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AS
AS 1038.4-1995

AS 1038.4-1995

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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Coal and coke - Analysis and testing Coke - Proximate analysis

Available format(s)

Hardcopy , PDF 1 User , PDF 3 Users , PDF 5 Users , PDF 9 Users

Superseded date

30-06-2017

Superseded by

AS 1038.4-2006

Language(s)

English

Published date

01-01-1995

Publisher

Standards Australia

Preview
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Hardcopy - English
PDF 1 User - English
PDF 3 Users - English
PDF 5 Users - English
PDF 9 Users - English
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1 - AS 1038.4-1995 COAL AND COKE - ANALYSIS AND TESTING - COKE - PROXIMATE ANALYSIS
4 - PREFACE
5 - CONTENTS
6 - SECTION 1 SCOPE AND GENERAL
6 - 1.1 SCOPE
6 - 1.2 REFERENCED DOCUMENTS
6 - 1.3 DEFINITIONS
6 - 1.4 SAFETY
6 - 1.5 SAMPLES
6 - 1.5.1 General
6 - 1.5.2 Equilibration
6 - 1.6 REPORTING OF RESULTS
6 - 1.7 PRECISION
7 - 1.8 TEST REPORT
8 - SECTION 2 DETERMINATION OF MOISTURE IN THE ANALYSIS SAMPLE
8 - 2.0 INTRODUCTION
8 - 2.1 SCOPE OF SECTION
8 - 2.2 DIRECT GRAVIMETRIC METHOD
8 - 2.2.1 Principle
8 - 2.2.2 Reagents
8 - 2.2.3 Apparatus
9 - 2.2.4 Procedure
10 - 2.2.5 Calculation
10 - 2.3 INDIRECT GRAVIMETRIC METHOD
10 - 2.3.1 Principle
10 - 2.3.2 Reagents
10 - 2.3.3 Apparatus
10 - 2.3.4 Procedure
12 - 2.3.5 Calculation
14 - SECTION 3 DETERMINATION OF ASH
14 - 3.0 INTRODUCTION
14 - 3.1 SCOPE OF SECTION
14 - 3.2 PRINCIPLE
14 - 3.3 APPARATUS
14 - 3.3.1 Muffle furnace
14 - 3. 3.2 Dish
14 - 3.3.3 Plate
14 - 3.3.4 Weighing device
14 - 3.4 PROCEDURE
15 - 3.5 CALCULATION
16 - SECTION 4 DETERMINATION OF VOLATILE MATTER
16 - 4.0 INTRODUCTION
16 - 4.1 SCOPE OF SECTION
16 - 4.2 PRINCIPLE
16 - 4.3 REAGENTS
16 - 4.3.1 Desiccant
16 - 4.3.2 Toluene
16 - 4.4 APPARATUS
16 - 4.4.1 Muffle furnace
16 - 4.4.2 Thermocouples
17 - 4.4.3 Crucible and lid
17 - 4.4.4 Stand
17 - 4.4.5 Weighing device
17 - 4.5 PROCEDURE
18 - 4.6 CALCULATION

Sets out methods for the determination of moisture, ash and volatile matter on the analysis sample of coke to obtain its proximate analysis. Residue is calculated by difference.

Committee
MN-001
DocumentType
Standard
ISBN
0 7262 9603 1
Pages
15
PublisherName
Standards Australia
Status
Superseded
SupersededBy
Supersedes
UnderRevision

This Standard sets out methods for the determination of moisture, ash and volatile matter on the analysis sample of coke to obtain its proximate analysis. Residue is calculated by difference.

First published as part of AS CK2.3-1949.
Revised and redesignated in part as AS K152.4-1965 (being endorsement of BS 1016.4:1957 without amendment).
Second edition 1968.
AS K152.4 withdrawn 1978.
Revised and redesignated AS 1038.4-1979.
Second edition 1995.

AS 2706-1984 Numerical values - Rounding and interpretation of limiting values
AS 2418-1995 Coal and coke - Glossary of terms (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.16-1996 Coal and coke - Analysis and testing - Assessment and reporting of results
AS 2646.7-1985 Sampling of solid mineral fuels Coke - Preparation of samples

AS 1038.8.2-2003 Coal and coke - Analysis and testing Coal and coke - Chlorine - High-temperature combustion method (Reconfirmed 2013)
AS 1038.6.1-1997 Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Carbon and hydrogen (Reconfirmed 2013)
AS 1038.14.2-2003 Coal and coke - Analysis and testing Higher rank coal ash and coke ash - Major and minor elements - Acid digestion/flame atomic absorption spectrometric method (Reconfirmed 2013)
AS 1038.16-2005 Coal and coke - Analysis and testing Assessment and reporting of results (Reconfirmed 2016)
AS 1038.21.1.2-2002 Coal and coke - Analysis and testing Higher rank coal and coke - Relative density - Analysis sample/volumetric method (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.14.1-1995 Coal and coke - Analysis and testing Higher rank coal ash and coke ash - Major and minor elements - Borate fusion/flame atomic absorption spectrometric method
AS 1038.9.1-1992 Coal and coke - Analysis and testing Coal and coke - Phosphorus - Ash digestion/molybdenum blue method
AS 1038.6.3.2-1997 Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Total sulfur - High-temperature combustion method
AS 1038.12.2-1999 Coal and coke - Analysis and testing Higher rank coal - Caking and coking properties - Determination of Gray-King coke type (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.10.1-2003 Coal and coke - Analysis and testing Determination of trace elements - Coal, coke and fly-ash - Determination of eleven trace elements - Flame atomic absorption spectrometric method (Reconfirmed 2013)
AS 1038.6.3.2-2003 Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Total sulfur - High-temperature combustion method (Reconfirmed 2013)
AS 1038.6.4-2005 Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Carbon, hydrogen and nitrogen - Instrumental method
AS 1038.10.5-1993 Coal and coke - Analysis and testing Coal, coke and fly-ash - Trace elements - Determination of mercury content
AS 1038.21.1.1-2002 Coal and coke - Analysis and testing Higher rank coal and coke - Relative density - Analysis sample/density bottle method
AS 1038.8.2-1996 Coal and coke - Analysis and testing Coal and coke - Chlorine - High-temperature combustion method
AS 1038.16-1996 Coal and coke - Analysis and testing - Assessment and reporting of results
AS 1038.15-1995 Coal and coke - Analysis and testing Higher rank coal ash and coke ash - Ash fusibility
AS 1038.14.1-2003 Coal and coke - Analysis and testing Higher rank coal ash and coke ash - Major and minor elements - Borate fusion/flame atomic absorption spectrometric method (Reconfirmed 2013)
AS 1038.6.2-1997 Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Nitrogen
AS 1038.5-1998 Coal and coke - Analysis and testing - Gross calorific value
AS 1038.14.2-1995 Coal and coke - Analysis and testing Higher rank coal ash and coke ash - Major and minor elements - Acid digestion/flame atomic absorption spectrometric method
AS 1038.10.5.1-2003 Coal and coke - Analysis and testing Coal, coke and fly-ash - Trace elements - Determination of mercury content - Tube combustion method (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.21.1.2-1994 Coal and coke - Analysis and testing Higher rank coal and coke - Relative density - Analysis sample/volumetric method
AS 1038.10.2-1998 Coal and coke - Analysis and testing Determination of trace elements - Coal and coke - Determination of arsenic, antimony and selenium - Hydride generation method (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.21.1.1-1994 Coal and coke - Analysis and testing Higher rank coal and coke - Relative density - Analysis sample/density bottle method
AS 2418-1995 Coal and coke - Glossary of terms (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.6.3.3-1997 Coal and coke - Analysis and testing Higher rank coal - Ultimate analysis - Total sulfur - Infrared method (Reconfirmed 2013)
AS 1038.6.3.1-1997 Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Total sulfur - Eschka method (Reconfirmed 2013)
AS 1038.10.4-2001 Coal and coke - Analysis and testing Determination of trace elements - Coal, coke and fly-ash - Determination of fluorine content - Pyrohydrolysis method (Reconfirmed 2013)

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