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CHEMICAL ANALYSIS OF REFRACTORY PRODUCTS BY X-RAY FLUORESCENCE (XRF) - FUSED CAST-BEAD METHOD
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Published date: 25-10-2011
Publisher: Ente Nazionale Italiano di Unificazione (UNI)
Foreword1 Scope2 Normative references 3 Types of material 4 Principle 5 Apparatus 6 Sample grinding7 Loss on ignition (and/or drying) 8 Flux 9 Fusion casting procedures10 Calibration11 Corrections12 Reproducibility and repeatability13 Accuracy determined by certified reference materials14 Definitions of limits of detection15 Test reportAnnex A (normative) - Calibration range and required detection limitsAnnex B (normative) - Corrections for tungsten carbide grinding mediaAnnex C (informative) - Examples of fluxes/flux ratiosAnnex D (normative) - Examples of CRM to be used to check synthetic calibrationsAnnex E (normative) - Examples of SeRMAnnex F (normative) - Equation for theoretical calculationsAnnex G (normative) - Certified reference materials (CRMs)Annex H (normative) - Method of inter-element correction used to compensate for the effects of co-existing components when using SeRM for calibrationAnnex I (normative) - Standard deviations achieved with certified reference materialsBibliography
Describes a method for the chemical analysis of refractory and technical ceramic raw materials, intermediates and products, by means of the X-ray fluorescence (XRF) fused cast-bead method.
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