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  • DIN EN 16691 E : 2015

    Current The latest, up-to-date edition.

    WATER QUALITY - DETERMINATION OF SELECTED POLYCYCLIC AROMATIC HYDROCARBONS (PAH) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS)

    Available format(s):  Hardcopy, PDF

    Language(s):  English

    Published date:  01-01-2015

    Publisher:  German Institute for Standardisation (Deutsches Institut für Normung)

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    Table of Contents - (Show below) - (Hide below)

    National foreword
    National Annex NA (informative) - Bibliography
    European foreword
    1 Scope
    2 Normative references
    3 Principle
    4 Interferences
    5 Reagents
    6 Apparatus
    7 Sampling
    8 Procedure
    9 Calibration
    10 Measurement of samples
    11 Identification of individual compounds by
       means of GC-MS (SIM)
    12 Calculation
    13 Expression of results
    14 Test report
    Annex A (informative) - Suitable gas chromatographic
            conditions and example chromatograms -
            GC-conditions
    Annex B (informative) - Repeatability and reproducibility
            data
    Annex C (informative) - Dilution Schedules for standards
    Annex D (informative) - Silica clean-up
    Annex E (informative) - Examples of suitable solid-phase
            extraction disks (SPE-disks)
    Bibliography

    Abstract - (Show below) - (Hide below)

    Defines a method for the determination of 7 polycyclic aromatic hydrocarbons (PAH) in whole water samples listed in Table 1.

    General Product Information - (Show below) - (Hide below)

    Document Type Standard
    Publisher German Institute for Standardisation (Deutsches Institut für Normung)
    Status Current

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 7981-1:2005 Water quality Determination of polycyclic aromatic hydrocarbons (PAH) Part 1: Determination of six PAH by high-performance thin-layer chromatography with fluorescence detection after liquid-liquid extraction
    EN ISO 17993 : 2003 WATER QUALITY - DETERMINATION OF 15 POLYCYCLIC AROMATIC HYDROCARBONS (PAH) IN WATER BY HPLC WITH FLUORESCENCE DETECTION AFTER LIQUID-LIQUID EXTRACTION
    NEN 7777 : 2011 + C1 2012 ENVIRONMENT AND FOOD - PERFORMANCE CHARACTERISTICS OF MEASUREMENT METHODS
    DIN ISO 5725-2:2002-12 Accuracy (trueness and precision) of measurement methods and results - Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method (ISO 5725-2:1994 including Technical Corrigendum 1:2002)
    ISO 1042:1998 Laboratory glassware One-mark volumetric flasks
    ISO/TS 13530:2009 Water quality — Guidance on analytical quality control for chemical and physicochemical water analysis
    ISO 22892:2006 Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry
    ISO 7981-2:2005 Water quality Determination of polycyclic aromatic hydrocarbons (PAH) Part 2: Determination of six PAH by high-performance liquid chromatography with fluorescence detection after liquid-liquid extraction
    ISO 17993:2002 Water quality — Determination of 15 polycyclic aromatic hydrocarbons (PAH) in water by HPLC with fluorescence detection after liquid-liquid extraction
    DIN ISO 28540:2014-05 Water quality - Determination of 16 polycyclic aromatic hydrocarbons (PAH) in water - Method using gas chromatography with mass spectrometric detection (GC-MS) (ISO 28540:2011)
    ISO 5667-3:2012 Water quality Sampling Part 3: Preservation and handling of water samples
    EN ISO 1042 : 1999 LABORATORY GLASSWARE - ONE-MARK VOLUMETRIC FLASKS
    ISO 5667-1:2006 Water quality Sampling Part 1: Guidance on the design of sampling programmes and sampling techniques
    ISO 28540:2011 Water quality — Determination of 16 polycyclic aromatic hydrocarbons (PAH) in water — Method using gas chromatography with mass spectrometric detection (GC-MS)
    ISO 6107-2:2006 Water quality Vocabulary Part 2:
    ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
    EN ISO 5667-3:2012 Water quality - Sampling - Part 3: Preservation and handling of water samples (ISO 5667-3:2012)
    ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
    ISO 8466-1:1990 Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function
    EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
    EN ISO 22892:2011 Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006)
    EN 15527:2008 Characterization of waste - Determination of polycyclic aromatic hydrocarbons (PAH) in waste using gas chromatography mass spectrometry (GC/MS)
    ISO/TS 28581:2012 Water quality — Determination of selected non-polar substances — Method using gas chromatography with mass spectrometric detection (GC-MS)
    EN ISO 5667-1 : 2006 COR 2007 WATER QUALITY - SAMPLING - PART 1: GUIDANCE ON THE DESIGN OF SAMPLING PROGRAMMES AND SAMPLING TECHNIQUES
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