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ASTM C 1068 : 2015

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by

Standard Guide for Qualification of Measurement Methods by a Laboratory Within the Nuclear Industry

Available format(s)

Hardcopy , PDF

Superseded date

10-11-2021

Superseded by

ASTM C 1068 : 2021

Language(s)

English

Published date

30-06-2015

€67.30
Excluding VAT

Committee
C 26
DocumentType
Guide
Pages
7
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1This guide provides guidance for selecting, validating, and qualifying measurement methods when qualification is required for a specific program. The recommended practices presented in this guide provide a major part of a quality assurance program for the laboratory data (see Fig. 1). Qualification helps to assure that the data produced will meet established requirements.

1.2The activities intended to assure the quality of analytical laboratory measurement data are diagrammed in Fig. 1. Discussion and guidance related to some of these activities appear in the following sections:

Section

Selection of Measurement Methods

5

Validation of Measurement Methods

6

Qualification of Measurement Methods

7

Control

8

Personnel Qualification

9

1.3This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

ASTM C 1316 : 2008 : R2017 Standard Test Method for Nondestructive Assay of Nuclear Material in Scrap and Waste by Passive-Active Neutron Counting Using <sup>252</sup>Cf Shuffler
ASTM C 1187 : 2015 Standard Guide for Establishing Surveillance Test Program for Boron-Based Neutron Absorbing Material Systems for Use in Nuclear Fuel Storage Racks In a Pool Environment
ASTM C 1672 : 2017 Standard Test Method for Determination of Uranium or Plutonium Isotopic Composition or Concentration by the Total Evaporation Method Using a Thermal Ionization Mass Spectrometer
ASTM C 697 : 2016 Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Plutonium Dioxide Powders and Pellets
ASTM C 1625 : 2019 Standard Test Method for Uranium and Plutonium Concentrations and Isotopic Abundances by Thermal Ionization Mass Spectrometry
ASTM C 1832 : 2021 Standard Test Method for Determination of Uranium Isotopic Composition by Modified Total Evaporation (MTE) Method Using Thermal Ionization Mass Spectrometer
ASTM C 1907 : 2021 Standard Practice for Preparation of Plutonium Materials by Pyrohydrolysis for Determination of Fluoride, Chloride, or Both
ASTM C 1187 : 2020 : REV A Standard Guide for Establishing Surveillance Test Program for Boron-based Neutron Absorbing Material Systems for Use in Nuclear Fuel Storage Racks in Pool Environment
ASTM C 759 : 2018 Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Plutonium Nitrate Solutions
ASTM C 1853 : 2017 Standard Test Method for The Determination of Carbon (Total) Content in Mixed Oxide ((U, Pu)O<inf>2</inf>) Sintered Pellets by Direct Combustion-Infrared Detection Method
ASTM C 1156 : 2018 Standard Guide for Establishing Calibration for a Measurement Method Used to Analyze Nuclear Fuel Cycle Materials
ASTM C 1625 : 2012 Standard Test Method for Uranium and Plutonium Concentrations and Isotopic Abundances by Thermal Ionization Mass Spectrometry
ASTM C 1854 : 2017 Standard Test Method for Determination of Hydrogen (total from all sources) in Mixed Oxide ((U, Pu)O<inf>2</inf>) Sintered Pellets by the Inert Gas Fusion Technique Followed by Thermal Conductivity Measurement
ASTM C 1855 : 2018 Standard Test Method for Determination of Uranium and Plutonium Concentration in Aqueous Solutions Using Hybrid K-Edge Densitometry and X-Ray Fluorescence
ASTM C 1009 : 2013 : REV A Standard Guide for Establishing and Maintaining a Quality Assurance Program for Analytical Laboratories Within the Nuclear Industry
ASTM C 698 : 2016 Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Mixed Oxides ((U, Pu)O<inf>2</inf>)
ASTM C 1832 : 2016 Standard Test Method for Determination of Uranium Isotopic Composition by the Modified Total Evaporation (MTE) Method Using a Thermal Ionization Mass Spectrometer
ASTM C 1742 : 2017 Standard Test Method for Isotopic Analysis of Uranium Hexafluoride by Double Standard Single-Collector Gas Mass Spectrometer Method (Withdrawn 2023)
ASTM C 1865 : 2018 Standard Test Method for The Determination of Carbon and Sulfur Content in Plutonium Oxide Powder by the Direct Combustion-Infrared Spectrophotometer
ASTM C 1210 : 2018 Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within the Nuclear Industry
ASTM C 1128 : 2018 Standard Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials
ASTM C 1267 : 2017 Standard Test Method for Uranium by Iron (II) Reduction in Phosphoric Acid Followed by Chromium (VI) Titration in the Presence of Vanadium
ASTM C 758 : 2018 Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Plutonium Metal
ASTM C 1817 : 2016 Standard Test Method for The Determination of the Oxygen to Metal (O/M) Ratio in Sintered Mixed Oxide ((U, Pu)O<inf>2</inf>) Pellets by Gravimetry
ASTM C 1871 : 2018 : REV A Standard Test Method for Determination of Uranium Isotopic Composition by the Double Spike Method Using a Thermal Ionization Mass Spectrometer
ASTM C 1108 : 2017 Standard Test Method for Plutonium by Controlled-Potential Coulometry
ASTM C 1207 : 2010 : R2018 Standard Test Method for Nondestructive Assay of Plutonium in Scrap and Waste by Passive Neutron Coincidence Counting
ASTM C 1165 : 2017 Standard Test Method for Determining Plutonium by Controlled-Potential Coulometry in H<inf>2</inf>SO<inf>4</inf> at a Platinum Working Electrode

ASTM C 1009 : 2013 : REV A Standard Guide for Establishing and Maintaining a Quality Assurance Program for Analytical Laboratories Within the Nuclear Industry
ASTM E 177 : 1990 : REV A : R1996 Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
ASTM E 2655 : 2008 Standard Guide for Reporting Uncertainty of Test Results and Use of the Term Measurement Uncertainty in ASTM Test Methods
ASTM C 1210 : 2018 Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within the Nuclear Industry
ASTM C 1128 : 2018 Standard Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials
ASTM C 1009 : 1996 : EDT 1 Standard Guide for Establishing a Quality Assurance Program for Analytical Chemistry Laboratories Within the Nuclear Industry (Withdrawn 2005)
ASTM C 1210 : 1996 : EDT 1 Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within the Nuclear Industry (Withdrawn 2005)
ASTM C 1210 : 2021 Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within Nuclear Industry
ASTM C 1128 : 1995 : EDT 1 Standard Guide for Preparation of Working Reference Materials for Use in the Analysis of Nuclear Fuel Cycle Materials
ASTM E 2554 : 2013 Standard Practice for Estimating and Monitoring the Uncertainty of Test Results of a Test Method Using Control Chart Techniques
ASTM C 1156 : 2003 : R2011 Standard Guide for Establishing Calibration for a Measurement Method Used to Analyze Nuclear Fuel Cycle Materials
ASTM C 1210 : 2012 Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within the Nuclear Industry
ASTM E 2655 : 2014 : R2020 Standard Guide for Reporting Uncertainty of Test Results and Use of the Term Measurement Uncertainty in ASTM Test Methods
ASTM C 1128 : 2015 Standard Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials
ASTM C 1210 : 2006 Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within the Nuclear Industry
ASTM E 2554 : 2018 : EDT 1 Standard Practice for Estimating and Monitoring the Uncertainty of Test Results of a Test Method Using Control Chart Techniques
ASTM C 1297 : 2003 : R2011 Standard Guide for Qualification of Laboratory Analysts for the Analysis of Nuclear Fuel Cycle Materials
ASTM C 1297 : 2003 Standard Guide for Qualification of Laboratory Analysts for the Analysis of Nuclear Fuel Cycle Materials
ASTM C 1297 : 1995 : EDT 1 Standard Guide for Qualification of Laboratory Analysts for the Analysis of Nuclear Fuel Cycle Materials
ASTM C 1156 : 2018 Standard Guide for Establishing Calibration for a Measurement Method Used to Analyze Nuclear Fuel Cycle Materials
ASTM E 2655 : 2014 Standard Guide for Reporting Uncertainty of Test Results and Use of the Term Measurement Uncertainty in ASTM Test Methods
ASTM C 1128 : 2001 Standard Guide for Preparation of Working Reference Materials for Use in the Analysis of Nuclear Fuel Cycle Materials
ASTM E 2554 : 2007 Standard Practice for Estimating and Monitoring the Uncertainty of Test Results of a Test Method in a Single Laboratory Using a Control Sample Program
ASTM C 1156 : 1995 : EDT 1 Standard Guide for Establishing Calibration for a Measurement Method Used to Analyze Nuclear Fuel Cycle Materials
ASTM E 2554 : 2018 Standard Practice for Estimating and Monitoring the Uncertainty of Test Results of a Test Method Using Control Chart Techniques
ASTM C 1009 : 2021 Standard Guide for Establishing and Maintaining a Quality Assurance Program for Analytical Laboratories Within the Nuclear Industry
ASTM C 1128 : 2001 : R2008 Standard Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials
ASTM C 1009 : 2013 Standard Guide for Establishing and Maintaining a Quality Assurance Program for Analytical Laboratories Within the Nuclear Industry
ASTM C 1156 : 2003 Standard Guide for Establishing Calibration for a Measurement Method Used to Analyze Nuclear Fuel Cycle Materials
ASTM C 1009 : 2006 Standard Guide for Establishing a Quality Assurance Program for Analytical Chemistry Laboratories Within the Nuclear Industry
ASTM C 1297 : 2018 Standard Guide for Qualification of Laboratory Analysts for the Analysis of Nuclear Fuel Cycle Materials

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