of Personal Sampling Pumps
    ASTM D 7707 : 2011 : R2016 Standard Specification for Wipe Sampling Materials for Beryllium in Surface Dust
    ASTM D 1193 : 1970 Standard Specification For Reagent Water
    ASTM D 1356 : 2014 : REV B Standard Terminology Relating to Sampling and Analysis of Atmospheres
    ASTM D 1356 : 2014 Standard Terminology Relating to Sampling and Analysis of Atmospheres
    ASTM E 1370 : 1996 : R2008 Standard Guide for Air Sampling Strategies for Worker and Workplace Protection
    ASTM D 1193 : 2006 Standard Specification for Reagent Water
    ASTM D 1193 : 1999 Standard Specification for Reagent Water
    ASTM E 1370 : 2021 Standard Guide for Air Sampling Strategies for Worker and Workplace Protection
    ASTM E 1792 : 1996 : REV A Standard Specification for Wipe Sampling Materials for Lead in Surface Dust
    ASTM D 5337 : 2004 Standard Practice for Flow Rate for Calibration of Personal Sampling Pumps
    ASTM D 1356 : 2005 Standard Terminology Relating to Sampling and Analysis of Atmospheres
    ASTM D 7035 : 2004 Standard Test Method for Determination of Metals and Metalloids in Airborne Particulate Matter by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
    ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
    ASTM D 7144 : 2005 Standard Practice for Collection of Surface Dust by Micro-vacuum Sampling for Subsequent Metals Determination
    ASTM D 6966 : 2013 Standard Practice for Collection of Settled Dust Samples Using Wipe Sampling Methods for Subsequent Determination of Metals
    ASTM D 7144 : 2005 : REV A Standard Practice for Collection of Surface Dust by Micro-vacuum Sampling for Subsequent Metals Determination
    ASTM D 7144 : 2005 : REV A : R2016 Standard Practice for Collection of Surface Dust by Micro-vacuum Sampling for Subsequent Metals Determination
    ASTM D 7707 :2011 Standard Specification for Wipe Sampling Materials for Beryllium in Surface Dust
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