Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Total sulfur - High-temperature combustion method (Reconfirmed 2013)

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10-11-2023

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29-09-2003

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Standards Australia

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1 - AS 1038.6.3.2-2003 COAL AND COKE-ANALYSIS AND TESTING - HIGHER RANK COAL AND COKE-ULTIMATE ANALYSIS-TOTAL SULFUR-HIGH...
4 - PREFACE
5 - CONTENTS
6 - FOREWORD
7 - 1 SCOPE
7 - 2 REFERENCED DOCUMENTS
7 - 3 DEFINITIONS
7 - 3.1 Repeatability (r)
7 - 4 PRINCIPLE
8 - 5 SAFETY
8 - 6 REAGENTS
8 - 6.1 General
8 - 6.2 Aluminium oxide
8 - 6.3 Alkaline absorbent
8 - 6.4 Sodium tetraborate solution (0.025 mol/L)
8 - 6.5 Standard sulfuric acid solution (0.0125 mol/L)
8 - 6.6 Hydrogen peroxide solution (9 g/L)
8 - 6.7 Mercury(II) oxycyanide solution
8 - 6.8 Screened indicator solution
9 - 6.9 Oxygen
9 - 7 APPARATUS
9 - 7.1 Purification train
9 - 7.2 Heating unit
9 - 7.3 Combustion tube
9 - 7.4 Combustion boat
9 - 7.5 Silica pusher
9 - 7.6 Nickel-chromium wire
9 - 7.7 Flowmeter
9 - 7.8 Pressure gauge
10 - 7.9 Silica adaptor
10 - 7.10 Absorption vessel
10 - 7.11 Heat-resistant stopper or tubing
10 - 7.12 Pressure regulator
10 - 7.13 Vacuum pump
10 - 7.14 Weighing device
10 - 8 SAMPLE
10 - 9 PROCEDURE
10 - 9.1 Preparation of apparatus
11 - 9.2 Determination of the blank
12 - 9.3 Combustion and absorption
12 - 9.4 Measurement
13 - 10 CALCULATION
13 - 11 REPORTING OF RESULTS
13 - 12 PRECISION
13 - 13 TEST REPORT

Sets out a method for determining the total sulfur content of an analysis sample by high temperature combustion.

Committee	MN-001
DocumentType	Standard
ISBN	0 7337 5483 X
Pages	7
ProductNote	Reconfirmed 06-08-2013
PublisherName	Standards Australia
Status	Withdrawn
Supersedes	DR 03089 CP AS 1038.6.3.2-1997 AS 1038.6.3.2-1997 AMDT 1

This Standard sets out a method for the determination of total sulfur in the analysis sample of higher rank coal and coke by the high-temperature combustion method.

Originated as part of AS CK2.3-1949.
Previous edition AS 1038.6.3.2-1997.
Third edition 2003.

AS 2508.6.020-1991	Safe storage and handling information card - Selenious acid, selenates and selenites
AS 2508.6.019-1995	Safe storage and handling information card - Lead alkyls
AS 1038.8.2-2003	Coal and coke - Analysis and testing Coal and coke - Chlorine - High-temperature combustion method (Reconfirmed 2013)
AS 2508.3.018-1983	Safe storage and handling information card - Methyl isobutyl carbinol
AS 2508.3.019-1983	Safe storage and handling information card - Methacrylates, HFP
AS 2243.6-1990	Safety in laboratories - Mechanical aspects
AS 2508.2.008-1984	Safe storage and handling information card - Oxygen (compressed)
AS 2508.8.006-1992	Safe storage and handling information card - Sodium hydroxide (solid and solution) (caustic soda)
AS 2508.5.004-1991	Safe storage and handling information card - Benzoyl peroxide
AS 2508.8.014-1985	Safe storage and handling information card - Mercury metal
AS 1038.4-2006	Coal and coke - Analysis and testing Coke - Proximate analysis
AS 2508.6.009-1990	Safe storage and handling information card - 1,1,1-trichloroethane (Methylchloroform)
AS 2508.3.033-1984	Safe storage and handling information card - Isoprene, inhibited
AS 2508.6.002-1985	Safe storage and handling information card - Cyanides (sodium and potassium)
AS 2508.3.032-1984	Safe storage and handling information card - Glycol ether acetates
AS 2508.2.007-2001	Safe storage and handling information card - Liquefied petroleum gas
AS 2508.8.013-1991	Safe storage and handling information card - Hydrofluoric acid (aqueous)
AS 2508.3.017-1983	Safe storage and handling information card - Ethanol/methylated spirits
AS 2508.5.001-1989	Safe storage and handling information card - Hydrogen peroxide
AS 2508.3.026-1995	Safe storage and handling information card - Propylene oxide
AS 2508.8.007-1990	Safe storage and handling information card - Nitric acid
AS 2508.5.003-1990	Safe storage and handling information card - Calcium hypochlorite
AS 2508.6.015-1983	Safe storage and handling information card - Methylene chloride (Dichloromethane)
AS 1038.3-2000	Coal and coke - Analysis and testing - Proximate analysis of higher rank coal
AS 2508.2.012-1985	Safe storage and handling information card - Non-flammable, inert, compressed gases (includes: argon, helium, krypton, neon, nitrogen and xenon)
AS 2508.3.020-1983	Safe storage and handling information card - Ethyl benzene
AS 2508.3.031-1983	Safe storage and handling information card - Tetrahydrofuran (THF)
AS 2508.3.002-1982	Safe storage and handling information card - Acetates (ethyl acetate, propyl acetates, butyl acetates, amyl acetate)
AS 2243.2-1990	Safety in laboratories - Chemical aspects
AS 2508.3.004-1982	Safe storage and handling information card - Acrylates (methyl, ethyl)
AS 2508.8.003-1990	Safe storage and handling information card - Sodium hypochlorite Hypochlorite solutions
AS 2508.2.005-1984	Safe storage and handling information card - Chlorine (compressed)
AS 2508.8.008-1992	Safe storage and handling information card - Maleic anhydride
AS 2243.8-1992	Safety in laboratories Fume cupboards
AS 2508.6.013-1991	Safe storage and handling information card - Trichloroethylene
AS 2508.2.001-1992	Safe storage and handling information card - Acetylene (Dissolved) (Ethyne)
AS 2508.6.007-1995	Safe storage and handling information card - Epichlorohydrin (Ech or 1-Chloro-2,3-epoxypropane)
AS 2508.2.003-1995	Safe storage and handling information card - Vinyl chloride (inhibited)
AS 2508.8.011-1995	Safe storage and handling information card - Methacrylic acid (inhibited)
AS 2508.3.023-1983	Safe storage and handling information card - Vinyl acetate (vinyl acetate monomer)
AS 2243.3-1991	Safety in laboratories Microbiology
AS 2508.3.022-1983	Safe storage and handling information card - Cumene (isopropyl-benzene)
AS 2508.3.021-1983	Safe storage and handling information card - Cyclohexanone
AS 2508.6.010-1983	Safe storage and handling information card - Toluene diisocyanate (TDI)
AS 2508.5.002-1990	Safe storage and handling information card - Ammonium nitrate
AS 1038.16-1996	Coal and coke - Analysis and testing - Assessment and reporting of results
AS 2508.6.028-1988	Safe storage and handling information card - Chloropicrin
AS 2508.8.012-1991	Safe storage and handling information card - Hydrogen fluoride (Anhydrous)(Anhydrous hydrofluoric acid)
AS 2243.7-1991	Safety in laboratories - Electrical aspects
AS 2508.6.016-1995	Safe storage and handling information card - Phenol (carbolic acid), cresols and cresylic acid
AS 2508.4.001-1982	Safe storage and handling information card - Calcium carbide
AS 2508.3.003-1982	Safe storage and handling information card - Acrylates (butyl, isobutyl)
AS 4264.2-1996	Coal and coke - Sampling Coke - Sampling procedures (Reconfirmed 2013)
AS 2508.3.030-1983	Safe storage and handling information card - Cyclohexane
AS 2508.6.024-1984	Safe storage and handling information card - Pentachlorophenol
AS 2508.6.003-1984	Safe storage and handling information card - Aniline (aminobenzene)
AS 1038.6.1-1997	Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Carbon and hydrogen (Reconfirmed 2013)
AS 2508.6.004-1984	Safe storage and handling information card - Cadmium compounds (other than selenide and sulphide)
AS 2508.6.006-1982	Safe storage and handling information card - Beryllium and compounds
AS 2508.8.018-1995	Safe storage and handling information card - Formaldehyde solutions (with not less than 25 percent formaldehyde)
AS 2508.8.002-1986	Safe storage and handling information card - Hydrochloric acid (muriatic acid, spirits of salts)
AS 2508.8.004-1992	Safe storage and handling information card - Acetic acid (containing more than 80 percent acid, by mass, in water)
AS 2508.2.011-1984	Safe storage and handling information card - Butadiene (inhibited)
AS 2508.3.024-1995	Safe storage and handling information card - Dimethylamine solution
AS 2508.8.016-1988	Safe storage and handling information card - Phosphoric acid (Orthophosphoric acid)
AS 2508.2.004-1995	Safe storage and handling information card - Ammonia (anhydrous)
AS 2508.2.002-1992	Safe storage and handling information card - Hydrogen (compressed)
AS 2508.6.014-1989	Safe storage and handling information card - Cyanides, inorganic (other than Sodium and Potassium Cyanides for which refer to AS 2508.6.002)
AS 2508.8.010-1990	Safe storage and handling information cards for hazardous materials - Sulfuric acid (up to 98% m/m)
AS 2508.8.005-1992	Safe storage and handling information card - Acetic acid (containing more than 10 percent but not more than 80 percent acid, by mass, in water)
AS 2508.6.023-1989	Safe storage and handling information card - Phenylmercuric compounds
AS 2508.3.028-1983	Safe storage and handling information card - Ethylene dichloride (1,2-dichloroethane, ethylene chloride (EDC))
AS 2508.8.001-1995	Safe storage and handling information card - Acetic anhydride
AS 2418-1995	Coal and coke - Glossary of terms (Reconfirmed 2013) (Reconfirmed 2023)
AS 2508.6.012-1988	Safe storage and handling information card - Diphenyl methane-4, 4-Diisocyanate [Methylene bis-(Phenylene) Diisocyanate] (MDI)
AS 2508.6.005-1984	Safe storage and handling information card - Fluorides (ammonium, potassium, magnesium or sodium fluoride)
AS 2508.2.006-1995	Safe storage and handling information card - Ethylene oxide
AS 2243.10-1993	Safety in laboratories - Storage of chemicals
AS 2508.6.011-1988	Safe storage and handling information card - Tetrachloroethylene (Perchloroethylene, Per or Perc)
AS 2508.6.001-1988	Safe storage and handling information card - Carbon tetrachloride (tetrachloromethane)
AS 1038.16-2005	Coal and coke - Analysis and testing Assessment and reporting of results (Reconfirmed 2016)
AS 2508.3.009-1982	Safe storage and handling information card - Hydrocarbon solvents
AS 2508.8.017-1988	Safe storage and handling information card - Aluminium chloride (Anhydrous)
AS 2508.6.022-1986	Safe storage and handling information card - Copper-chrome-arsenic
AS 2508.3.025-1983	Safe storage and handling information cards for hazardous materials - Chlorobenzene (monochlorobenzene)
AS 2508.3.029-1983	Safe storage and handling information card - Glycol ethers (flammable)
AS 2508.10.001-2000	Safe storage and handling information card - Agricultural and veterinary chemicals (Packaged products only)
AS 2243.4-1998	Safety in laboratories - Ionizing radiations
AS 2508.3.015-1992	Safe storage and handling information card - Toluene (toluol)
AS 2508.3.010-1995	Safe storage and handling information card - Amines (isopropylamine, diethylamine, triethylamine)
AS 2706-1984	Numerical values - Rounding and interpretation of limiting values
AS 2508.3.005-1995	Safe storage and handling information card - Benzene
AS 2508.6.021-1984	Safe storage and handling information card - Sodium pentachlorophenate
AS 2508.3.006-1995	Safe storage and handling information card - Butanols, propanols, amyl alcohols
AS 2508.8.009-1990	Safe storage and handling information card - Sulfuric acid (Oleum)
AS 2508.6.025-1984	Safe storage and handling information card - Arsenic acid
AS 2508.5.005-1992	Safe storage and handling information card - Methyl ethyl ketone peroxide (MEKP) (not more than 50% in solution with not more than 10% available oxygen)
AS 2243.1-1990	Safety in laboratories General
AS 2243.9-1991	Safety in laboratories - Recirculating fume cabinets
AS 2508.2.009-1984	Safe storage and handling information card - Oxygen (refrigerated liquid)
AS 2508.6.018-1989	Safe storage and handling information card - Lead arsenate and Lead aresenite
AS 2508.3.016-1982	Safe storage and handling information card - Methyl isobutyl ketone (MIBK)
AS 2508.6.008-1989	Safe storage and handling information card - Ammonium thioglycolate
AS 2508.3.027-1983	Safe storage and handling information card - Diacetone alcohol
AS 2508.8.015-1988	Safe storage and handling information card - Dilute ammonia solution containing 10 percent up to 35 percent m/m ammonia
AS 2508.3.007-1995	Safe storage and handling information card - Carbon disulphide
AS 2508.3.008-1983	Safe storage and handling information cards for hazardous materials - Acrylonitrile (inhibited)
AS 2508.3.001-1982	Safe storage and handling information card - Acetone
AS 2508.3.034-1984	Safe storage and handling information card - Pentanes
AS 2508.3.011-1992	Safe storage and handling information card - Methanol (methyl alcohol)
AS 2508.2.010-1984	Safe storage and handling information card - Sulphur dioxide (liquefied)
AS 2508.6.027-1984	Safe storage and handling information card - Tributyltin-oxide
AS 2706-2003	Numerical values - Rounding and interpretation of limiting values (Reconfirmed 2018)
AS 2508.3.014-1992	Safe storage and handling information card - Xylenes (xylols)
AS 2508.2.013-1992	Safe storage and handling information card - Ethylene (ethene)
AS 2508.3.013-1984	Safe storage and handling information card - Methyl ethyl ketone (MEK)
AS 2508.6.026-1984	Safe storage and handling information card - Formaldehyde solutions - Flashpoint above 61 degrees Celsius
AS 1038.4-1995	Coal and coke - Analysis and testing Coke - Proximate analysis
AS 2508.3.012-1982	Safe storage and handling information card - Styrene (vinyl benzene, styrene monomer)
AS 2508.6.017-1989	Safe storage and handling information card - Lead acetate
AS 2243.5-1993	Safety in laboratories Non-ionizing radiations
AS 4264.1-1995	Coal and coke - Sampling Higher rank coal - Sampling procedures

AS 1038.8.2-2003	Coal and coke - Analysis and testing Coal and coke - Chlorine - High-temperature combustion method (Reconfirmed 2013)
AS 1038.6.1-1997	Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Carbon and hydrogen (Reconfirmed 2013)
AS 1038.11-2002	Coal and coke - Analysis and testing Coal - Forms of sulfur (Reconfirmed 2013)
AS 2096-1987	Classification and coding systems for Australian coals (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.14.2-2003	Coal and coke - Analysis and testing Higher rank coal ash and coke ash - Major and minor elements - Acid digestion/flame atomic absorption spectrometric method (Reconfirmed 2013)
AS 1038.16-2005	Coal and coke - Analysis and testing Assessment and reporting of results (Reconfirmed 2016)
AS 2519-1993	Guide to the technical evaluation of higher rank coal deposits (Reconfirmed 2013) (Reconfirmed 2023)
TR 2.12B-3	Reference Materials - Coal - Preparation of ASRM 012B-3
AS 1038.14.1-2003	Coal and coke - Analysis and testing Higher rank coal ash and coke ash - Major and minor elements - Borate fusion/flame atomic absorption spectrometric method (Reconfirmed 2013)
AS 1038.22-2000	Coal and coke - Analysis and testing Higher rank coal - Mineral matter and water of constitution (Reconfirmed 2013) (Reconfirmed 2023)
TR 2.12C-3-2008	Certified reference materials Coal - Preparation and certification of ASCRM 012C-3
AS 2418-1995	Coal and coke - Glossary of terms (Reconfirmed 2013) (Reconfirmed 2023)

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AS 1038.6.3.2-2003

Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Total sulfur - High-temperature combustion method (Reconfirmed 2013)

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