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  • PREN 17212 : DRAFT 2017

    Current The latest, up-to-date edition.

    ANIMAL FEEDING STUFFS: METHODS OF SAMPLING AND ANALSYSIS - DETERMINATION OF MELAMINE AND CYANURIC ACID CONTENT BYLIQUID CHROMATOGRAPHIC METHOD WITH MASS SPECTROMETRIC DETECTION (LC-MS/MS)

    Available format(s): 

    Language(s): 

    Published date:  09-01-2018

    Publisher:  Comite Europeen de Normalisation

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    Table of Contents - (Show below) - (Hide below)

    European foreword
    Introduction
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Principle
    5 Reagents
    6 Apparatus
    7 Preparation of sample
    8 Procedure
    9 HPLC-MS/MS analysis
    10 Calculation
    11 Precision
    12 Test report
    Annex A (informative) - Examples for suitable MS detection
            conditions
    Annex B (informative) - Results of the international
            collaborative trial
    Annex C (informative) - Results of the in-house validation
            of the method
    Annex D (informative) - Typical chromatograms
    Bibliography

    Abstract - (Show below) - (Hide below)

    Provides a high-performance liquid chromatographic (HPLC) mass spectrometric (MS) method for screening and quantification of melamine in the concentration range between < 1 mg/kg and 100 mg/kg feed.

    General Product Information - (Show below) - (Hide below)

    Comment Closes On
    Committee TC 327
    Document Type Draft
    Publisher Comite Europeen de Normalisation
    Status Current

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 5725-1:1994 Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions
    ISO 11843-2:2000 Capability of detection — Part 2: Methodology in the linear calibration case
    ISO 24276:2006 Foodstuffs Methods of analysis for the detection of genetically modified organisms and derived products General requirements and definitions
    EN ISO/IEC 17043:2010 Conformity assessment - General requirements for proficiency testing (ISO/IEC 17043:2010)
    ISO 6497:2002 Animal feeding stuffs Sampling
    ISO/IEC Guide 99:2007 International vocabulary of metrology Basic and general concepts and associated terms (VIM)
    ISO 3534-2:2006 Statistics Vocabulary and symbols Part 2: Applied statistics
    ISO/IEC 17043:2010 Conformity assessment — General requirements for proficiency testing
    EN ISO 6498:2012 Animal feeding stuffs - Guidelines for sample preparation (ISO 6498:2012)
    ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
    EN ISO 6497 : 2005 ANIMAL FEEDING STUFFS - SAMPLING
    ISO 6498:2012 Animal feeding stuffs — Guidelines for sample preparation
    ISO 16577:2016 Molecular biomarker analysis — Terms and definitions
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