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AS
AS 1038.14.1-2003

AS 1038.14.1-2003

Withdrawn

Withdrawn

A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.

Coal and coke - Analysis and testing Higher rank coal ash and coke ash - Major and minor elements - Borate fusion/flame atomic absorption spectrometric method (Reconfirmed 2013)

Available format(s)

Hardcopy , PDF 1 User , PDF 3 Users , PDF 5 Users , PDF 9 Users

Withdrawn date

10-11-2023

Language(s)

English

Published date

14-11-2003

Publisher

Standards Australia

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Hardcopy - English
PDF 1 User - English
PDF 3 Users - English
PDF 5 Users - English
PDF 9 Users - English
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This Standard has been reconfirmed. To view or download the Reconfirmation Notice please click here.

1 - AS 1038.14.1-2003 COAL AND COKE-ANALYSIS AND TESTING - HIGHER RANK COAL ASH AND COKE ASH-MAJOR AND MINOR ELEMENTS-BORATE...
4 - PREFACE
5 - CONTENTS
6 - 1 SCOPE
6 - 2 REFERENCED DOCUMENTS
7 - 3 DEFINITIONS
7 - 4 PRINCIPLE
7 - 5 SAFETY
7 - 6 REAGENTS
7 - 6.1 General
7 - 6.2 Lithium tetraborate, anhydrous (minimum 98% Li2B4O7)
7 - 6.3 Solutions
7 - 6.3.1 Nitric acid
7 - 6.3.2 Nitric acid (1+1)
8 - 6.3.3 Nitric acid (1+9)
8 - 6.3.4 Nitric acid (1+19)
8 - 6.3.5 Hydrochloric acid
8 - 6.4 Standard solutions
8 - 6.4.1 Standard aluminium solution
8 - 6.4.2 Standard barium solution
8 - 6.4.3 Standard calcium solution
8 - 6.4.4 Standard iron solution
8 - 6.4.5 Standard magnesium solution
8 - 6.4.6 Standard manganese solution
8 - 6.4.7 Standard potassium solution
8 - 6.4.8 Standard silicon solution
9 - 6.4.9 Standard sodium solution
9 - 6.4.10 Standard strontium solution
9 - 6.4.11 Standard titanium solution
9 - 6.4.12 Standard zinc solution
9 - 6.4.13 Lanthanum/zirconium solution
9 - 6.4.14 Lithium tetraborate solution
9 - 6.4.15 Matrix matching solution for sample dilution
9 - 6.5 Calibration solutions
9 - 7 APPARATUS
9 - 7.1 General
9 - 7.2 Atomic absorption spectrometer
10 - 7.3 Platinum or platinum/gold crucibles and lids
10 - 7.4 Plastic bottles
10 - 7.5 Weighing device
10 - 8 SAMPLE PREPARATION
10 - 9 PROCEDURE
10 - 9.1 Number of determinations
10 - 9.2 Blank test
10 - 9.3 Check test
12 - 9.4 Determination
12 - 9.4.1 Decomposition of test portion
13 - 9.4.2 Test solutions
14 - 9.5 Measurement
14 - 9.5.1 General
14 - 9.5.2 Calibration graphs
14 - 9.5.3 Graph linearity
14 - 9.5.4 Background correction
14 - 10 CALCULATION
15 - 11 REPORTING OF RESULTS
15 - 12 PRECISION
15 - 13 TEST REPORT

Sets out a method for the determination of twelve elements in higher rank coal ash and coke ash by flame atomic absorption spectrometry after borate fusion. Methods for the determination of a further two elements are also referenced.

Committee
MN-001
DocumentType
Standard
ISBN
0 7337 5572 0
Pages
12
ProductNote
Reconfirmed 06-08-2013
PublisherName
Standards Australia
Status
Withdrawn
Supersedes

This Standard sets out a method for the determination of silicon, aluminium, iron, calcium, magnesium, sodium, potassium, titanium, manganese, barium, strontium and zinc in higher rank coal ash and coke ash by flame atomic absorption spectrometry after borate fusion. A spectrophotometric method for the determination of phosphorus and a method for the determination of sulfur are also referenced. This method is suitable for the determination of the above elements (expressed as oxides), in the concentration ranges specified in Table 1.

Originated as AS K152.14-1967.
Previous edition AS 1038.14.1-1995.
Third edition 2003.

AS 2508.3.034-1984 Safe storage and handling information card - Pentanes
AS 2508.8.009-1990 Safe storage and handling information card - Sulfuric acid (Oleum)
AS 2508.3.027-1983 Safe storage and handling information card - Diacetone alcohol
AS 2508.6.002-1985 Safe storage and handling information card - Cyanides (sodium and potassium)
AS 2508.2.007-2001 Safe storage and handling information card - Liquefied petroleum gas
AS 2508.3.008-1983 Safe storage and handling information cards for hazardous materials - Acrylonitrile (inhibited)
AS 2508.6.017-1989 Safe storage and handling information card - Lead acetate
AS 2243.3-1991 Safety in laboratories Microbiology
AS 1038.6.3.2-2003 Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Total sulfur - High-temperature combustion method (Reconfirmed 2013)
AS 2508.3.014-1992 Safe storage and handling information card - Xylenes (xylols)
AS 2508.6.020-1991 Safe storage and handling information card - Selenious acid, selenates and selenites
AS 2508.2.013-1992 Safe storage and handling information card - Ethylene (ethene)
AS 2508.3.025-1983 Safe storage and handling information cards for hazardous materials - Chlorobenzene (monochlorobenzene)
AS 1038.4-2006 Coal and coke - Analysis and testing Coke - Proximate analysis
AS 2508.3.016-1982 Safe storage and handling information card - Methyl isobutyl ketone (MIBK)
BS ISO 23380:2013 Selection of methods for the determination of trace elements in coal
AS 2508.6.022-1986 Safe storage and handling information card - Copper-chrome-arsenic
AS 2508.6.001-1988 Safe storage and handling information card - Carbon tetrachloride (tetrachloromethane)
AS 2243.1-1990 Safety in laboratories General
AS 2508.3.032-1984 Safe storage and handling information card - Glycol ether acetates
AS 2508.2.010-1984 Safe storage and handling information card - Sulphur dioxide (liquefied)
AS 2508.6.008-1989 Safe storage and handling information card - Ammonium thioglycolate
AS 2508.3.009-1982 Safe storage and handling information card - Hydrocarbon solvents
AS 2508.6.009-1990 Safe storage and handling information card - 1,1,1-trichloroethane (Methylchloroform)
AS 2243.9-1991 Safety in laboratories - Recirculating fume cabinets
AS 2508.3.029-1983 Safe storage and handling information card - Glycol ethers (flammable)
AS 1038.4-1995 Coal and coke - Analysis and testing Coke - Proximate analysis
AS 2508.3.033-1984 Safe storage and handling information card - Isoprene, inhibited
06/30145838 DC : DRAFT APR 2006 ISO 23380 - GUIDANCE ON THE DETERMINATION OF TRACE ELEMENTS IN COAL
AS 2706-2003 Numerical values - Rounding and interpretation of limiting values (Reconfirmed 2018)
AS 2508.8.012-1991 Safe storage and handling information card - Hydrogen fluoride (Anhydrous)(Anhydrous hydrofluoric acid)
AS 2508.3.030-1983 Safe storage and handling information card - Cyclohexane
AS 2508.6.024-1984 Safe storage and handling information card - Pentachlorophenol
AS 2508.6.003-1984 Safe storage and handling information card - Aniline (aminobenzene)
AS 2243.7-1991 Safety in laboratories - Electrical aspects
AS 2508.6.016-1995 Safe storage and handling information card - Phenol (carbolic acid), cresols and cresylic acid
AS 2508.4.001-1982 Safe storage and handling information card - Calcium carbide
AS 2508.3.003-1982 Safe storage and handling information card - Acrylates (butyl, isobutyl)
AS 2508.3.012-1982 Safe storage and handling information card - Styrene (vinyl benzene, styrene monomer)
AS 2508.3.010-1995 Safe storage and handling information card - Amines (isopropylamine, diethylamine, triethylamine)
AS 2706-1984 Numerical values - Rounding and interpretation of limiting values
AS 2508.3.005-1995 Safe storage and handling information card - Benzene
AS 2508.6.021-1984 Safe storage and handling information card - Sodium pentachlorophenate
AS 2508.6.025-1984 Safe storage and handling information card - Arsenic acid
AS 2508.6.007-1995 Safe storage and handling information card - Epichlorohydrin (Ech or 1-Chloro-2,3-epoxypropane)
AS 2508.2.003-1995 Safe storage and handling information card - Vinyl chloride (inhibited)
AS 2508.3.004-1982 Safe storage and handling information card - Acrylates (methyl, ethyl)
AS 2508.8.011-1995 Safe storage and handling information card - Methacrylic acid (inhibited)
AS 2508.8.003-1990 Safe storage and handling information card - Sodium hypochlorite Hypochlorite solutions
AS 2508.2.005-1984 Safe storage and handling information card - Chlorine (compressed)
AS 1038.9.3-2000 Coal and coke - Analysis and testing Coal and coke - Phosphorus - Ash digestion/phosphomolybdovanadate method (Reconfirmed 2013)
AS 2508.8.008-1992 Safe storage and handling information card - Maleic anhydride
AS 2243.8-1992 Safety in laboratories Fume cupboards
AS 2508.6.013-1991 Safe storage and handling information card - Trichloroethylene
AS 2508.8.002-1986 Safe storage and handling information card - Hydrochloric acid (muriatic acid, spirits of salts)
AS 2508.8.004-1992 Safe storage and handling information card - Acetic acid (containing more than 80 percent acid, by mass, in water)
AS 2508.2.011-1984 Safe storage and handling information card - Butadiene (inhibited)
AS 2508.3.024-1995 Safe storage and handling information card - Dimethylamine solution
AS 2508.8.007-1990 Safe storage and handling information card - Nitric acid
AS 2508.3.002-1982 Safe storage and handling information card - Acetates (ethyl acetate, propyl acetates, butyl acetates, amyl acetate)
AS 2243.2-1990 Safety in laboratories - Chemical aspects
AS 2508.5.003-1990 Safe storage and handling information card - Calcium hypochlorite
AS 1038.3-2000 Coal and coke - Analysis and testing - Proximate analysis of higher rank coal
AS 2134.1-1999 Recommended practice for chemical analysis by atomic absorption spectrometry Flame atomic absorption spectrometry (Reconfirmed 2016)
AS 2508.3.031-1983 Safe storage and handling information card - Tetrahydrofuran (THF)
AS 2508.6.004-1984 Safe storage and handling information card - Cadmium compounds (other than selenide and sulphide)
AS 2508.6.006-1982 Safe storage and handling information card - Beryllium and compounds
AS 2508.8.018-1995 Safe storage and handling information card - Formaldehyde solutions (with not less than 25 percent formaldehyde)
AS 2508.8.013-1991 Safe storage and handling information card - Hydrofluoric acid (aqueous)
AS 2508.3.026-1995 Safe storage and handling information card - Propylene oxide
AS 2508.8.015-1988 Safe storage and handling information card - Dilute ammonia solution containing 10 percent up to 35 percent m/m ammonia
AS 2508.6.005-1984 Safe storage and handling information card - Fluorides (ammonium, potassium, magnesium or sodium fluoride)
AS 2508.3.011-1992 Safe storage and handling information card - Methanol (methyl alcohol)
AS 2508.3.006-1995 Safe storage and handling information card - Butanols, propanols, amyl alcohols
AS 2508.3.013-1984 Safe storage and handling information card - Methyl ethyl ketone (MEK)
AS 2508.2.001-1992 Safe storage and handling information card - Acetylene (Dissolved) (Ethyne)
AS 2508.8.005-1992 Safe storage and handling information card - Acetic acid (containing more than 10 percent but not more than 80 percent acid, by mass, in water)
AS 2508.6.026-1984 Safe storage and handling information card - Formaldehyde solutions - Flashpoint above 61 degrees Celsius
AS 2508.6.019-1995 Safe storage and handling information card - Lead alkyls
AS 2508.3.018-1983 Safe storage and handling information card - Methyl isobutyl carbinol
AS 2243.6-1990 Safety in laboratories - Mechanical aspects
AS 2508.2.008-1984 Safe storage and handling information card - Oxygen (compressed)
AS 2508.8.006-1992 Safe storage and handling information card - Sodium hydroxide (solid and solution) (caustic soda)
AS 2508.6.023-1989 Safe storage and handling information card - Phenylmercuric compounds
AS 2508.8.016-1988 Safe storage and handling information card - Phosphoric acid (Orthophosphoric acid)
AS 2508.2.004-1995 Safe storage and handling information card - Ammonia (anhydrous)
AS 2508.2.002-1992 Safe storage and handling information card - Hydrogen (compressed)
AS 2508.6.014-1989 Safe storage and handling information card - Cyanides, inorganic (other than Sodium and Potassium Cyanides for which refer to AS 2508.6.002)
AS 2508.3.001-1982 Safe storage and handling information card - Acetone
AS 2508.8.010-1990 Safe storage and handling information cards for hazardous materials - Sulfuric acid (up to 98% m/m)
AS 2508.3.028-1983 Safe storage and handling information card - Ethylene dichloride (1,2-dichloroethane, ethylene chloride (EDC))
AS 2508.8.001-1995 Safe storage and handling information card - Acetic anhydride
AS 2418-1995 Coal and coke - Glossary of terms (Reconfirmed 2013) (Reconfirmed 2023)
AS 2508.2.006-1995 Safe storage and handling information card - Ethylene oxide
AS 2243.10-1993 Safety in laboratories - Storage of chemicals
AS 2508.6.011-1988 Safe storage and handling information card - Tetrachloroethylene (Perchloroethylene, Per or Perc)
AS 1038.16-2005 Coal and coke - Analysis and testing Assessment and reporting of results (Reconfirmed 2016)
AS 2508.3.023-1983 Safe storage and handling information card - Vinyl acetate (vinyl acetate monomer)
AS 2508.3.022-1983 Safe storage and handling information card - Cumene (isopropyl-benzene)
AS 2508.3.021-1983 Safe storage and handling information card - Cyclohexanone
AS 2508.6.010-1983 Safe storage and handling information card - Toluene diisocyanate (TDI)
AS 2508.5.002-1990 Safe storage and handling information card - Ammonium nitrate
AS 1038.16-1996 Coal and coke - Analysis and testing - Assessment and reporting of results
AS 2508.6.028-1988 Safe storage and handling information card - Chloropicrin
AS 2508.3.020-1983 Safe storage and handling information card - Ethyl benzene
AS 2508.5.004-1991 Safe storage and handling information card - Benzoyl peroxide
AS 2508.8.014-1985 Safe storage and handling information card - Mercury metal
AS 2508.5.005-1992 Safe storage and handling information card - Methyl ethyl ketone peroxide (MEKP) (not more than 50% in solution with not more than 10% available oxygen)
AS 2508.10.001-2000 Safe storage and handling information card - Agricultural and veterinary chemicals (Packaged products only)
AS 2243.4-1998 Safety in laboratories - Ionizing radiations
AS 2508.3.015-1992 Safe storage and handling information card - Toluene (toluol)
AS 2508.6.027-1984 Safe storage and handling information card - Tributyltin-oxide
AS 2508.6.015-1983 Safe storage and handling information card - Methylene chloride (Dichloromethane)
AS 2508.6.018-1989 Safe storage and handling information card - Lead arsenate and Lead aresenite
AS 2508.5.001-1989 Safe storage and handling information card - Hydrogen peroxide
AS 2508.3.017-1983 Safe storage and handling information card - Ethanol/methylated spirits
AS 2508.6.012-1988 Safe storage and handling information card - Diphenyl methane-4, 4-Diisocyanate [Methylene bis-(Phenylene) Diisocyanate] (MDI)
AS 2508.2.012-1985 Safe storage and handling information card - Non-flammable, inert, compressed gases (includes: argon, helium, krypton, neon, nitrogen and xenon)
AS 2508.2.009-1984 Safe storage and handling information card - Oxygen (refrigerated liquid)
AS 2508.8.017-1988 Safe storage and handling information card - Aluminium chloride (Anhydrous)
AS 2508.3.007-1995 Safe storage and handling information card - Carbon disulphide
ISO 23380:2013 Selection of methods for the determination of trace elements in coal
AS 2508.3.019-1983 Safe storage and handling information card - Methacrylates, HFP
AS 2243.5-1993 Safety in laboratories Non-ionizing radiations

AS 1038.16-2005 Coal and coke - Analysis and testing Assessment and reporting of results (Reconfirmed 2016)
AS 2519-1993 Guide to the technical evaluation of higher rank coal deposits (Reconfirmed 2013) (Reconfirmed 2023)
AS 4828.1-2009 Degradability of plastics Methods of test - Determination of level of prodegradant ions
AS 2418-1995 Coal and coke - Glossary of terms (Reconfirmed 2013) (Reconfirmed 2023)

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