ASTM D 4274 : 2016 : REDLINE
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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Standard Test Methods for Testing Polyurethane Raw Materials: Determination of Hydroxyl Numbers of Polyols
13-08-2021
English
01-04-2016
Important note : Users cannot be edited or removed once added to your Multi user PDF.CONTAINED IN VOL. 08.02, 2016 Defines the hydroxyl groups in polyester and polyether polypols containing primary and secondary hydroxyl groups.
| Committee |
D 20
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| DocumentType |
Redline
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| Pages |
13
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| PublisherName |
American Society for Testing and Materials
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| Status |
Superseded
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| SupersededBy |
1.1These test methods measure the hydroxyl groups in polyester and polyether polyols containing primary and secondary hydroxyl groups. They also apply to many other hydroxyl-containing substances.
1.1.1Test Method A—Acetic Anhydride Pressure Bottle, recommended for polyesters.
1.1.2Test Method B—Phthalic Anhydride Pressure Bottle, recommended for polyethers and polyesters.
1.1.3Test Method C—Phthalic Anhydride Reflux, recommended for polyethers and polyesters.
1.1.4Test Method D—Imidazole–Catalyzed Phthalic Anhydride Pressure Bottle, recommended for polyethers, polyesters, polymer polyols, and amine-initiated polyols.
1.1.5Test Method E—Imidazole-Catalyzed Pyromellitic Dianhydride Esterification, recommended for polyols used for flexible and rigid polyurethane foams and urethane elastomers. It is recommended for polyester polyols, polyether polyols, amine-started polyols, and polymer polyols (polyacrylonitrile/copolystyrene-based).
1.2Another ASTM test method for measuring hydroxyl groups is Test Method E222.
1.3The values stated in SI units are to be regarded as the standard.
1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Note 1:This standard, ISO 14900 and ISO 6796 address the same subject matter, but differ in technical content.
| Standards | Relationship |
| UNE 53985-1:2004 | Identical |
| BS ISO 14900:2017 | Plastics. Polyols for use in the production of polyurethane. Determination of hydroxyl number |
| ASTM D 6342 : 2012 : R2017 : EDT 1 | Standard Practice for Polyurethane Raw Materials: Determining Hydroxyl Number of Polyols by Near Infrared (NIR) Spectroscopy |
| ASTM E 1899 : 2016 : REDLINE | Standard Test Method for Hydroxyl Groups Using Reaction with <emph type="ital">p</emph >-Toluenesulfonyl Isocyanate (TSI) and Potentiometric Titration with Tetrabutylammonium Hydroxide |
| ISO 14900:2017 | Plastics — Polyols for use in the production of polyurethane — Determination of hydroxyl number |
| NASA MSFC PROC 3687 : 2015 | MATERIAL SPECIFICATION FOR POLYURETHANE FOAM - SPRAYABLE |
| NASA MSFC SPEC 2083 : 2007 | MULTIPROGRAM/PROJECT COMMON USE DOCUMENT FOAM, POLYURETHANE |
| NASA MSFC SPEC 3686 : A2015 | MATERIAL SPECIFICATION FOR POLYURETHANE FOAM - SPRAYABLE |
| ASTM D 6342 : 20121 | Standard Practice for Polyurethane Raw Materials: Determining Hydroxyl Number of Polyols by Near Infrared (NIR) Spectroscopy |
| ASTM E 222 : 2017 : REDLINE | Standard Test Methods for Hydroxyl Groups Using Acetic Anhydride Acetylation |
| ISO 6796:1981 | Polyglycols for industrial use — Determination of hydroxyl number — Phthalic anhydride esterification method |
| ASTM E 200 : 2016 : REDLINE | Standard Practice for Preparation, Standardization, and Storage of Standard and Reagent Solutions for Chemical Analysis |
| ASTM E 180 : 2003 | Standard Practice for Determining the Precision of ASTM Methods for Analysis and Testing of Industrial and Specialty Chemicals (Withdrawn 2009) |
| ASTM E 203 : 2016 : REDLINE | Standard Test Method for Water Using Volumetric Karl Fischer Titration |
| ISO 14900:2017 | Plastics — Polyols for use in the production of polyurethane — Determination of hydroxyl number |
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