ASTM C 1108 : 1999
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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Standard Test Method for Plutonium by Controlled-Potential Coulometry
Hardcopy , PDF
11-11-2014
English
10-01-1999
Important note : Users cannot be edited or removed once added to your Multi user PDF.| Committee |
C 26
|
| DocumentType |
Test Method
|
| Pages |
8
|
| PublisherName |
American Society for Testing and Materials
|
| Status |
Superseded
|
| SupersededBy |
1.1 This test method describes the determination of plutonium in solutions of unirradiated nuclear-grade (that is, high-purity) materials by controlled-potential coulometry. Controlled-potential coulometry may be performed in a choice of supporting electrolytes, such as 0.9 HNO 3 , 1 HClO 4 , 1 HCl, 5 HCl, and 0.5 H 2 SO 4 . Limitations on the use of selected supporting electrolytes are discussed in Section 5. Optimum quantities of plutonium for this procedure are 5 to 10 mg.
1.2 Plutonium-bearing materials are radioactive and toxic. Adequate laboratory facilities, such as gloved boxes, fume hoods, controlled ventilation, etc., along with safe techniques must be used in handling specimens containing these materials.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
| ASTM C 1165 : 2017 | Standard Test Method for Determining Plutonium by Controlled-Potential Coulometry in H<inf>2</inf>SO<inf>4</inf> at a Platinum Working Electrode |
| ASTM C 1128 : 2018 | Standard Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials |
| ASTM C 759 : 2018 | Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Plutonium Nitrate Solutions |
| ASTM C 698 : 2016 | Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Mixed Oxides ((U, Pu)O<inf>2</inf>) |
| ASTM C 758 : 2018 | Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Plutonium Metal |
| ASTM C 697 : 2016 | Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Plutonium Dioxide Powders and Pellets |
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