• BS EN 1601:2017

    Current The latest, up-to-date edition.

    Liquid petroleum products. Determination of organic oxygenate compounds and total organically bound oxygen content in unleaded petrol. Method by gas chromatography (O-FID)

    Available format(s):  Hardcopy, PDF

    Language(s):  English

    Published date:  14-09-2017

    Publisher:  British Standards Institution

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    Table of Contents - (Show below) - (Hide below)

    European foreword
    Introduction
    1 Scope
    2 Normative references
    3 Principle
    4 Reagents and materials
    5 Apparatus
    6 Sampling
    7 Procedure
    8 Calculation
    9 Procedure for the determination of a higher
       oxygenate compound content
    10 Total organically bound oxygen content
    11 Expression of results
    12 Precision
    13 Test report
    Annex A (informative) - Guidance on the oxygen selective
            detection (O-FID) technique
    Bibliography

    Abstract - (Show below) - (Hide below)

    Defines a gas chromatographic method for the quantitative determination, in unleaded petrol having a final boiling point not greater than 220 degrees C, of individual organic oxygenate compounds in the range 0,17% (m/m) to 15% (m/m) in a direct analysis (without dilution), and total organically bound oxygen up to 3,9% (m/m).

    Scope - (Show below) - (Hide below)

    This European Standard specifies a gas chromatographic method for the quantitative determination, in unleaded petrol having a final boiling point not greater than 220 °C, of individual organic oxygenate compounds in the range 0,17 % (m/m) to 15 % (m/m) in a direct analysis (without dilution), and total organically bound oxygen up to 3,9 % (m/m). For samples for which one of the oxygenate compounds content is higher than 15 % (m/m), a procedure with a dilution of the sample before the analysis is given. NOTE 1 The conversion from percent mass to percent volume is done using the calculation mentioned in 8.3 and 9.5.3. NOTE 2 Precision data are not available for an oxygenate compound content higher than 15 % (m/m); see Introduction. NOTE 3 For the purposes of this European Standard, the terms \'% (m/m)\' and \'% (V/V)\' are used to represent respectively the mass fraction, µ, respectively the volume fraction, ?. WARNING - The use of this European Standard can involve hazardous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of users of this European Standard to take appropriate measures to ensure the safety and health of personnel prior to application of the standard, and fulfil statutory and regulatory requirements for this purpose.

    General Product Information - (Show below) - (Hide below)

    Committee PTI/13
    Development Note Supersedes 94/504465 DC. (03/2005) 2014 Edition is dual-numbered as BS 2000-408(2014). Supersedes BS 2000-408(1997) & 12/30264358 DC. (09/2014) Supersedes 16/30339201 DC. (09/2017)
    Document Type Standard
    Publisher British Standards Institution
    Status Current
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    BS 7800:2006 Automotive fuel. High octane (super) unleaded petrol. Specification
    BS 7800:2000 Automotive fuel. High octane (super) unleaded petrol. Specification
    BS 4040:2001 Specification for leaded petrol (gasoline) for motor vehicles

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 3171:1988 Petroleum liquids — Automatic pipeline sampling
    EN 228:2012+A1:2017 Automotive fuels - Unleaded petrol - Requirements and test methods
    ISO 3170:2004 Petroleum liquids — Manual sampling
    ISO 3675:1998 Crude petroleum and liquid petroleum products Laboratory determination of density Hydrometer method
    EN ISO 12185:1996 Crude petroleum and petroleum products - Determination of density - Oscillating U-tube method (ISO 12185:1996)
    EN ISO 3675:1998 Crude petroleum and liquid petroleum products - Laboratory determination of density - Hydrometer method (ISO 3675:1998)
    ISO 12185:1996 Crude petroleum and petroleum products — Determination of density — Oscillating U-tube method
    ISO 3838:2004 Crude petroleum and liquid or solid petroleum products Determination of density or relative density Capillary-stoppered pyknometer and graduated bicapillary pyknometer methods
    ISO 4259:2006 Petroleum products Determination and application of precision data in relation to methods of test
    EN ISO 3170:2004 Petroleum liquids - Manual sampling (ISO 3170:2004)
    EN ISO 3838:2004 Crude petroleum and liquid or solid petroleum products - Determination of density or relative density - Capillary-stoppered pyknometer and graduated bicapillary pyknometer methods (ISO 3838:2004)
    EN ISO 3171:1999 Petroleum liquids - Automatic pipeline sampling (ISO 3171:1988)
    EN ISO 4259:2006 Petroleum products - Determination and application of precision data in relation to methods of test (ISO 4259:2006)
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