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AS 2816-1992

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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Copper, lead and zinc sulfide concentrates - Determination of hygroscopic moisture in the analysis sample - Gravimetric method

Available format(s)

Hardcopy , PDF 1 User , PDF 3 Users , PDF 5 Users , PDF 9 Users

Superseded date

30-06-2017

Superseded by

AS ISO 9599:2016

Language(s)

English

Published date

01-01-1992

€15.02
Excluding VAT

1 - AS 2816-1992 COPPER, LEAD AND ZINC CULFIDE CONCENTRATES-DETERMINATION OF HYGROSCOPIC MOISTURE IN THE ANALYSIS SAMPLE-GRAVIMER
4 - PREFACE
5 - Foreword
6 - 1 Scope
6 - 2 Principl e
6 - 3 Reagents
6 - 3.1 Desiccant,
6 - 4 Apparatus
6 - 4.1 Analytical balance,
6 - 4.2 Laboratory oven,
6 - 4.3 Weighing vessels,
6 - 4.4 Flat dish,
6 - 5 Sampling and samples
6 - 5.1 Laboratory sample
6 - 5.2 Preparation of the test sample
7 - 6 Procedure
7 - 6.1 Preparation of the weighing vessel
7 - 6.2 Test portion
7 - 6.3 Determination
7 - 7 ExpressI on of results
7 - 8 Test report
8 - Annex A - Method for samples susceptible to oxidation - Drying in nitrogen
8 - A.1 Principl e
8 - A.2 Reagents
8 - A.3 Apparatus
8 - A.4 Procedure
9 - A.5 Expressi on of results
9 - A.6 Test report
10 - Annex B - Bibliography

Specifies a gravimetric loss-in-mass method for the determination of hygroscopic moisture content. Applicable to copper, lead and zinc sulfide concentrates with hygroscopic moisture contents between 0.05 percent (m/m) and 2 percent (m/m). This Standard is identical with and reproduced from ISO 9599:1991.

Committee
MN-005
DocumentType
Standard
ISBN
0 7262 7124 1
Pages
5
PublisherName
Standards Australia
Status
Superseded
SupersededBy
Supersedes
UnderRevision

This International Standard specifies a gravimetric loss-in-mass method for the determination of the hygroscopic moisture content in analysis samples of copper, lead and zinc sulfide concentrates.The method is applicable to copper, lead and zinc sulfide concentrates free from volatile organic flotation reagents, for example kerosene, and with hygroscopic moisture contents between 0,05 % (m/m) and 2 % (m/m). It is used to correct the analysis results from the equilibrated moisture level to the dry basis.NOTE 1 The result of the determination of hygroscopic moisture using this International Standard should not be reported as part of the analysis of a concentrate sample. When the bulk moisture content of a commercial shipment of concentrate is required, the method specified [1]should be used. The determination of hygroscopic moisture and the determination of bulk moisture content are connected with each other. In both determinations the same state of dryness has to be achieved, in order to ascertain the correct metal content of a lot.This method is not applicable to sulfide concentrates which are susceptible to oxidation (see 6.3, note 2). Annex A sets out a modified procedure which can be used in this case.

Standards Relationship
ISO 9599:1991 Identical

First published as AS 2816-1985.
Second edition 1992.

AS 2863-1999 Copper, lead and zinc sulfide concentrates - Determination of mass loss of bulk material on drying

AS 2917.3-1994 Copper sulfide concentrates - Determination of copper content - Electrogravimetric method
AS 4030.1-2002 Lead sulfide concentrates - Chemical analysis Determination of lead content - EDTA titration method after acid digestion
AS 2917.1-1986 Methods for the analysis of copper sulphide concentrates - Determination of copper (short iodide titrimetric method)
AS 2917.3-2008 Copper sulfide concentrates Determination of copper - Electrogravimetric method (Reconfirmed 2021)
AS 2863-2008 Copper, lead, zinc and nickel concentrates - Determination of mass loss of bulk material on drying (Reconfirmed 2021)
AS 3895.1-1991 Methods for the analysis of copper, lead, zinc, gold and silver ores Determination of gold (Fire assay - Flame AAS method)
AS 2863-1999 Copper, lead and zinc sulfide concentrates - Determination of mass loss of bulk material on drying
AS 4030.1-1992 Methods for the analysis of lead sulfide concentrates Determination of lead content - Acid dissolution solvent extraction EDTA titration method
AS 2678.1-1999 Zinc sulfide concentrates - Chemical analysis Determination of zinc content - Solvent extraction and EDTA titrimetric method
AS 2678.2-1999 Zinc sulfide concentrates - Chemical analysis Determination of zinc content - Ion-exchange method
AS 2678.2-2008 Zinc sulfide concentrates - Chemical analysis Determination of zinc - Ion-exchange/EDTA titrimetric method
AS 2917.1-1994 Copper sulfide concentrates - Determination of copper content Titrimetric methods
AS 2917.2-1994 Copper sulfide concentrates - Determination of gold and silver contents Fire assay gravimetric and atomic absorption spectrometric method
AS 2678.1-2008 Zinc sulfide concentrates - Chemical analysis Determination of zinc - Solvent extraction and EDTA titrimetric method
AS 4030.2-1996 Methods for the analysis of lead sulfide concentrates Determination of lead content - Back titration of EDTA after precipitation of lead sulfate

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