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    S.R. CEN/TS 15968:2010

    Current The latest, up-to-date edition.

    DETERMINATION OF EXTRACTABLE PERFLUOROOCTANESULPHONATE (PFOS) IN COATED AND IMPREGNATED SOLID ARTICLES, LIQUIDS AND FIRE FIGHTING FOAMS - METHOD FOR SAMPLING, EXTRACTION AND ANALYSIS BY LC-QMS OR LC-TANDEM/MS

    Available format(s):  Hardcopy, PDF

    Language(s):  English

    Published date:  01-01-2010

    Publisher:  National Standards Authority of Ireland

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    Introduction
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Symbols and abbreviations
    5 Principle
    6 Apparatus and Reagents
    7 Sampling
    8 Sample pre-treatment
    9 Extraction
    10 Interference with LC-tandemMS
    11 Analysis
    12 System suitability test
    14 Expression of results
    15 Test report
    Annex A (informative) - LC-QMS and LC-TOFMS
    Annex B (informative) - Sampling of liquids (example)
    Annex C (informative) - Confirmation of compound
            identity by MS methods
    Bibliography

    Abstract - (Show below) - (Hide below)

    Specifies the determination of perfluorooctanesulfonate (PFOS) in concentrated extracts from coated and impregnated solid articles, liquids and fire extinguishing foams using high performance liquid chromatography-tandem mass spectrometry (LC-tandemMS) or quadrupole mass spectrometry (LC-qMS).

    General Product Information - (Show below) - (Hide below)

    Document Type Standard
    Publisher National Standards Authority of Ireland
    Status Current

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 15194:2009 In vitro diagnostic medical devices Measurement of quantities in samples of biological origin Requirements for certified reference materials and the content of supporting documentation
    ISO 6427:2013 Plastics — Determination of matter extractable by organic solvents (conventional methods)
    EN ISO 6427:2014 Plastics - Determination of matter extractable by organic solvents (conventional methods) (ISO 6427:2013)
    EN ISO 8130-9:1999 Coating powders - Part 9: Sampling (ISO 8130-9:1992)
    ISO 187:1990 Paper, board and pulps — Standard atmosphere for conditioning and testing and procedure for monitoring the atmosphere and conditioning of samples
    ISO 25101:2009 Water quality Determination of perfluorooctanesulfonate (PFOS) and perfluorooctanoate (PFOA) Method for unfiltered samples using solid phase extraction and liquid chromatography/mass spectrometry
    ISO 9113:1986 Plastics Polypropylene (PP) and propylene-copolymer thermoplastics Determination of isotactic index
    EN 20187:1993 Paper, board and pulps - Standard atmosphere for conditioning and testing and procedure for monitoring the atmosphere and conditioning of samples (ISO 187:1990)
    ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
    ISO 8466-1:1990 Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function
    EN ISO 2419:2012 Leather - Physical and mechanical tests - Sample preparation and conditioning (ISO 2419:2012)
    EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
    ISO 8130-9:1992 Coating powders Part 9: Sampling
    ISO 2419:2012 Leather — Physical and mechanical tests — Sample preparation and conditioning
    EN 12127:1997 Textiles - Fabrics - Determination of mass per unit area using small samples
    EN ISO 15194:2009 In vitro diagnostic medical devices - Measurement of quantities in samples of biological origin - Requirements for certified reference materials and the content of supporting documentation (ISO 15194:2009)
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