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AS
AS 1038.6.3.2-2003

AS 1038.6.3.2-2003

Withdrawn

Withdrawn

A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.

Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Total sulfur - High-temperature combustion method (Reconfirmed 2013)

Available format(s)

Hardcopy , PDF 1 User , PDF 3 Users , PDF 5 Users , PDF 9 Users

Withdrawn date

10-11-2023

Language(s)

English

Published date

29-09-2003

Publisher

Standards Australia

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Hardcopy - English
PDF 1 User - English
PDF 3 Users - English
PDF 5 Users - English
PDF 9 Users - English
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This Standard has been reconfirmed. To view or download the Reconfirmation Notice please click here.

1 - AS 1038.6.3.2-2003 COAL AND COKE-ANALYSIS AND TESTING - HIGHER RANK COAL AND COKE-ULTIMATE ANALYSIS-TOTAL SULFUR-HIGH...
4 - PREFACE
5 - CONTENTS
6 - FOREWORD
7 - 1 SCOPE
7 - 2 REFERENCED DOCUMENTS
7 - 3 DEFINITIONS
7 - 3.1 Repeatability (r)
7 - 4 PRINCIPLE
8 - 5 SAFETY
8 - 6 REAGENTS
8 - 6.1 General
8 - 6.2 Aluminium oxide
8 - 6.3 Alkaline absorbent
8 - 6.4 Sodium tetraborate solution (0.025 mol/L)
8 - 6.5 Standard sulfuric acid solution (0.0125 mol/L)
8 - 6.6 Hydrogen peroxide solution (9 g/L)
8 - 6.7 Mercury(II) oxycyanide solution
8 - 6.8 Screened indicator solution
9 - 6.9 Oxygen
9 - 7 APPARATUS
9 - 7.1 Purification train
9 - 7.2 Heating unit
9 - 7.3 Combustion tube
9 - 7.4 Combustion boat
9 - 7.5 Silica pusher
9 - 7.6 Nickel-chromium wire
9 - 7.7 Flowmeter
9 - 7.8 Pressure gauge
10 - 7.9 Silica adaptor
10 - 7.10 Absorption vessel
10 - 7.11 Heat-resistant stopper or tubing
10 - 7.12 Pressure regulator
10 - 7.13 Vacuum pump
10 - 7.14 Weighing device
10 - 8 SAMPLE
10 - 9 PROCEDURE
10 - 9.1 Preparation of apparatus
11 - 9.2 Determination of the blank
12 - 9.3 Combustion and absorption
12 - 9.4 Measurement
13 - 10 CALCULATION
13 - 11 REPORTING OF RESULTS
13 - 12 PRECISION
13 - 13 TEST REPORT

Sets out a method for determining the total sulfur content of an analysis sample by high temperature combustion.

Committee
MN-001
DocumentType
Standard
ISBN
0 7337 5483 X
Pages
7
ProductNote
Reconfirmed 06-08-2013
PublisherName
Standards Australia
Status
Withdrawn
Supersedes

This Standard sets out a method for the determination of total sulfur in the analysis sample of higher rank coal and coke by the high-temperature combustion method.

Originated as part of AS CK2.3-1949.
Previous edition AS 1038.6.3.2-1997.
Third edition 2003.

AS 2508.6.020-1991 Safe storage and handling information card - Selenious acid, selenates and selenites
AS 2508.6.019-1995 Safe storage and handling information card - Lead alkyls
AS 1038.8.2-2003 Coal and coke - Analysis and testing Coal and coke - Chlorine - High-temperature combustion method (Reconfirmed 2013)
AS 2508.3.018-1983 Safe storage and handling information card - Methyl isobutyl carbinol
AS 2508.3.019-1983 Safe storage and handling information card - Methacrylates, HFP
AS 2243.6-1990 Safety in laboratories - Mechanical aspects
AS 2508.2.008-1984 Safe storage and handling information card - Oxygen (compressed)
AS 2508.8.006-1992 Safe storage and handling information card - Sodium hydroxide (solid and solution) (caustic soda)
AS 2508.5.004-1991 Safe storage and handling information card - Benzoyl peroxide
AS 2508.8.014-1985 Safe storage and handling information card - Mercury metal
AS 1038.4-2006 Coal and coke - Analysis and testing Coke - Proximate analysis
AS 2508.6.009-1990 Safe storage and handling information card - 1,1,1-trichloroethane (Methylchloroform)
AS 2508.3.033-1984 Safe storage and handling information card - Isoprene, inhibited
AS 2508.6.002-1985 Safe storage and handling information card - Cyanides (sodium and potassium)
AS 2508.3.032-1984 Safe storage and handling information card - Glycol ether acetates
AS 2508.2.007-2001 Safe storage and handling information card - Liquefied petroleum gas
AS 2508.8.013-1991 Safe storage and handling information card - Hydrofluoric acid (aqueous)
AS 2508.3.017-1983 Safe storage and handling information card - Ethanol/methylated spirits
AS 2508.5.001-1989 Safe storage and handling information card - Hydrogen peroxide
AS 2508.3.026-1995 Safe storage and handling information card - Propylene oxide
AS 2508.8.007-1990 Safe storage and handling information card - Nitric acid
AS 2508.5.003-1990 Safe storage and handling information card - Calcium hypochlorite
AS 2508.6.015-1983 Safe storage and handling information card - Methylene chloride (Dichloromethane)
AS 1038.3-2000 Coal and coke - Analysis and testing - Proximate analysis of higher rank coal
AS 2508.2.012-1985 Safe storage and handling information card - Non-flammable, inert, compressed gases (includes: argon, helium, krypton, neon, nitrogen and xenon)
AS 2508.3.020-1983 Safe storage and handling information card - Ethyl benzene
AS 2508.3.031-1983 Safe storage and handling information card - Tetrahydrofuran (THF)
AS 2508.3.002-1982 Safe storage and handling information card - Acetates (ethyl acetate, propyl acetates, butyl acetates, amyl acetate)
AS 2243.2-1990 Safety in laboratories - Chemical aspects
AS 2508.3.004-1982 Safe storage and handling information card - Acrylates (methyl, ethyl)
AS 2508.8.003-1990 Safe storage and handling information card - Sodium hypochlorite Hypochlorite solutions
AS 2508.2.005-1984 Safe storage and handling information card - Chlorine (compressed)
AS 2508.8.008-1992 Safe storage and handling information card - Maleic anhydride
AS 2243.8-1992 Safety in laboratories Fume cupboards
AS 2508.6.013-1991 Safe storage and handling information card - Trichloroethylene
AS 2508.2.001-1992 Safe storage and handling information card - Acetylene (Dissolved) (Ethyne)
AS 2508.6.007-1995 Safe storage and handling information card - Epichlorohydrin (Ech or 1-Chloro-2,3-epoxypropane)
AS 2508.2.003-1995 Safe storage and handling information card - Vinyl chloride (inhibited)
AS 2508.8.011-1995 Safe storage and handling information card - Methacrylic acid (inhibited)
AS 2508.3.023-1983 Safe storage and handling information card - Vinyl acetate (vinyl acetate monomer)
AS 2243.3-1991 Safety in laboratories Microbiology
AS 2508.3.022-1983 Safe storage and handling information card - Cumene (isopropyl-benzene)
AS 2508.3.021-1983 Safe storage and handling information card - Cyclohexanone
AS 2508.6.010-1983 Safe storage and handling information card - Toluene diisocyanate (TDI)
AS 2508.5.002-1990 Safe storage and handling information card - Ammonium nitrate
AS 1038.16-1996 Coal and coke - Analysis and testing - Assessment and reporting of results
AS 2508.6.028-1988 Safe storage and handling information card - Chloropicrin
AS 2508.8.012-1991 Safe storage and handling information card - Hydrogen fluoride (Anhydrous)(Anhydrous hydrofluoric acid)
AS 2243.7-1991 Safety in laboratories - Electrical aspects
AS 2508.6.016-1995 Safe storage and handling information card - Phenol (carbolic acid), cresols and cresylic acid
AS 2508.4.001-1982 Safe storage and handling information card - Calcium carbide
AS 2508.3.003-1982 Safe storage and handling information card - Acrylates (butyl, isobutyl)
AS 4264.2-1996 Coal and coke - Sampling Coke - Sampling procedures (Reconfirmed 2013)
AS 2508.3.030-1983 Safe storage and handling information card - Cyclohexane
AS 2508.6.024-1984 Safe storage and handling information card - Pentachlorophenol
AS 2508.6.003-1984 Safe storage and handling information card - Aniline (aminobenzene)
AS 1038.6.1-1997 Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Carbon and hydrogen (Reconfirmed 2013)
AS 2508.6.004-1984 Safe storage and handling information card - Cadmium compounds (other than selenide and sulphide)
AS 2508.6.006-1982 Safe storage and handling information card - Beryllium and compounds
AS 2508.8.018-1995 Safe storage and handling information card - Formaldehyde solutions (with not less than 25 percent formaldehyde)
AS 2508.8.002-1986 Safe storage and handling information card - Hydrochloric acid (muriatic acid, spirits of salts)
AS 2508.8.004-1992 Safe storage and handling information card - Acetic acid (containing more than 80 percent acid, by mass, in water)
AS 2508.2.011-1984 Safe storage and handling information card - Butadiene (inhibited)
AS 2508.3.024-1995 Safe storage and handling information card - Dimethylamine solution
AS 2508.8.016-1988 Safe storage and handling information card - Phosphoric acid (Orthophosphoric acid)
AS 2508.2.004-1995 Safe storage and handling information card - Ammonia (anhydrous)
AS 2508.2.002-1992 Safe storage and handling information card - Hydrogen (compressed)
AS 2508.6.014-1989 Safe storage and handling information card - Cyanides, inorganic (other than Sodium and Potassium Cyanides for which refer to AS 2508.6.002)
AS 2508.8.010-1990 Safe storage and handling information cards for hazardous materials - Sulfuric acid (up to 98% m/m)
AS 2508.8.005-1992 Safe storage and handling information card - Acetic acid (containing more than 10 percent but not more than 80 percent acid, by mass, in water)
AS 2508.6.023-1989 Safe storage and handling information card - Phenylmercuric compounds
AS 2508.3.028-1983 Safe storage and handling information card - Ethylene dichloride (1,2-dichloroethane, ethylene chloride (EDC))
AS 2508.8.001-1995 Safe storage and handling information card - Acetic anhydride
AS 2418-1995 Coal and coke - Glossary of terms (Reconfirmed 2013) (Reconfirmed 2023)
AS 2508.6.012-1988 Safe storage and handling information card - Diphenyl methane-4, 4-Diisocyanate [Methylene bis-(Phenylene) Diisocyanate] (MDI)
AS 2508.6.005-1984 Safe storage and handling information card - Fluorides (ammonium, potassium, magnesium or sodium fluoride)
AS 2508.2.006-1995 Safe storage and handling information card - Ethylene oxide
AS 2243.10-1993 Safety in laboratories - Storage of chemicals
AS 2508.6.011-1988 Safe storage and handling information card - Tetrachloroethylene (Perchloroethylene, Per or Perc)
AS 2508.6.001-1988 Safe storage and handling information card - Carbon tetrachloride (tetrachloromethane)
AS 1038.16-2005 Coal and coke - Analysis and testing Assessment and reporting of results (Reconfirmed 2016)
AS 2508.3.009-1982 Safe storage and handling information card - Hydrocarbon solvents
AS 2508.8.017-1988 Safe storage and handling information card - Aluminium chloride (Anhydrous)
AS 2508.6.022-1986 Safe storage and handling information card - Copper-chrome-arsenic
AS 2508.3.025-1983 Safe storage and handling information cards for hazardous materials - Chlorobenzene (monochlorobenzene)
AS 2508.3.029-1983 Safe storage and handling information card - Glycol ethers (flammable)
AS 2508.10.001-2000 Safe storage and handling information card - Agricultural and veterinary chemicals (Packaged products only)
AS 2243.4-1998 Safety in laboratories - Ionizing radiations
AS 2508.3.015-1992 Safe storage and handling information card - Toluene (toluol)
AS 2508.3.010-1995 Safe storage and handling information card - Amines (isopropylamine, diethylamine, triethylamine)
AS 2706-1984 Numerical values - Rounding and interpretation of limiting values
AS 2508.3.005-1995 Safe storage and handling information card - Benzene
AS 2508.6.021-1984 Safe storage and handling information card - Sodium pentachlorophenate
AS 2508.3.006-1995 Safe storage and handling information card - Butanols, propanols, amyl alcohols
AS 2508.8.009-1990 Safe storage and handling information card - Sulfuric acid (Oleum)
AS 2508.6.025-1984 Safe storage and handling information card - Arsenic acid
AS 2508.5.005-1992 Safe storage and handling information card - Methyl ethyl ketone peroxide (MEKP) (not more than 50% in solution with not more than 10% available oxygen)
AS 2243.1-1990 Safety in laboratories General
AS 2243.9-1991 Safety in laboratories - Recirculating fume cabinets
AS 2508.2.009-1984 Safe storage and handling information card - Oxygen (refrigerated liquid)
AS 2508.6.018-1989 Safe storage and handling information card - Lead arsenate and Lead aresenite
AS 2508.3.016-1982 Safe storage and handling information card - Methyl isobutyl ketone (MIBK)
AS 2508.6.008-1989 Safe storage and handling information card - Ammonium thioglycolate
AS 2508.3.027-1983 Safe storage and handling information card - Diacetone alcohol
AS 2508.8.015-1988 Safe storage and handling information card - Dilute ammonia solution containing 10 percent up to 35 percent m/m ammonia
AS 2508.3.007-1995 Safe storage and handling information card - Carbon disulphide
AS 2508.3.008-1983 Safe storage and handling information cards for hazardous materials - Acrylonitrile (inhibited)
AS 2508.3.001-1982 Safe storage and handling information card - Acetone
AS 2508.3.034-1984 Safe storage and handling information card - Pentanes
AS 2508.3.011-1992 Safe storage and handling information card - Methanol (methyl alcohol)
AS 2508.2.010-1984 Safe storage and handling information card - Sulphur dioxide (liquefied)
AS 2508.6.027-1984 Safe storage and handling information card - Tributyltin-oxide
AS 2706-2003 Numerical values - Rounding and interpretation of limiting values (Reconfirmed 2018)
AS 2508.3.014-1992 Safe storage and handling information card - Xylenes (xylols)
AS 2508.2.013-1992 Safe storage and handling information card - Ethylene (ethene)
AS 2508.3.013-1984 Safe storage and handling information card - Methyl ethyl ketone (MEK)
AS 2508.6.026-1984 Safe storage and handling information card - Formaldehyde solutions - Flashpoint above 61 degrees Celsius
AS 1038.4-1995 Coal and coke - Analysis and testing Coke - Proximate analysis
AS 2508.3.012-1982 Safe storage and handling information card - Styrene (vinyl benzene, styrene monomer)
AS 2508.6.017-1989 Safe storage and handling information card - Lead acetate
AS 2243.5-1993 Safety in laboratories Non-ionizing radiations
AS 4264.1-1995 Coal and coke - Sampling Higher rank coal - Sampling procedures

AS 1038.8.2-2003 Coal and coke - Analysis and testing Coal and coke - Chlorine - High-temperature combustion method (Reconfirmed 2013)
AS 1038.6.1-1997 Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Carbon and hydrogen (Reconfirmed 2013)
AS 1038.11-2002 Coal and coke - Analysis and testing Coal - Forms of sulfur (Reconfirmed 2013)
AS 2096-1987 Classification and coding systems for Australian coals (Reconfirmed 2013) (Reconfirmed 2023)
AS 1038.14.2-2003 Coal and coke - Analysis and testing Higher rank coal ash and coke ash - Major and minor elements - Acid digestion/flame atomic absorption spectrometric method (Reconfirmed 2013)
AS 1038.16-2005 Coal and coke - Analysis and testing Assessment and reporting of results (Reconfirmed 2016)
AS 2519-1993 Guide to the technical evaluation of higher rank coal deposits (Reconfirmed 2013) (Reconfirmed 2023)
TR 2.12B-3 Reference Materials - Coal - Preparation of ASRM 012B-3
AS 1038.14.1-2003 Coal and coke - Analysis and testing Higher rank coal ash and coke ash - Major and minor elements - Borate fusion/flame atomic absorption spectrometric method (Reconfirmed 2013)
AS 1038.22-2000 Coal and coke - Analysis and testing Higher rank coal - Mineral matter and water of constitution (Reconfirmed 2013) (Reconfirmed 2023)
TR 2.12C-3-2008 Certified reference materials Coal - Preparation and certification of ASCRM 012C-3
AS 2418-1995 Coal and coke - Glossary of terms (Reconfirmed 2013) (Reconfirmed 2023)

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