• ISO 14388-3:2014

    Current The latest, up-to-date edition.

    Soil quality Acid-base accounting procedure for acid sulfate soils Part 3: Suspension peroxide oxidation combined acidity and sulfur (SPOCAS) methodology

    Available format(s):  Hardcopy, PDF, PDF 3 Users, PDF 5 Users, PDF 9 Users

    Language(s):  French, English

    Published date:  24-07-2014

    Publisher:  International Organization for Standardization

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    Abstract - (Show below) - (Hide below)

    ISO 14388-3:2014 specifies a suite of methods used to determine net acidity in acid sulfate soils. ISO 14388-3:2014 specifies a method for the determination of pH in a 1 mol/l potassium chloride soil suspension (pHKCl) and where required, titratable actual acidity (TAA). Following this, potassium chloride extractable sulfur (SKCl), calcium (CaKCl) and magnesium (MgKCl) are determined. On a separate test portion, following digestion with 30 % hydrogen peroxide, peroxide pH (pHOX), titratable peroxide acidity (TPA) and excess acid neutralizing capacity (ANCE) are determined. Following this, peroxide sulfur (SP), calcium (CaP) and magnesium (MgP) are determined. On samples where jarosite is present, or where pHKCl is < 4,5, residual acid soluble sulfur (SRAS) is determined on the soil residue remaining after peroxide digestion. Titratable sulfidic acidity (TSA), reacted calcium (CaA), reacted magnesium (MgA) and peroxide oxidizable sulfur (SPOS) are then determined by difference. For peat samples containing substantial levels of organic sulfur, the SPOCAS suite is generally unsuitable for estimating sulfide content, and the chromium reducible suite of procedures should be used instead.

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    Development Note Supersedes ISO/DIS 14388-3. (07/2014)
    Document Type Standard
    Publisher International Organization for Standardization
    Status Current

    Standards Referenced By This Book - (Show below) - (Hide below)

    ISO 14388-1:2014 Soil quality Acid-base accounting procedure for acid sulfate soils Part 1: Introduction and definitions, symbols and acronyms, sampling and sample preparation
    BS ISO 14388-1:2014 Soil quality. Acid-base accounting procedure for acid sulfate soils Introduction and definitions, symbols and acronyms, sampling and sample preparation

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 14254:2001 Soil quality Determination of exchangeable acidity in barium chloride extracts
    ISO 8655-5:2002 Piston-operated volumetric apparatus Part 5: Dispensers
    ISO 8655-1:2002 Piston-operated volumetric apparatus Part 1: Terminology, general requirements and user recommendations
    ISO 1042:1998 Laboratory glassware One-mark volumetric flasks
    ISO 648:2008 Laboratory glassware — Single-volume pipettes
    ISO 835:2007 Laboratory glassware — Graduated pipettes
    ISO 8655-2:2002 Piston-operated volumetric apparatus Part 2: Piston pipettes
    ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
    ISO 8655-3:2002 Piston-operated volumetric apparatus Part 3: Piston burettes
    ISO 14388-1:2014 Soil quality Acid-base accounting procedure for acid sulfate soils Part 1: Introduction and definitions, symbols and acronyms, sampling and sample preparation
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