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    I.S. EN 17425:2021

    Current The latest, up-to-date edition.

    Foodstuffs - Determination of ergot alkaloids in cereals and cereal products by dSPE clean-up and HPLC-MS/MS

    Available format(s):  Hardcopy, PDF

    Language(s):  English

    Published date:  06-05-2021

    Publisher:  National Standards Authority of Ireland

    For Harmonized Standards, check the EU site to confirm that the Standard is cited in the Official Journal.
    Only cited Standards give presumption of conformance to New Approach Directives/Regulations.

    Dates of withdrawal of national standards are available from NSAI.

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    Table of Contents - (Show below) - (Hide below)

    European foreword
    Introduction
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Principle
    5 Reagents
    6 Apparatus and equipment
    7 Procedure
    8 LC-MS/MS analysis
    9 Calculation
    10 Precision
    11 Test report
    Annex A (informative) Example conditions for suitable LC-MS/MS systems
    Annex B (informative) Typical chromatograms
    Annex C (informative) Precision data
    Annex D (informative) Data comparison
    Bibliography

    Abstract - (Show below) - (Hide below)

    This document describes a method for the determination of the sum of six ergot alkaloids (ergocornine, ergometrine, ergocristine, ergotamine, ergosine and ergocryptine) and their -inine epimer pairs by liquid chromatography coupled with tandem mass spectrometry (LC-MS/MS) after clean-up by dispersive solid phase extraction (dSPE).

    General Product Information - (Show below) - (Hide below)

    Committee CEN/TC 275
    Document Type Standard
    Product Note The date of any NSAI previous adoption may not match the date of its original CEN/CENELEC document.
    Publisher National Standards Authority of Ireland
    Status Current
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