• BS EN 15944:2010

    Current The latest, up-to-date edition.

    Liquid petroleum products. Determination of nickel and vanadium content. Inductively coupled plasma optical emission spectrometry method (ICP OES)

    Available format(s):  Hardcopy, PDF

    Language(s):  English

    Published date:  30-11-2010

    Publisher:  British Standards Institution

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    1 Scope
    2 Normative references
    3 Principle
    4 Reagents
    5 Apparatus
    6 Sampling
    7 Preparation of calibration solutions
    8 Calibration
    9 Sample analysis
    10 Calculation
    11 Expression of results
    12 Precision
    13 Test report
    Bibliography

    Abstract - (Show below) - (Hide below)

    Defines an inductively coupled plasma optical emission spectrometry (ICP OES) method for the determination of nickel content in the range 4 mg/kg to 55 mg/kg and of vanadium content in the range 4 mg/kg to 150 mg/kg in fuel oils and residual fuel oils.

    Scope - (Show below) - (Hide below)

    This European Standard specifies an inductively coupled plasma optical emission spectrometry (ICP OES) method for the determination of nickel content in the range 4 mg/kg to 55 mg/kg and of vanadium content in the range 4 mg/kg to 150 mg/kg in fuel oils and residual fuel oils.

    NOTE 1 Nickel content can be determined from 2 mg/kg to 4 mg/kg and vanadium content can be determined from 1 mg/kg to 4 mg/kg. However, the precision was not established as no samples with nickel and vanadium contents in these ranges were included in the interlaboratory test. Nickel and vanadium contents higher than those reported can be determined after sample dilution. However, the precision was not established for diluted samples.

    NOTE 2 For the purposes of this European Standard, the term “% (V/V)?? is used to represent the volume fraction (φ).

    WARNING — The use of this standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.

    General Product Information - (Show below) - (Hide below)

    Committee PTI/13
    Development Note Also numbered as BS 2000-587(2010). Supersedes 09/30201423 DC. (12/2010)
    Document Type Standard
    Publisher British Standards Institution
    Status Current
    Supersedes

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 3171:1988 Petroleum liquids — Automatic pipeline sampling
    ISO 3170:2004 Petroleum liquids — Manual sampling
    ISO 1042:1998 Laboratory glassware One-mark volumetric flasks
    EN ISO 1042 : 1999 LABORATORY GLASSWARE - ONE-MARK VOLUMETRIC FLASKS
    DIN 51790-6:2007-11 TESTING OF LIQUID FUELS - DETERMINATION OF THE VANADIUM AND NICKEL CONTENT - PART 6: DIRECT DETERMINATION BY OPTICAL EMISSION SPECTRAL ANALYSIS WITH INDUCTIVELY COUPLED PLASMA (ICP OES)
    ISO 4259:2006 Petroleum products Determination and application of precision data in relation to methods of test
    EN 13131:2000 Liquid petroleum products - Determination of nickel and vanadium content - Atomic absorption spectrometric method
    EN ISO 3170:2004 Petroleum liquids - Manual sampling (ISO 3170:2004)
    EN ISO 3171:1999 Petroleum liquids - Automatic pipeline sampling (ISO 3171:1988)
    EN ISO 4259:2006 Petroleum products - Determination and application of precision data in relation to methods of test (ISO 4259:2006)
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