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  • DIN EN 14902:2005-10

    Current The latest, up-to-date edition.

    AMBIENT AIR QUALITY - STANDARD METHOD FOR THE MEASUREMENT OF PB, CD, AS AND NI IN THE PM10 FRACTION OF SUSPENDED PARTICULATE MATTER

    Available format(s):  Hardcopy, PDF

    Language(s): 

    Published date:  01-01-2005

    Publisher:  German Institute for Standardisation (Deutsches Institut für Normung)

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    1 Scope
    2 Normative references
    3 Terms, definitions and abbreviations
    4 Principle
    5 Requirements
    6 Reagents and gases
    7 Apparatus
    8 Sampling
    9 Analysis
    10 Quality control
    11 Calculation of results
    12 Estimation of the measurement uncertainty of the method
    13 Performance characteristics determined in field tests
    14 Reporting of results
    Annex A (informative) Examples of closed vessel microwave
                           digestion procedures
    Annex B (informative) Typical laboratory filter blank values
                           as determined in the field validation
                           tests
    Annex C (informative) Analytical interferences
    Annex D (informative) Approach to uncertainty estimation used
                           in the field validation tests
    Annex E (normative) List of minimum QA/QC procedures
    Annex F (informative) Procedure for the determination of the
                           uncertainty of the method for an
                           individual laboratory
    Annex ZA (informative) Relationship with EU Directives
    Bibliography

    Abstract - (Show below) - (Hide below)

    Describes a method for the determination of particulate lead (Pb), cadmium (Cd), arsenic (As) and nickel (Ni) in ambient air that can be used in the framework of the European Council Directive on Ambient Air Quality Assessment and Management and the 1st and 4th Daughter Directives.

    General Product Information - (Show below) - (Hide below)

    Document Type Standard
    Publisher German Institute for Standardisation (Deutsches Institut für Normung)
    Status Current

    Standards Referenced By This Book - (Show below) - (Hide below)

    VDI 2267 Blatt 1:2012-10 Determination of suspended matter in ambient air - Measurement of the element concentration after sampling on filters - Determination of Al, As, Ba, Ca, Cd, Co, Cr, Cu, Fe, K, Mg, Mn, Na, Ni, Pb, Sb, Se, Sn, Tl, V and Zn by graphite furnace atomic absorption spectrometry (GF-AAS), by optical emission spectrometry with inductively coupled plasma (ICP-OES) and inductively coupled plasma mass spectrometry (ICP-MS)
    VDI 2267 Blatt 12:2008-10 Determination of suspended matter in ambient air - Measurement of As, Ca, Cd, Co, Cr, Cu, Fe, Mn, Ni, Pb, Sb and Zn by energy dispersive X-ray fluorescense (ED XRF)
    VDI 2463 Blatt 7:2014-05 Particulate matter measurement - Determination of suspended particulate matter and gaseous chemical compounds in ambient air and indoor air - Active sampling via low-volume sampler (LVS)
    VDI 2267 Blatt 3:2015-03 Determination of suspended matter in ambient air - Digestion variants for dust samples for the subsequent determination of the mass concentration of Al, Sb, As, Pb, Cd, Ca, Cr, Co, Fe, K, Cu, Mg, Mn, Na, Ni, Se, V and Zn
    DIN EN 12341:2014-08 Ambient air - Standard gravimetric measurement method for the determination of the PM or PM mass concentration of suspended particulate matter
    DIN EN 16450:2015-10 (Draft) AMBIENT AIR - AUTOMATED MEASURING SYSTEMS FOR THE MEASUREMENT OF THE CONCENTRATION OF PARTICULATE MATTER (PM10; PM2,5)
    DIN EN 16913:2015-10 (Draft) AMBIENT AIR - STANDARD METHOD FOR MEASUREMENT OF NO[3][-], SO[4][2-], CL[-], NH[4][+], NA[+], K[+], MG[2+], CA[2+] IN PM2,5 AS DEPOSITED ON FILTERS

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO/IEC 17025:2005 General requirements for the competence of testing and calibration laboratories
    EN 13274-7:2008 Respiratory protective devices - Methods of test - Part 7: Determination of particle filter penetration
    NFT 90 210 : 2009 WATER QUALITY - PROTOCOL FOR THE INITIAL METHOD PERFORMANCE ASSESSMENT IN A LABORATORY
    VDI 2449 Blatt 1:1995-02 Measurement methods test criteria - Determination of performance characteristics for the measurement of gaseous pollutants (immission)
    EN 1822-5:2009 High efficiency air filters (EPA, HEPA and ULPA) - Part 5: Determining the efficiency of filter elements
    VDI 2267 Blatt 5:1997-11 Determination of suspended matter in ambient air - Determination of the mass concentration of Be, Cd, Co, Cr, Cu, Fe, Mn, Ni, Pb, Sb, V, Zn by optical emission spectrometry (ICP-OES) after sampling on filters and digestion in an oxidising agent
    ISO 5725-4:1994 Accuracy (trueness and precision) of measurement methods and results Part 4: Basic methods for the determination of the trueness of a standard measurement method
    DIN 32645:2008-11 CHEMICAL ANALYSIS - DECISION LIMIT, DETECTION LIMIT AND DETERMINATION LIMIT UNDER REPEATABILITY CONDITIONS - TERMS, METHODS, EVALUATION
    VDI 2267 Blatt 11:1986-01 Determination of suspended particulates in ambient air; measurement of the mass concentration of lead by energy dispersive X-ray fluorescence-analysis
    VDI 2267 Blatt 15:2005-11 Determination of suspended matter in ambient air - Measurement of the mass concentration of Al, As, Ca, Cd, Co, Cr, Cu, K, Mn, Ni, Pb, Sb, V, Zn as part of dust precipitation by mass spectrometry (ICP-MS)
    VDI 2267 Blatt 7:1988-11 Chemical analysis of particulates in ambient air; determination of thallium and its inorganic compounds as part of the dust precipitation by atomic absorption spectrometry
    ENV 13005 : DRAFT 1999 GUIDE TO THE EXPRESSION OF UNCERTAINTY IN MEASUREMENT
    VDI 2267 Blatt 9:2002-07 Determination of suspended particulates matter in ambient air - Measurement of the mass concentration of mercury - Sampling by sorption as amalgam and determination by atomic fluorescense spectrometry (AFS) with cold vapour technique
    VDI 2267 Blatt 4:1987-03 Chemical analysis of particulates in ambient air; determination of lead, cadmium and their inorganic compounds as part of the dust precipitation by atomic absorption spectrometry
    DIN ISO 5725-4:2003-01 ACCURACY (TRUENESS AND PRECISION) OF MEASUREMENT METHODS AND RESULTS - PART 4: BASIC METHODS FOR THE DETERMINATION OF THE TRUENESS OF A STANDARD MEASUREMENT METHOD
    ISO 6955:1982 Analytical spectroscopic methods Flame emission, atomic absorption, and atomic fluorescence Vocabulary
    VDI 2267 Blatt 1:2012-10 Determination of suspended matter in ambient air - Measurement of the element concentration after sampling on filters - Determination of Al, As, Ba, Ca, Cd, Co, Cr, Cu, Fe, K, Mg, Mn, Na, Ni, Pb, Sb, Se, Sn, Tl, V and Zn by graphite furnace atomic absorption spectrometry (GF-AAS), by optical emission spectrometry with inductively coupled plasma (ICP-OES) and inductively coupled plasma mass spectrometry (ICP-MS)
    CR 14377:2002 Air quality - Approach to uncertainty estimation for ambient air reference measurement methods
    EN 12341:2014 Ambient air - Standard gravimetric measurement method for the determination of the PM10 or PM2,5 mass concentration of suspended particulate matter
    VDI 2267 Blatt 14:2003-12 Determination of suspended matter in ambient air - Measurement of Al, As, Ca, Cd, Co, Cr, Cu, Fe, K, Mg, Mn, Na, Ni, Pb, V, Zn as part of dust deposition by optical emission spectrometry (ICP OES)
    VDI 2267 Blatt 2:1983-02 Determination of suspended particulates in ambient air; measurement of lead by X-ray fluorescence
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