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  • EN 16174:2012

    Withdrawn A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.

    Sludge, treated biowaste and soil - Digestion of aqua regia soluble fractions of elements

    Available format(s): 

    Withdrawn date:  28-02-2013

    Language(s): 

    Published date:  22-08-2012

    Publisher:  Comite Europeen de Normalisation

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    Introduction
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Principle
    5 Interferences and sources of errors
    6 Reagents
    7 Apparatus
    8 Procedure
    9 Test report
    Annex A (informative) - Repeatability and
            reproducibility data
    Bibliography

    Abstract - (Show below) - (Hide below)

    This European Standard specifies two methods for digestion of sludge, treated biowaste and soil by the use of aqua regia as digestion solution.This European Standard is applicable for the following elements: Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium (Cd), calcium (Ca), cerium (Ce), cesium (Cs), chromium (Cr), cobalt (Co), copper (Cu), dysprosium (Dy), erbium (Er), europium (Eu), gadolinium (Gd), gallium (Ga), germanium (Ge), gold (Au), hafnium (Hf), holmium (Ho), indium (In), iridium (Ir), iron (Fe), lanthanum (La), lead (Pb), lithium (Li), lutetium (Lu), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), neodymium (Nd), nickel (Ni), palladium (Pd), phosphorus (P), platinum (Pt), potassium (K), praseodymium (Pr), rubidium (Rb), rhenium (Re), rhodium (Rh), ruthenium (Ru), samarium (Sm), scandium (Sc), selenium (Se), silicon (Si), silver (Ag), sodium (Na), strontium (Sr), sulphur (S), tellurium (Te), terbium (Tb), thallium (Tl), thorium (Th), thulium (Tm), tin (Sn), titanium (Ti), tungsten (W), uranium (U), vanadium (V), ytterbium (Yb), yttrium (Y), zinc (Zn), and zirconium (Zr).This European Standard may also be applicable for the digestion of other elements.Digestion with aqua regia will not necessarily accomplish total decomposition of the sample. The extracted analyte concentrations may not necessarily reflect the total content in the sample.

    General Product Information - (Show below) - (Hide below)

    Committee CEN/TC 444
    Development Note Supersedes PREN 16174. (09/2012)
    Document Type Standard
    Publisher Comite Europeen de Normalisation
    Status Withdrawn

    Standards Referenced By This Book - (Show below) - (Hide below)

    S.R. CEN/TS 16171:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY (ICP-MS)
    S.R. CEN/TS 16170:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRY (ICP-OES)
    PD ISO/TS 16965:2013 Soil quality. Determination of trace elements using inductively coupled plasma mass spectrometry (ICP-MS)
    CEN/CENELEC GUIDE 33 : 2016 GUIDE FOR ADDRESSING ENVIRONMENTAL ISSUES IN TESTING STANDARDS
    ISO/TS 16965:2013 Soil quality Determination of trace elements using inductively coupled plasma mass spectrometry (ICP-MS)
    CEN/TS 16171:2012 Sludge, treated biowaste and soil - Determination of elements using inductively coupled plasma mass spectrometry (ICP-MS)
    CEN/TS 16172:2013 Sludge, treated biowaste and soil - Determination of elements using graphite furnace atomic absorption spectrometry (GF-AAS)
    EN 16175-2:2016 Sludge, treated biowaste and soil - Determination of mercury - Part 2: Cold-vapour atomic fluorescence spectrometry (CV-AFS)
    CEN/TS 16175-1:2013 Sludge, treated biowaste and soil - Determination of mercury - Part 1: Cold-vapour atomic absorption spectrometry (CV-AAS)
    UNI CEN/TS 16170 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRY (ICP-OES)
    BS EN 16175-2:2016 Sludge, treated biowaste and soil. Determination of mercury Cold-vapour atomic fluorescence spectrometry (CV-AFS)
    UNI CEN/TS 16172 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY (GF-AAS)
    16/30330779 DC : 0 BS EN 16964 - FERTILIZERS - EXTRACTION OF TOTAL MICRO-NUTRIENTS IN FERTILIZERS AND REMOVAL OF ORGANIC COMPOUNDS FROM FERTILIZER EXTRACTS
    UNI CEN/TS 16188 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS IN AQUA REGIA AND NITRIC ACID DIGESTS - FLAME ATOMIC ABSORPTION SPECTROMETRY METHOD (FAAS)
    I.S. EN 16175-1:2016 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 1: COLD-VAPOUR ATOMIC ABSORPTION SPECTROMETRY (CV-AAS)
    UNI CEN/TS 16171 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY (ICP-MS)
    S.R. CEN/TS 16172:2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY (GF-AAS)
    S.R. CEN/TS 16175-2:2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 2: COLD-VAPOUR ATOMIC FLUORESCENCE SPECTROMETRY (CV-AFS)
    I.S. EN 16171:2016 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY (ICP-MS)
    I.S. EN 16170:2016 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRY (ICP-OES)
    I.S. EN 16175-2:2016 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 2: COLD-VAPOUR ATOMIC FLUORESCENCE SPECTROMETRY (CV-AFS)
    S.R. CEN/TS 16175-1:2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 1: COLD-VAPOUR ATOMIC ABSORPTION SPECTROMETRY (CV-AAS)
    CEN/TS 16175-2:2013 Sludge, treated biowaste and soil - Determination of mercury - Part 2: Cold-vapour atomic fluorescence spectrometry (CV-AFS)
    CEN/TS 16170:2012 Sludge, treated biowaste and soil - Determination of elements using inductively coupled plasma optical emission spectrometry (ICP-OES)

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 11466:1995 Soil quality — Extraction of trace elements soluble in aqua regia
    ISO 11074:2015 Soil quality — Vocabulary
    EN 1483:2007 Water quality - Determination of mercury - Method using atomic absorption spectrometry
    EN ISO 11885:2009 Water quality - Determination of selected elements by inductively coupled plasma optical emission spectrometry (ICP-OES) (ISO 11885:2007)
    ISO 11969:1996 Water quality Determination of arsenic Atomic absorption spectrometric method (hydride technique)
    EN ISO 5961 : 1995 WATER QUALITY - DETERMINATION OF CADMIUM BY ATOMIC ABSORPTION SPECTROMETRY (ISO 5961:1994)
    ISO 5961:1994 Water quality Determination of cadmium by atomic absorption spectrometry
    EN 15936:2012 Sludge, treated biowaste, soil and waste - Determination of total organic carbon (TOC) by dry combustion
    ISO 11464:2006 Soil quality Pretreatment of samples for physico-chemical analysis
    ISO 8288:1986 Water quality — Determination of cobalt, nickel, copper, zinc, cadmium and lead — Flame atomic absorption spectrometric methods
    ISO 11885:2007 Water quality Determination of selected elements by inductively coupled plasma optical emission spectrometry (ICP-OES)
    EN 1233 : 1996 WATER QUALITY - DETERMINATION OF CHROMIUM - ATOMIC ABSORPTION SPECTROMETRIC METHODS
    EN 13346 : 2000 CHARACTERIZATION OF SLUDGES - DETERMINATION OF TRACE ELEMENTS AND PHOSPHORUS - AQUA REGIA EXTRACTION METHODS
    ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
    EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
    EN 13650:2001 Soil improvers and growing media - Extraction of aqua regia soluble elements
    EN 13657:2002 Characterization of waste - Digestion for subsequent determination of aqua regia soluble portion of elements
    EN 16179:2012 Sludge, treated biowaste and soil - Guidance for sample pretreatment
    EN ISO 11969:1996 WATER QUALITY - DETERMINATION OF ARSENIC - ATOMIC ABSORPTION SPECTROMETRIC METHOD (HYDRIDE TECHNIQUE)
    EN 45001 : 1989 GENERAL CRITERIA FOR THE OPERATION OF TESTING LABORATORIES
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