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ASTM C 698 : 2016 : REDLINE

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Current

The latest, up-to-date edition.

Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Mixed Oxides ((U, Pu)O2)

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English

Published date

01-06-2016

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CONTAINED IN VOL. 12.01, 2016 Defines procedures for the chemical, mass spectrometric, and spectrochemical analysis of nucleargrade mixed oxides, (U, Pu)O[2], powders and pellets to determine compliance with specifications.

Committee
C 26
DocumentType
Redline
Pages
40
PublisherName
American Society for Testing and Materials
Status
Current

1.1These test methods cover procedures for the chemical, mass spectrometric, and spectrochemical analysis of nuclear-grade mixed oxides, (U, Pu)O2, powders and pellets to determine compliance with specifications.

1.2The analytical procedures appear in the following order:

Sections

Uranium in the Presence of Pu by Potentiometric Titration

  2

Plutonium by Controlled-Potential Coulometry

  2

Plutonium by Amperometric Titration with Iron (II)

  2

Nitrogen by Distillation Spectrophotometry Using Nessler Reagent

8 to 15

Carbon (Total) by Direct Combustion-Thermal Conductivity

16 to 26

Total Chlorine and Fluorine by Pyrohydrolysis

27 to 34

Sulfur by Distillation-Spectrophotometry

35 to 43

Moisture by the Coulometric, Electrolytic Moisture Analyzer

44 to 51

Isotopic Composition by Mass Spectrometry

  3

Rare Earths by Copper Spark Spectroscopy

52 to 59

Trace Impurities by Carrier Distillation Spectroscopy

60 to 68

Impurities by Spark-Source Mass Spectrography

69 to 75

Total Gas in Reactor-Grade Mixed Dioxide Pellets

   4

Tungsten by Dithiol-Spectrophotometry

76 to 84

Rare Earth Elements by Spectroscopy

85 to 88

Plutonium-238 Isotopic Abundance by Alpha Spectrometry

  5

Americium-241 in Plutonium by Gamma-Ray Spectrometry

Uranium and Plutonium Isotopic Analysis by Mass Spectrometry

89 to 97

Oxygen-to-Metal Atom Ratio by Gravimetry

98 to 105

1.3The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. (For specific safety precaution statements, see Sections 6, 13.2.5, 41.7, and 93.6.1.)

BS ISO 21613 : 2015 (U, PU)O[2] POWDERS AND SINTERED PELLETS - DETERMINATION OF CHLORINE AND FLUORINE
ASTM C 1854 : 2017 Standard Test Method for Determination of Hydrogen (total from all sources) in Mixed Oxide ((U, Pu)O<inf>2</inf>) Sintered Pellets by the Inert Gas Fusion Technique Followed by Thermal Conductivity Measurement
ASTM C 1030 : 2010 Standard Test Method for Determination of Plutonium Isotopic Composition by Gamma-Ray Spectrometry
ASTM D 6884 : 2003 : R2010 Standard Practice for Installation of Articulating Concrete Block (ACB) Revetment Systems
ASTM C 1853 : 2017 Standard Test Method for The Determination of Carbon (Total) Content in Mixed Oxide ((U, Pu)O<inf>2</inf>) Sintered Pellets by Direct Combustion-Infrared Detection Method
ASTM D 6884 : 2003 : R2015 : EDT 1 Standard Practice for Installation of Articulating Concrete Block (ACB) Revetment Systems (Withdrawn 2024)
ISO 21613:2015 (U, Pu)O2 Powders and sintered pellets — Determination of chlorine and fluorine
ASTM C 758 : 2004 : R2010 Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Plutonium Metal
ASTM C 1817 : 2016 : REDLINE Standard Test Method for The Determination of the Oxygen to Metal (O/M) Ratio in Sintered Mixed Oxide ((U, Pu)O<inf>2</inf>) Pellets by Gravimetry
I.S. EN ISO 21613:2017 (U, PU)O2 POWDERS AND SINTERED PELLETS - DETERMINATION OF CHLORINE AND FLUORINE (ISO 21613:2015)
EN ISO 21613:2017 (U, Pu)O2 Powders and sintered pellets - Determination of chlorine and fluorine (ISO 21613:2015)
ASTM C 1233 : 2015 : REDLINE Standard Practice for Determining Equivalent Boron Contents of Nuclear Materials
ASTM C 833 : 2017 : REDLINE Standard Specification for Sintered (Uranium-Plutonium) Dioxide Pellets for Light Water Reactors
ASTM C 1008 : 1999 : R2008 Standard Specification for Sintered (Uranium-Plutonium) Dioxide<br> Pellets<span class='unicode'>—</span>Fast Reactor Fuel (Withdrawn 2014)
13/30254322 DC : 0 BS ISO 21613 - (U, PU)O[2] POWDERS AND SINTERED PELLETS - DETERMINATION OF CHLORINE AND FLUORINE
ASTM C 1307 : 2015 : REDLINE Standard Test Method for Plutonium Assay by Plutonium (III) Diode Array Spectrophotometry
ASTM D 6884 : 2003 Standard Practice for Installation of Articulating Concrete Block (ACB) Revetment Systems
ASTM C 1816 : 2016 : REDLINE Standard Practice for The Ion Exchange Separation of Small Volume Samples Containing Uranium, Americium, and Plutonium Prior to Isotopic Abundance and Content Analysis
ANSI N15.35 : 1983 NONDESTRUCTIVE ASSAY BY COUNTING PASSIVE GAMMA RAYS, GUIDE TO PREPARING CALIBRATION MATERIAL FOR,
ASTM C 1411 : 2014 : REDLINE Standard Practice for The Ion Exchange Separation of Uranium and Plutonium Prior to Isotopic Analysis
ASTM C 1008 : 1999 Standard Specification for Sintered (Uranium-Plutonium) Dioxide Pellets-Fast Reactor Fuel
ASTM C 1682 : 2017 : REDLINE Standard Guide for Characterization of Spent Nuclear Fuel in Support of Interim Storage, Transportation and Geologic Repository Disposal
ASTM C 758 : 2004 Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Plutonium Metal

ASTM C 1233 : 2015 : REDLINE Standard Practice for Determining Equivalent Boron Contents of Nuclear Materials
ASTM C 697 : 2016 : REDLINE Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Plutonium Dioxide Powders and Pellets
ASTM C 1625 : 2012 : REDLINE Standard Test Method for Uranium and Plutonium Concentrations and Isotopic Abundances by Thermal Ionization Mass Spectrometry
ASTM C 1637 : 2013 : REDLINE Standard Test Method for the Determination of Impurities in Plutonium Metal: Acid Digestion and Inductively Coupled Plasma-Mass Spectroscopy (ICP-MS) Analysis
ASTM E 116 : 1997 Standard Practice for Photographic Photometry in Spectrochemical Analysis (Withdrawn 2002)
ASTM C 833 : 2017 : REDLINE Standard Specification for Sintered (Uranium-Plutonium) Dioxide Pellets for Light Water Reactors
ASTM C 1672 : 2017 : REDLINE Standard Test Method for Determination of Uranium or Plutonium Isotopic Composition or Concentration by the Total Evaporation Method Using a Thermal Ionization Mass Spectrometer
ASTM C 1817 : 2016 : REDLINE Standard Test Method for The Determination of the Oxygen to Metal (O/M) Ratio in Sintered Mixed Oxide ((U, Pu)O<inf>2</inf>) Pellets by Gravimetry
ASTM C 1432 : 2015 : REDLINE Standard Test Method for Determination of Impurities in Plutonium: Acid Dissolution, Ion Exchange Matrix Separation, and Inductively Coupled Plasma-Atomic Emission Spectroscopic (ICP/AES) Analysis
ASTM C 1068 : 2015 : REDLINE Standard Guide for Qualification of Measurement Methods by a Laboratory Within the Nuclear Industry
ASTM C 1168 : 2015 : REDLINE Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis
ASTM C 1204 : 2014 : REDLINE Standard Test Method for Uranium in Presence of Plutonium by Iron(II) Reduction in Phosphoric Acid Followed by Chromium(VI) Titration
ASTM E 115 : 1997 Standard Practice for Photographic Processing in Optical Emission Spectrographic Analysis (Withdrawn 2002)
ASTM C 1268 : 2015 : REDLINE Standard Test Method for Quantitative Determination of <sup>241</sup>Am in Plutonium by Gamma-Ray Spectrometry

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