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  • EN 14902:2005/AC:2006

    Current The latest, up-to-date edition.

    AMBIENT AIR QUALITY - STANDARD METHOD FOR THE MEASUREMENT OF PB, CD, AS AND NI IN THE PM10 FRACTION OF SUSPENDED PARTICULATE MATTER

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    Published date:  18-10-2006

    Publisher:  Comite Europeen de Normalisation

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    1 Scope
    2 Normative references
    3 Terms, definitions and abbreviations
    4 Principle
    5 Requirements
    6 Reagents and gases
    7 Apparatus
    8 Sampling
    9 Analysis
    10 Quality control
    11 Calculation of results
    12 Estimation of the measurement uncertainty of the method
    13 Performance characteristics determined in field tests
    14 Reporting of results
    Annex A (informative) - Examples of closed vessel microwave
            digestion procedures
    Annex B (informative) - Typical laboratory filter blank values
            as determined in the field validation tests
    Annex C (informative) - Analytical interferences
    Annex D (informative) - Approach to uncertainty estimation used
            in the field validation tests
    Annex E (normative) - List of minimum QA/QC procedures
    Annex F (informative) Procedure for the determination of the
            uncertainty of the method for an individual laboratory
    Annex ZA (informative) - Relationship with EU Directives
    Bibliography

    Abstract - (Show below) - (Hide below)

    Describes a method for the determination of particulate lead (Pb), cadmium (Cd), arsenic (As) and nickel (Ni) in ambient air that can be used in the framework of the European Council Directive on Ambient Air Quality Assessment and Management and the 1st and 4th Daughter Directives.

    General Product Information - (Show below) - (Hide below)

    Committee TC 264
    Document Type Standard
    Publisher Comite Europeen de Normalisation
    Status Current

    Standards Referenced By This Book - (Show below) - (Hide below)

    BS ISO 21438-3:2010 Workplace atmospheres. Determination of inorganic acids by ion chromatography Hydrofluoric acid and particulate fluorides
    08/30182314 DC : DRAFT JULY 2008 BS EN 15841 - AIR QUALITY - AMBIENT AIR - DETERMINATION OF LEAD, NICKEL, ARSENIC AND CADMIUM IN ATMOSPHERIC DEPOSITION
    15/30314073 DC : 0 BS 16913 - AMBIENT AIR - STANDARD METHOD FOR MEASUREMENT OF NO[3][-], SO[4][2-], CL[-], NH[4][+], NA[+], K[+], MG[2+], CA[2+] IN PM2,5
    UNI EN 15836-2 : 2010 PLASTICS - PLASTICIZED POLY(VINYL CHLORIDE) (PVC-P) MEMBRANES FOR INGROUND SWIMMING POOLS - PART 2: REINFORCED MEMBRANES OF NOMINAL THICKNESS EQUAL TO OR GREATER THAN 1,5 MM
    S.R. CEN/TS 16645:2014 AMBIENT AIR - METHOD FOR THE MEASUREMENT OF BENZ[A]ANTHRACENE, BENZO[B]FLUORANTHENE, BENZO[J]FLUORANTHENE, BENZO[K]FLUORANTHENE, DIBENZ[A,H]ANTHRACENE, INDENO[1,2,3-CD]PYRENE AND BENZO[GHI]PERYLENE
    I.S. EN 15841:2009 AMBIENT AIR QUALITY - STANDARD METHOD FOR DETERMINATION OF ARSENIC, CADMIUM, LEAD AND NICKEL IN ATMOSPHERIC DEPOSITION
    I.S. EN 15836-2:2010 PLASTICS - PLASTICIZED POLY(VINYL CHLORIDE) (PVC-P) MEMBRANES FOR INGROUND SWIMMING POOLS - PART 2: REINFORCED MEMBRANES OF NOMINAL THICKNESS EQUAL TO OR GREATER THAN 1,5 MM
    UNI EN 15841 : 2010 AMBIENT AIR QUALITY - STANDARD METHOD FOR DETERMINATION OF ARSENIC, CADMIUM, LEAD AND NICKEL IN ATMOSPHERIC DEPOSITION
    BS EN 12341:2014 Ambient air. Standard gravimetric measurement method for the determination of the PM10 or PM2$d,5 mass concentration of suspended particulate matter
    UNE-EN 1540:2012 Workplace exposure - Terminology
    DIN EN 15549:2008-06 Air quality - Standard method for the measurement of the concentration of benzo[a]pyrene in ambient air
    EN 1540:2011 Workplace exposure - Terminology
    EN 12341:2014 Ambient air - Standard gravimetric measurement method for the determination of the PM10 or PM2,5 mass concentration of suspended particulate matter
    DIN EN 15836-1:2010-11 Plastics - Plasticized poly(vinyl chloride) (PVC-P) membranes for inground swimming pools - Part 1: Homogenous membranes of nominal thickness equal to or greater than 0,75 mm
    UNE-EN 15836-1:2010 Plastics - Plasticized poly(vinyl chloride) (PVC-P) membranes for inground swimming pools - Part 1: Homogenous membranes of nominal thickness equal to or greater than 0,75 mm
    10/30213522 DC : DRAFT JUNE 2010 BS ISO 15202-2 - WORKPLACE AIR - DETERMINATION OF METALS AND METALLOIDS IN AIRBORNE PARTICULATE MATTER BY INDUCTIVELY COUPLED PLASMA ATOMIC EMISSION SPECTROMETRY - PART 2: SAMPLE PREPARATION
    12/30258004 DC : 0 BS ISO 17091 - WORKPLACE AIR - DETERMINATION OF LITHIUM HYDROXIDE, SODIUM HYDROXIDE, POTASSIUM HYDROXIDE AND CALCIUM DIHYDROXIDE - METHOD BY MEASUREMENT OF CORRESPONDING CATIONS BY SUPPRESSED ION CHROMATOGRAPHY
    BS ISO 18158:2016 Workplace air. Terminology
    DIN EN 15841:2010-04 Ambient air quality - Standard method for determination of arsenic, cadmium, lead and nickel in atmospheric deposition
    08/30181781 DC : DRAFT JULY 2008 BS EN 15836-2 - PLASTICS - PLASTICIZED POLY(VINYL CHLORIDE) (PVC-P) MEMBRANES FOR INGROUND SWIMMING POOLS - PART 2: REINFORCED MEMBRANES OF NOMINAL THICKNESS EQUAL TO OR GREATER THAN 1,5 MM
    08/30181778 DC : DRAFT JULY 2008 BS EN 15836-1 - PLASTICS - PLASTICIZED POLY(VINYL CHLORIDE) (PVC-P) MEMBRANES FOR INGROUND SWIMMING POOLS - PART 1: HOMOGENOUS MEMBRANES OF NOMINAL THICKNESS EQUAL TO OR GREATER THAN 0,75 MM
    UNE-EN 15841:2010 Ambient air quality - Standard method for determination of arsenic, cadmium, lead and nickel in atmospheric deposition
    ISO 18158:2016 Workplace air Terminology
    ISO 15202-2:2012 Workplace air Determination of metals and metalloids in airborne particulate matter by inductively coupled plasma atomic emission spectrometry Part 2: Sample preparation
    UNE-EN 12341:2015 Ambient air - Standard gravimetric measurement method for the determination of the PM10 or PM2,5 mass concentration of suspended particulate matter
    DIN EN 12341:1999-03 AMBIENT AIR - STANDARD GRAVIMETRIC MEASUREMENT METHOD FOR THE DETERMINATION OF THE PM[10] OR PM[2],[5] MASS CONCENTRATION OF SUSPENDED PARTICULATE MATTER
    I.S. EN 12341:2014 AMBIENT AIR - STANDARD GRAVIMETRIC MEASUREMENT METHOD FOR THE DETERMINATION OF THE PM[10] OR PM[2,5] MASS CONCENTRATION OF SUSPENDED PARTICULATE MATTER
    I.S. EN 1540:2011 WORKPLACE EXPOSURE - TERMINOLOGY
    VDI 2267 Blatt 1:2012-10 Determination of suspended matter in ambient air - Measurement of the element concentration after sampling on filters - Determination of Al, As, Ba, Ca, Cd, Co, Cr, Cu, Fe, K, Mg, Mn, Na, Ni, Pb, Sb, Se, Sn, Tl, V and Zn by graphite furnace atomic absorption spectrometry (GF-AAS), by optical emission spectrometry with inductively coupled plasma (ICP-OES) and inductively coupled plasma mass spectrometry (ICP-MS)
    VDI 2267 Blatt 12:2008-10 Determination of suspended matter in ambient air - Measurement of As, Ca, Cd, Co, Cr, Cu, Fe, Mn, Ni, Pb, Sb and Zn by energy dispersive X-ray fluorescense (ED XRF)
    VDI 2463 Blatt 7:2014-05 Particulate matter measurement - Determination of suspended particulate matter and gaseous chemical compounds in ambient air and indoor air - Active sampling via low-volume sampler (LVS)
    FD ISO/TR 14294 : 2011 FD WORKPLACE ATMOSPHERES - MEASUREMENT OF DERMAL EXPOSURE - PRINCIPLES AND METHODS
    UNE-EN 15836-2:2010 Plastics - Plasticized poly(vinyl chloride) (PVC-P) membranes for inground swimming pools - Part 2: Reinforced membranes of nominal thickness equal to or greater than 1,5 mm
    08/30163839 DC : DRAFT MAY 2008 BS EN 13890 - WORKPLACE EXPOSURE - PROCEDURES FOR MEASURING METALS AND METALLOIDS IN AIRBORNE PARTICLES - REQUIREMENTS AND TEST METHODS
    NF EN 15841 : 2010 AMBIENT AIR QUALITY - STANDARD METHOD FOR DETERMINATION OF ARSENIC, CADMIUM, LEAD AND NICKEL IN ATMOSPHERIC DEPOSITION
    ISO 21438-3:2010 Workplace atmospheres — Determination of inorganic acids by ion chromatography — Part 3: Hydrofluoric acid and particulate fluorides
    I.S. EN 15836-1:2010 PLASTICS - PLASTICIZED POLY(VINYL CHLORIDE) (PVC-P) MEMBRANES FOR INGROUND SWIMMING POOLS - PART 1: HOMOGENOUS MEMBRANES OF NOMINAL THICKNESS EQUAL TO OR GREATER THAN 0,75 MM
    ISO 17091:2013 Workplace air — Determination of lithium hydroxide, sodium hydroxide, potassium hydroxide and calcium dihydroxide — Method by measurement of corresponding cations by suppressed ion chromatography
    I.S. EN 15549:2008 AIR QUALITY - STANDARD METHOD FOR THE MEASUREMENT OF THE CONCENTRATION OF BENZO[A]PYRENE IN AMBIENT AIR
    DIN EN 12341:2014-08 Ambient air - Standard gravimetric measurement method for the determination of the PM or PM mass concentration of suspended particulate matter
    UNI EN 12341 : 2014 AMBIENT AIR - STANDARD GRAVIMETRIC MEASUREMENT METHOD FOR THE DETERMINATION OF THE PM10 OR PM2,5 MASS CONCENTRATION OF SUSPENDED PARTICULATE MATTER
    DIN EN 15836-2:2010-11 Plastics - Plasticized poly(vinyl chloride) (PVC-P) membranes for inground swimming pools - Part 2: Reinforced membranes of nominal thickness equal to or greater than 1,5 mm
    UNI EN 15836-1 : 2010 PLASTICS - PLASTICIZED POLY(VINYL CHLORIDE) (PVC-P) MEMBRANES FOR INGROUND SWIMMING POOLS - PART 1: HOMOGENOUS MEMBRANES OF NOMINAL THICKNESS EQUAL TO OR GREATER THAN 0,75 MM
    BS EN 15841:2009 Ambient air quality. Standard method for determination of arsenic, cadmium, lead and nickel in atmospheric deposition
    BS EN 15836-1:2010 Plastics. Plasticized poly(vinyl chloride) (PVC-P) membranes for inground swimming pools Homogenous membranes of nominal thickness equal to or greater than 0,75 mm
    DIN EN 15841 E : 2010 AMBIENT AIR QUALITY - STANDARD METHOD FOR DETERMINATION OF ARSENIC, CADMIUM, LEAD AND NICKEL IN ATMOSPHERIC DEPOSITION
    15/30269207 DC : 0 BS ISO 18158 - WORKPLACE AIR - TERMINOLOGY
    UNI EN 15549 : 2008 AIR QUALITY - STANDARD METHOD FOR THE MEASUREMENT OF THE CONCENTRATION OF BENZO[A]PYRENE IN AMBIENT AIR
    ISO/TR 14294:2011 Workplace atmospheres Measurement of dermal exposure Principles and methods
    UNI EN 1540 : 2012 WORKPLACE EXPOSURE - TERMINOLOGY
    EN 15841:2009 Ambient air quality - Standard method for determination of arsenic, cadmium, lead and nickel in atmospheric deposition
    EN 15836-2:2010 Plastics - Plasticized poly(vinyl chloride) (PVC-P) membranes for inground swimming pools - Part 2: Reinforced membranes of nominal thickness equal to or greater than 1,5 mm
    EN 15549:2008 Air quality - Standard method for the measurement of the concentration of benzo[a]pyrene in ambient air
    EN 15836-1:2010 Plastics - Plasticized poly(vinyl chloride) (PVC-P) membranes for inground swimming pools - Part 1: Homogenous membranes of nominal thickness equal to or greater than 0,75 mm
    06/30142044 DC : 0 EN 15549 - AIR QUALITY - STANDARD METHOD FOR THE MEASUREMENT OF THE CONCENTRATION OF BENZO(A)PYRENE IN AMBIENT AIR
    PD ISO/TR 14294:2011 Workplace atmospheres. Measurement of dermal Exposure. Principles and methods
    BS ISO 15202-2:2012 Workplace air. Determination of metals and metalloids in airborne particulate matter by inductively coupled plasma atomic emission spectrometry Sample preparation
    DIN EN 15549 E : 2008 AIR QUALITY - STANDARD METHOD FOR THE MEASUREMENT OF THE CONCENTRATION OF BENZO[A]PYRENE IN AMBIENT AIR
    BS ISO 17091:2013 Workplace air. Determination of lithium hydroxide, sodium hydroxide, potassium hydroxide and calcium dihydroxide. Method by measurement of corresponding cations by suppressed ion chromatography
    BS EN 15549:2008 Air quality. Standard method for the measurement of the concentration of benzo(a)pyrene in ambient air
    BS ISO 30011:2010 Workplace air. Determination of metals and metalloids in airborne particulate matter by inductively coupled plasma mass spectrometry
    BS EN 15836-2:2010 Plastics. Plasticized poly(vinyl chloride) (PVC-P) membranes for inground swimming pools Reinforced membranes of nominal thickness equal to or greater than 1,5 mm
    PD CEN/TS 16645:2014 Ambient air. Method for the measurement of benz[a]anthracene, benzo[b]fluoranthene, benzo[j]fluoranthene, benzo[k]fluoranthene, dibenz[a,h]anthracene, indeno[1,2,3-cd]pyrene and benzo[ghi]perylene
    UNI CEN/TS 16645 : 2014 AMBIENT AIR - METHOD FOR THE MEASUREMENT OF BENZ[A]ANTHRACENE, BENZO[B]FLUORANTHENE, BENZO[J]FLUORANTHENE, BENZO[K]FLUORANTHENE, DIBENZ[A,H]ANTHRACENE, INDENO[1,2,3-CD]PYRENE AND BENZO[GHI]PERYLENE
    ISO 30011:2010 Workplace air Determination of metals and metalloids in airborne particulate matter by inductively coupled plasma mass spectrometry
    BS EN 1540:2011 Workplace exposure. Terminology
    CEN/TS 16645:2014 Ambient air - Method for the measurement of benz[a]anthracene, benzo[b]fluoranthene, benzo[j]fluoranthene, benzo[k]fluoranthene, dibenz[a,h]anthracene, indeno[1,2,3-cd]pyrene and benzo[ghi]perylene

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO/IEC 17025:2005 General requirements for the competence of testing and calibration laboratories
    EN 13274-7:2008 Respiratory protective devices - Methods of test - Part 7: Determination of particle filter penetration
    NFT 90 210 : 2009 WATER QUALITY - PROTOCOL FOR THE INITIAL METHOD PERFORMANCE ASSESSMENT IN A LABORATORY
    VDI 2449 Blatt 1:1995-02 Measurement methods test criteria - Determination of performance characteristics for the measurement of gaseous pollutants (immission)
    EN 1822-5:2009 High efficiency air filters (EPA, HEPA and ULPA) - Part 5: Determining the efficiency of filter elements
    ISO 5725-4:1994 Accuracy (trueness and precision) of measurement methods and results Part 4: Basic methods for the determination of the trueness of a standard measurement method
    DIN 32645:2008-11 CHEMICAL ANALYSIS - DECISION LIMIT, DETECTION LIMIT AND DETERMINATION LIMIT UNDER REPEATABILITY CONDITIONS - TERMS, METHODS, EVALUATION
    ENV 13005 : DRAFT 1999 GUIDE TO THE EXPRESSION OF UNCERTAINTY IN MEASUREMENT
    ISO 6955:1982 Analytical spectroscopic methods Flame emission, atomic absorption, and atomic fluorescence Vocabulary
    CR 14377:2002 Air quality - Approach to uncertainty estimation for ambient air reference measurement methods
    EN 12341:2014 Ambient air - Standard gravimetric measurement method for the determination of the PM10 or PM2,5 mass concentration of suspended particulate matter
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