• PD ISO/TS 16965:2013

    Current The latest, up-to-date edition.

    Soil quality. Determination of trace elements using inductively coupled plasma mass spectrometry (ICP-MS)

    Available format(s):  Hardcopy, PDF

    Language(s):  English

    Published date:  31-10-2013

    Publisher:  British Standards Institution

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    Introduction
    1 Scope
    2 Normative references
    3 Principle
    4 Interferences
    5 Reagents
    6 Apparatus
    7 Procedure
    8 Calculation
    9 Expression of results
    10 Performance characteristics
    11 Test report
    Annex A (informative) - Selected isotopes and spectral
            interferences for quadrupole ICP-MS instruments
    Bibliography

    Abstract - (Show below) - (Hide below)

    Defines a method for the determination of the following elements in aqua regia or nitric acid digests or other extraction solutions of sludge, treated biowaste and soil: Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium (Cd), calcium (Ca), cerium (Ce), cesium (Cs), chromium (Cr), cobalt (Co), copper (Cu), dysprosium (Dy), erbium (Er), europium (Eu), gadolinium (Gd), gallium (Ga), germanium (Ge), gold (Au), hafnium (Hf), holmium (Ho), indium (In), iridium (Ir), iron (Fe), lanthanum (La), lead (Pb), lithium (Li), lutetium (Lu), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), neodymium (Nd), nickel (Ni), palladium (Pd), phosphorus (P), platinum (Pt), potassium (K), praseodymium (Pr), rhenium (Re), rhodium (Rh), rubidium (Rb), ruthenium (Ru), samarium (Sm), scandium (Sc), selenium (Se), silicon (Si), silver (Ag), sodium (Na), strontium (Sr), sulfur (S), tellurium (Te), terbium (Tb), thallium (Tl), thorium (Th), thulium (Tm), tin (Sn), titanium (Ti), tungsten (W), uranium (U), vanadium (V), ytterbium(Yb), yttrium (Y), zinc (Zn) and zirconium (Zr).

    Scope - (Show below) - (Hide below)

    This Technical Specification specifies a method for the determination of the following elements in aqua regia or nitric acid digests or other extraction solutions of sludge, treated biowaste and soil:

    Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium(Cd), calcium (Ca), cerium (Ce), cesium (Cs), chromium (Cr), cobalt (Co), copper (Cu), dysprosium(Dy), erbium (Er), europium (Eu), gadolinium (Gd), gallium (Ga), germanium (Ge), gold (Au), hafnium (Hf), holmium (Ho), indium (In), iridium (Ir), iron (Fe), lanthanum (La), lead (Pb), lithium (Li), lutetium(Lu), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), neodymium (Nd), nickel(Ni), palladium (Pd), phosphorus (P), platinum (Pt), potassium (K), praseodymium (Pr), rhenium (Re), rhodium (Rh), rubidium (Rb), ruthenium (Ru), samarium (Sm), scandium (Sc), selenium (Se), silicon (Si), silver(Ag), sodium (Na), strontium (Sr), sulfur (S), tellurium (Te), terbium (Tb), thallium (Tl), thorium (Th), thulium (Tm), tin (Sn), titanium (Ti), tungsten (W), uranium (U), vanadium (V), ytterbium(Yb), yttrium (Y), zinc(Zn) and zirconium (Zr).

    The working range depends on the matrix and the interferences encountered.

    The limit of detection is between 0,1mg/kg dry matter and 2,0mg/kg dry matter for most elements.

    The limit of detection will be higher in cases where the determination is likely to have interferences (see Clause4) or in the case of memory effects (see e.g. 8.2 of ISO17294-1:2004).

    General Product Information - (Show below) - (Hide below)

    Committee EH/4
    Document Type Standard
    Publisher British Standards Institution
    Status Current

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 11466:1995 Soil quality — Extraction of trace elements soluble in aqua regia
    EN 16174:2012 Sludge, treated biowaste and soil - Digestion of aqua regia soluble fractions of elements
    ISO 17294-1:2004 Water quality — Application of inductively coupled plasma mass spectrometry (ICP-MS) — Part 1: General guidelines
    EN 16173:2012 Sludge, treated biowaste and soil - Digestion of nitric acid soluble fractions of elements
    ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
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