• BS EN 14185-2:2006

    Current The latest, up-to-date edition.

    Non fatty foods. Determination of N-methylcarbamate residues HPLC method with clean-up on a diatomaceous earth column

    Available format(s):  Hardcopy, PDF

    Language(s):  English

    Published date:  30-06-2006

    Publisher:  British Standards Institution

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    1 Scope
    2 Principle
    3 Reagents
    4 Apparatus
    5 Sampling
    6 Preparation of the samples
    7 Procedure
    8 Calculation of the results
    9 Confirmatory tests
    10 Precision, Repeatability and Reproducibility
    11 Test report
    Annex A (informative) Precision Data
    Bibliography

    Abstract - (Show below) - (Hide below)

    Specifies a high performance liquid chromatographic (HPLC) method for the determination of residues of N-methylcarbamate pesticides in fruits and vegetables and is based on the method of Krause.

    Scope - (Show below) - (Hide below)

    This draft European Standard specifies a high performance liquid chromatographic (HPLC) method for the determination of residues of N-methylcarbamate pesticides in fruits and vegetables and is based on the method of Krause [1]. The method has been validated by collaborative study for aldicarb, carbofuran, furathiocarb, methomyl, oxamyl, propoxur and thiodicarb parent compounds and for the metabolites aldicarb sulfoxide, aldicarb sulfone (aldoxycarb) and 3-hydroxy-carbofuran in tomatoes and oranges at levels between 0,04 mg/kg and 0,25 mg/kg. No collaborative data are available for the performance of the method in the determination of other significant compounds although it is known that the method is unsatisfactory for benfuracarb.

    General Product Information - (Show below) - (Hide below)

    Committee AW/275
    Development Note Supersedes 04/30124414 DC (06/2006)
    Document Type Standard
    Publisher British Standards Institution
    Status Current
    Supersedes

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 5725-1:1994 Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions
    ISO 5725-3:1994 Accuracy (trueness and precision) of measurement methods and results — Part 3: Intermediate measures of the precision of a standard measurement method
    ISO 5725-6:1994 Accuracy (trueness and precision) of measurement methods and results — Part 6: Use in practice of accuracy values
    ISO 5725-4:1994 Accuracy (trueness and precision) of measurement methods and results Part 4: Basic methods for the determination of the trueness of a standard measurement method
    ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
    ISO 5725-5:1998 Accuracy (trueness and precision) of measurement methods and results — Part 5: Alternative methods for the determination of the precision of a standard measurement method
    ISO 1750:1981 Pesticides and other agrochemicals — Common names
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