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AS
AS 1038.10.3-1998

AS 1038.10.3-1998

Current

Current

The latest, up-to-date edition.

Coal and coke - Analysis and testing Determination of trace elements - Coal and coke - Determination of boron content - ICP-AES method (Reconfirmed 2013) (Reconfirmed 2023)

Available format(s)

Hardcopy , PDF 1 User , PDF 3 Users , PDF 5 Users , PDF 9 Users

Language(s)

English

Published date

05-06-1998

Publisher

Standards Australia

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Hardcopy - English
PDF 1 User - English
PDF 3 Users - English
PDF 5 Users - English
PDF 9 Users - English
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This Standard has been reconfirmed. To view or download the Reconfirmation Notice please click here.

1 - AS 1038.10.3-1998 COAL AND COKE-ANALYSIS AND TESTING - DETERMINATION OF TRACE ELEMENTS-COAL AND COKE-DETERMINATION OF BORON....
4 - PREFACE
5 - CONTENTS
6 - 1 SCOPE
6 - 2 REFERENCED DOCUMENTS
6 - 3 DEFINITIONS
6 - 4 PRINCIPLE
6 - 5 SAFETY
6 - 6 REAGENTS
6 - 6.1 General
6 - 6.2 Eschka mixture
7 - 6.3 Hydrochloric acid
7 - 6.4 Standard solutions
7 - 6.4.1 Boron stock solution (100 mg/L)
7 - 6.4.2 Dilute boron stock solution (5 mg/L)
7 - 7 APPARATUS
7 - 7.1 General
7 - 7.2 Muffle furnace
7 - 7.3 Crucible
7 - 7.4 Silica plate
7 - 7.6 Inductively coupled plasma atomic emission spectrometer
7 - 7.6.1 General
7 - 7.6.2 Short-term stability
7 - 7.6.3 Background equivalent concentration and detection limit
7 - 7.5 Receptacles
7 - 7.7 Weighing device
8 - 8 SAMPLE
8 - 8.1 General
8 - 8.2 Equilibration of the sample
8 - 9 PROCEDURE
8 - 9.1 Blank determination
8 - 9.2 Preparation of test solution
8 - 9.3 Preparation of calibration solutions
9 - 9.4 Calibration of the inductively coupled plasma atomic emission spectrometer
9 - 9.5 Determination of boron
9 - 10 CALCULATION
9 - 11 REPORTING OF RESULTS
9 - 12 PRECISION
9 - 13 TEST REPORT

Sets out a method for the determination of boron in higher rank coal and coke using an inductively-coupled plasma atomic emission spectrometer after ashing of the coal or coke in the presence of Eschka mixture.

Committee
MN/1
DocumentType
Standard
ISBN
0 7337 1925 2
Pages
4
ProductNote
Reconfirmed 06-08-2013
PublisherName
Standards Australia
Status
Current
Supersedes

This Standard sets out a method for the determination of boron in higher rank coal and coke using an inductively-coupled plasma atomic emission spectrometer after ashing of the coal or coke in the presence of Eschka mixture.

Originated as AS 1038.10.3-1988.
Second edition 1998.

AS 1038.3-2000 Coal and coke - Analysis and testing - Proximate analysis of higher rank coal
BS ISO 23380:2013 Selection of methods for the determination of trace elements in coal
AS 3641.2-1999 Recommended practice for atomic emission spectrometric analysis Inductively coupled plasma excitation
06/30145838 DC : DRAFT APR 2006 ISO 23380 - GUIDANCE ON THE DETERMINATION OF TRACE ELEMENTS IN COAL
AS 2418-1995 Coal and coke - Glossary of terms (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.16-2005 Coal and coke - Analysis and testing Assessment and reporting of results (Reconfirmed 2016)
AS 1038.16-1996 Coal and coke - Analysis and testing - Assessment and reporting of results
AS 4264.2-1996 Coal and coke - Sampling Coke - Sampling procedures (Reconfirmed 2013)
AS 1038.3-1989 Coal and coke - Analysis and testing - Proximate analysis of higher rank coal
AS 2706-2003 Numerical values - Rounding and interpretation of limiting values (Reconfirmed 2018)
ISO 23380:2013 Selection of methods for the determination of trace elements in coal
AS 4264.1-1995 Coal and coke - Sampling Higher rank coal - Sampling procedures

AS 1038.16-2005 Coal and coke - Analysis and testing Assessment and reporting of results (Reconfirmed 2016)
AS 2519-1993 Guide to the technical evaluation of higher rank coal deposits (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.10.0-2002 Coal and coke - Analysis and testing Determination of trace elements - Guide to the determination of trace elements (Reconfirmed 2013)
AS 1038.16-1996 Coal and coke - Analysis and testing - Assessment and reporting of results
AS 2418-1995 Coal and coke - Glossary of terms (Reconfirmed 2013) (Reconfirmed 2023)

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