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  • ASTM D 4307 : 2017 : REDLINE

    Current The latest, up-to-date edition.

    Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards

    Available format(s):  PDF

    Language(s):  English

    Published date:  01-05-2017

    Publisher:  American Society for Testing and Materials

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    Abstract - (Show below) - (Hide below)

    CONTAINED IN VOL. 05.02, 2015 Defines a laboratory procedure for the preparation of small volumes of multicomponent liquid blends for use as analytical standards.

    Scope - (Show below) - (Hide below)

    1.1This practice covers a laboratory procedure for the preparation of small volumes of multicomponent liquid blends for use as analytical standards.

    1.2This practice is applicable to components that are normally liquids at ambient temperature and pressure, or solids that will form a solution when blended with liquids. Butanes can be included if precaution is used in blending them.

    1.3This practice is limited to those components that fulfill the following conditions:

    1.3.1They are completely soluble in the final blend.

    1.3.2They are not reactive with other blend components or with blend containers.

    1.3.3The combined vapor pressure of the blended components is such that there is no selective evaporation of any of the components.

    1.3.3.1The butane content of the blend is not to exceed 10 %. (Warning—Extremely flammable liquefied gas under pressure. Vapor reduces oxygen available for breathing.) Components with a vapor pressure higher than butanes are not to be blended.

    1.4The values stated in SI units are to be regarded as the standard.

    1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

    1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

    General Product Information - (Show below) - (Hide below)

    Committee D 02
    Document Type Redline
    Publisher American Society for Testing and Materials
    Status Current

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM D 5623 : 1994 : R2009 Standard Test Method for Sulfur Compounds in Light Petroleum Liquids by Gas Chromatography and Sulfur Selective Detection
    ASTM D 6296 : 1998 Standard Test Method for Total Olefins in Spark-Ignition Engine Fuels by Multi-dimensional Gas Chromatography
    ASTM D 6142 : 2016 : REDLINE Standard Test Method for Analysis of Phenol by Capillary Gas Chromatography
    ASTM D 7151 : 2015 : REDLINE Standard Test Method for Determination of Elements in Insulating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
    ASTM U 01 : 2013 Normal Paraffins by Subtractive GC
    ASTM D 7875 : 2014 Standard Test Method for Determination of Butanol and Acetone Content of Butanol for Blending with Gasoline by Gas Chromatography
    ASTM D 7578 : 2015-06 GUIDE FOR CALIBRATION REQUIREMENTS FOR ELEMENTAL ANALYSIS OF PETROLEUM PRODUCTS AND LUBRICANTS
    ASTM D 7040 :2004 Standard Test Method for Determination of Low Levels of Phosphorus in ILSAC GF 4 and Similar Grade Engine Oils by Inductively Coupled Plasma Atomic Emission Spectrometry
    ASTM D 7040 : 2004 : R2010 Standard Test Method for Determination of Low Levels of Phosphorus in ILSAC GF 4 and Similar Grade Engine Oils by Inductively Coupled Plasma Atomic Emission Spectrometry
    ASTM U 00 : 2013 C8 and Lower Boiling Paraffins and Naphthenes in Low-Olefin Hydrocarbons by GC
    ASTM UOP 980 : 2007 C5 and Lower Boiling Dienes, Olefins, and Paraffins in Naphthas by GC
    ASTM UOP 555 : 2010 Trace Impurities in Benzene by GC
    ASTM UOP 621 : 1998 Boiling Point Distribution of Hydrocarbons by Gas Chromatography
    ASTM D 5623 : 1994 : R1999 : EDT 1 Standard Test Method for Sulfur Compounds in Light Petroleum Liquids by Gas Chromatography and Sulfur Selective Detection
    ASTM UOP 976 : 2002 Trace C4-C9 Saturates in High Purity Aromatics by GC
    ASTM D 7754 : 2016 : REDLINE Standard Test Method for Determination of Trace Oxygenates in Automotive Spark-Ignition Engine Fuel by Multidimensional Gas Chromatography
    ASTM D 7920 : 2015 Standard Test Method for Determination of Fuel Methanol (M99) and Methanol Fuel Blends (M10 to M99) by Gas Chromatography
    ASTM D 7776 : 2012 Standard Guide for Self-Assessment of Quality System Practices in Petroleum Products and Lubricant Testing Laboratories (Withdrawn 2017)
    ASTM UOP 931 : 2010 Trace Impurities in Mixed Xylenes by GC
    ASTM D 5441 : 1998 : R2003 : EDT 1 Standard Test Method for Analysis of Methyl Tert-Butyl Ether (MTBE) by Gas Chromatography
    ASTM D 5986 : 1996 : R2011 Standard Test Method for Determination of Oxygenates, Benzene, Toluene, C8-C 12 Aromatics and Total Aromatics in Finished Gasoline by Gas Chromatography/Fourier Transform Infrared Spectroscopy
    ASTM D 6296 : 1998 : R2003 : EDT 1 Standard Test Method for Total Olefins in Spark-Ignition Engine Fuels by Multi-dimensional Gas Chromatography
    ASTM D 7059 : 2009 : R2013 Standard Test Method for Determination of Methanol in Crude Oils by Multidimensional Gas Chromatography
    ASTM D 7806 : 2012 Standard Test Method for Determination of the Fatty Acid Methyl Ester (FAME) Content of a Blend of Biodiesel and Petroleum-Based Diesel Fuel Oil Using Mid-Infrared Spectroscopy
    ASTM UOP 688 : 2009 Normal Olefins and Normal Paraffins by GC
    ASTM D 5442 : 2017 : REDLINE Standard Test Method for Analysis of Petroleum Waxes by Gas Chromatography
    ASTM D 6293 : 1998 Standard Test Method for Oxygenates and Paraffin, Olefin, Naphthene, Aromatic (O-PONA) Hydrocarbon Types in Low-Olefin Spark Ignition Engine Fuels by Gas Chromatography
    ASTM U 09 : 2011 Trace Hydrocarbons in Udex Solvent by GC
    ASTM D 7740 : 201 Standard Practice for Optimization, Calibration, and Validation of Atomic Absorption Spectrometry for Metal Analysis of Petroleum Products and Lubricants
    ASTM D 4626 : 1995 : R2000 Standard Practice for Calculation of Gas Chromatographic Response Factors
    ASTM UOP 551 : 2008 C6 and Lower Boiling Hydrocarbons in Olefin Free Naphthas by GC
    ASTM D 7266 : 2013 : R2018 : EDT 1 Standard Test Method for Analysis of Cyclohexane by Gas Chromatography (External Standard)
    EN 13405 : 2002 SURFACE ACTIVE AGENTS - DETERMINATION OF DIALKYL-TETRALINS CONTENT IN LINEAR ALKYLBENZENE BY HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC)
    ASTM D 4951 : 2014 : REDLINE Standard Test Method for Determination of Additive Elements in Lubricating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry
    ASTM D 5845 : 2001 : R2016 Standard Test Method for Determination of MTBE, ETBE, TAME, DIPE, Methanol, Ethanol and tert-Butanol in Gasoline by Infrared Spectroscopy
    ASTM D 5845 : 2001 : R2011 Standard Test Method for Determination of MTBE, ETBE, TAME, DIPE, Methanol, Ethanol and tert-Butanol in Gasoline by Infrared Spectroscopy
    ASTM UOP 968 : 2000 Foots Oil in Methyl Isobutyl Ketone by GC
    ASTM UOP 720 : 2008 Impurities in, and Purity of, High Purity p-Xylene by GC
    ASTM D 4626 : 1995 : R2005 Standard Practice for Calculation of Gas Chromatographic Response Factors
    ASTM D 5986 : 1996 : R2001 Standard Test Method for Determination of Oxygenates, Benzene, Toluene, C8-C12 Aromatics and Total Aromatics in Finished Gasoline by Gas Chromatography/Fourier Transform Infrared Spectroscopy
    ASTM D 7059 : 2009 : R2017 Standard Test Method for Determination of Methanol in Crude Oils by Multidimensional Gas Chromatography
    ASTM D 7920 : 2015 : EDT 1 Standard Test Method for Determination of Fuel Methanol (M99) and Methanol Fuel Blends (M10 to M99) by Gas Chromatography
    ASTM D 7807 : 2012 Standard Test Method for Determination of Boiling Range Distribution of Hydrocarbon and Sulfur Components of Petroleum Distillates by Gas Chromatography and Chemiluminescence Detection
    ASTM D 6144 : 2017 : REDLINE Standard Test Method for Analysis of AMS (α-Methylstyrene) by Capillary Gas Chromatography
    ASTM D 5501 : 2012 Standard Test Method for Determination of Ethanol and Methanol Content in Fuels Containing Greater than 20% Ethanol by Gas Chromatography
    ASTM D 6277 : 2007 : R2012 Standard Test Method for Determination of Benzene in Spark-Ignition Engine Fuels Using Mid Infrared Spectroscopy
    ASTM D 7040 : 2004 : R2015 Standard Test Method for Determination of Low Levels of Phosphorus in ILSAC GF 4 and Similar Grade Engine Oils by Inductively Coupled Plasma Atomic Emission Spectrometry
    ASTM D 6296 : 1998 : R2013 Standard Test Method for Total Olefins in Spark-ignition Engine Fuels by Multidimensional Gas Chromatography
    ASTM D 7371 : 2014 : REDLINE Standard Test Method for Determination of Biodiesel (Fatty Acid Methyl Esters) Content in Diesel Fuel Oil Using Mid Infrared Spectroscopy (FTIR-ATR-PLS Method)
    ASTM D 5769 : 2015 : REDLINE Standard Test Method for Determination of Benzene, Toluene, and Total Aromatics in Finished Gasolines by Gas Chromatography/Mass Spectrometry
    ASTM UOP 733 : 2010 Residual Triglycerides in Deoxygenated Feedstocks by GC
    ASTM D 5845 : 2001 : R2006 Standard Test Method for Determination of MTBE, ETBE, TAME, DIPE, Methanol, Ethanol and tert-Butanol in Gasoline by Infrared Spectroscopy
    ASTM D 8071 : 2017 Standard Test Method for Determination of Hydrocarbon Group Types and Select Hydrocarbon and Oxygenate Compounds in Automotive Spark-Ignition Engine Fuel Using Gas Chromatography with Vacuum Ultraviolet Absorption Spectroscopy Detection (GC-VUV)
    ASTM D 7691 : 2016 : REDLINE Standard Test Method for Multielement Analysis of Crude Oils Using Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
    ASTM D 7576 : 2016 : REDLINE Standard Test Method for Determination of Benzene and Total Aromatics in Denatured Fuel Ethanol by Gas Chromatography
    ASTM UOP303 : 2007 Impurities in Catalysts by ICP-OES
    ASTM D 6443 : 2014 : REDLINE TEST METHOD FOR DETERMINATION OF CALCIUM, CHLORINE, COPPER, MAGNESIUM, PHOSPHORUS, SULFUR, AND ZINC IN UNUSED LUBRICATING OILS AND ADDITIVES BY WAVELENGTH DISPERSIVE X-RAY FLUORESCENCE SPECTROMETRY (MATHEMATICAL CORRECTION PROCEDURE)
    ASTM U 05 : 2013 Trace Impurities in High Purity Ethyl Benzene by GC
    ASTM D 7740 : 2011 : R2016 Standard Practice for Optimization, Calibration, and Validation of Atomic Absorption Spectrometry for Metal Analysis of Petroleum Products and Lubricants
    ASTM UOP744 : 2006 Aromatics in Hydrocarbons by GC
    ASTM D 7059 : 2009 Standard Test Method for Determination of Methanol in Crude Oils by Multidimensional Gas Chromatography
    ASTM D 5060 : 2012 : REDLINE Standard Test Method for Determining Impurities in High-Purity Ethylbenzene by Gas Chromatography
    ASTM D 7266 : 2013 Standard Test Method for Analysis of Cyclohexane by Gas Chromatography (External Standard)
    ASTM D 5580 : 2015 : REDLINE Standard Test Method for Determination of Benzene, Toluene, Ethylbenzene, p/m-Xylene, o-Xylene, C9 and Heavier Aromatics, and Total Aromatics in Finished Gasoline by Gas Chromatography
    ASTM D 6277 : 2007 Standard Test Method for Determination of Benzene in Spark-Ignition Engine Fuels Using Mid Infrared Spectroscopy
    ASTM D 7861 : 2014 : EDT 1 Standard Test Method for Determination of Fatty Acid Methyl Esters (FAME) in Diesel Fuel by Linear Variable Filter (LVF) Array Based Mid-Infrared Spectroscopy
    ASTM D 7861 : 2014 Standard Test Method for Determination of Fatty Acid Methyl Esters (FAME) in Diesel Fuel by Linear Variable Filter (LVF) Array Based Mid-Infrared Spectroscopy
    ASTM D 5441 : 1998 : R2013 Standard Test Method for Analysis of Methyl Tert-Butyl Ether (MTBE) by Gas Chromatography
    ASTM UOP 863 : 2001 Trace Desorbent in C10-C18 Molex Products by GC
    ASTM UOP 702 : 2009 Impurities in Distilled High Purity Cumene by GC
    ASTM D 5501 : 2012 : R2016 Standard Test Method for Determination of Ethanol and Methanol Content in Fuels Containing Greater than 20% Ethanol by Gas Chromatography
    ASTM UOP 934 : 1994 Diolefins in C5 Olefinic Hydrocarbon Streams by GC (Withdrawn 2011)
    ASTM D 8110 : 2017 Standard Test Method for Elemental Analysis of Distillate Products by Inductively Coupled Plasma Mass Spectrometry (ICP-MS)
    ASTM UOP 543 : 2011 Trace Non-Aromatic Hydrocarbons in High-Purity Aromatics by GC
    ASTM D 5501 : 2012 : EDT 1 Standard Test Method for Determination of Ethanol and Methanol Content in Fuels Containing Greater than 20% Ethanol by Gas Chromatography
    ASTM D 4735 : 2015 : REDLINE TEST METHOD FOR DETERMINATION OF TRACE THIOPHENE IN REFINED BENZENE BY GAS CHROMATOGRAPHY
    ASTM U 00 : 2006 Trace Oxygenated Hydrocarbons in Liquid Hydrocarbon Streams by GC
    ASTM D 6730 : 2001 : R2016 Standard Test Method for Determination of Individual Components in Spark Ignition Engine Fuels by 100–Metre Capillary (with Precolumn) High-Resolution Gas Chromatography
    ASTM D 6839 : 2017-06 TEST METHOD FOR HYDROCARBON TYPES, OXYGENATED COMPOUNDS, AND BENZENE IN SPARK IGNITION ENGINE FUELS BY GAS CHROMATOGRAPHY
    ASTM D 6296 : 1998 : R2008 Standard Test Method for Total Olefins in Spark-ignition Engine Fuels by Multidimensional Gas Chromatography
    ASTM D 7360 : 2016 : REDLINE Standard Test Method for Analysis of Benzene by Gas Chromatography with External Calibration
    ASTM D 4626 : 1995 : R2010 Standard Practice for Calculation of Gas Chromatographic Response Factors
    ASTM D 5623 : 1994 : R2014 Standard Test Method for Sulfur Compounds in Light Petroleum Liquids by Gas Chromatography and Sulfur Selective Detection
    ASTM D 6730 : 2001 : R2006 : EDT 1 Standard Test Method for Determination of Individual Components in Spark Ignition Engine Fuels by 100–Metre Capillary (with Precolumn) High-Resolution Gas Chromatography
    ASTM D 7266 : 2013 : EDT 1 Standard Test Method for Analysis of Cyclohexane by Gas Chromatography (External Standard)
    ASTM D 5441 : 1998 : R2017 Standard Test Method for Analysis of Methyl Tert-Butyl Ether (MTBE) by Gas Chromatography
    ASTM D 8003 : 2015 Standard Test Method for Determination of Light Hydrocarbons and Cut Point Intervals in Live Crude Oils and Condensates by Gas Chromatography
    ASTM UOP 868 : 1988 Trace Saturates in High Purity Aromatics by GC
    BS EN 13405:2002 Surface active agents. Determination of dialkyl-tetralins content in linear alkylbenzene by high performance liquid chromatography (HPLC)
    ASTM D 6293 : 1998 : R2003 : EDT 1 Standard Test Method for Oxygenates and Paraffin, Olefin, Naphthene, Aromatic (O-PONA) Hydrocarbon Types in Low-Olefin Spark Ignition Engine Fuels by Gas Chromatography (Withdrawn 2009)
    ASTM D 4626 : 1995 : R2015 Standard Practice for Calculation of Gas Chromatographic Response Factors
    ASTM D 6730 : 2001 Standard Test Method for Determination of Individual Components in Spark Ignition Engine Fuels by 100-Metre Capillary (with Precolumn) High-Resolution Gas Chromatography
    GOST R 52256 : 2004 ERRATA 2009 GASOLINE - DETERMINATION OF MTBE, ETBE, TAME, DIPE, METHANOL, ETHANOL AND TRET-BUTANOL BY METHOD OF INFRA-RED SPECTROSCOPY
    ASTM D 6730 : 2001 : R2006 Standard Test Method for Determination of Individual Components in Spark Ignition Engine Fuels by 100-Metre Capillary (with Precolumn) High-Resolution Gas Chromatography
    ASTM D 5441 : 1998 : R2008 : EDT 1 Standard Test Method for Analysis of Methyl Tert-Butyl Ether (MTBE) by Gas Chromatography
    ASTM UOP 870 : 1990 Carbon Number Distribution of Paraffins, Naphthenes and Aromatics by GC
    ASTM D 5986 : 1996 : R2006 Standard Test Method for Determination of Oxygenates, Benzene, Toluene, C8-C 12 Aromatics and Total Aromatics in Finished Gasoline by Gas Chromatography/Fourier Transform Infrared Spectroscopy
    ASTM D 5441 : 1998 Standard Test Method for Analysis of Methyl Tert-Butyl Ether (MTBE) by Gas Chromatography
    ASTM D 5845 : 2001 Standard Test Method for Determination of MTBE, ETBE, TAME, DIPE, Methanol, Ethanol and tert-Butanol in Gasoline by Infrared Spectroscopy
    ASTM UOP 725 : 1986 Pentenes and Lower Boiling Hydrocarbons in Olefinic Gasolines by GC (Withdrawn 2013)
    ASTM UOP 537 : 1991 Alcohol and Ketone Mixtures by GC
    ASTM D 7974 : 2015 Standard Test Method for Determination of Farnesane, Saturated Hydrocarbons, and Hexahydrofarnesol Content of Synthesized Iso-Paraffins (SIP) Fuel for Blending with Jet Fuel by Gas Chromatography
    ASTM D 5986 : 1996 : R2015 Standard Test Method for Determination of Oxygenates, Benzene, Toluene, C8–C 12 Aromatics and Total Aromatics in Finished Gasoline by Gas Chromatography/Fourier Transform Infrared Spectroscopy
    ASTM UOP 732 : 2009 Analysis of Distillate Fuels Derived from Oxygenated (Bio) Feedstocks by GC
    ASTM D 6584 : 2017 : REDLINE Standard Test Method for Determination of Total Monoglycerides, Total Diglycerides, Total Triglycerides, and Free and Total Glycerin in B-100 Biodiesel Methyl Esters by Gas Chromatography
    ASTM D 7796 : 2017 : REDLINE Standard Test Method for Analysis of Ethyl tert-Butyl Ether (ETBE) by Gas Chromatography
    ASTM D 4420 : 1994 Standard Test Method for Determination of Aromatics in Finished Gasoline by Gas Chromatography)
    ASTM D 3797 : 2005 Standard Test Method for Analysis of o-Xylene by Gas Chromatography (Withdrawn 2014)
    ASTM D 7845 : 2017 : REDLINE Standard Test Method for Determination of Chemical Species in Marine Fuel Oil by Multidimensional Gas Chromatography/Mass Spectrometry
    ASTM D 7057 : 2018 : REDLINE Standard Test Method for Analysis of Isopropylbenzene (Cumene) by Gas Chromatography (External Standard)
    ASTM D 5986 : 1996 Standard Test Method for Determination of Oxygenates, Benzene, Toluene, C8-C12 Aromatics and Total Aromatics in Finished Gasoline by Gas Chromatography/Fourier Transform Infrared Spectroscopy
    ASTM D 6730 : 2001 : R2011 Standard Test Method for Determination of Individual Components in Spark Ignition Engine Fuels by 100–Metre Capillary (with Precolumn) High-Resolution Gas Chromatography
    ASTM D 5623 : 1994 : R2004 : EDT 1 Standard Test Method for Sulfur Compounds in Light Petroleum Liquids by Gas Chromatography and Sulfur Selective Detection
    ASTM UOP 799 : 2008 Chloride in Liquid Hydrocarbons by Dry Colorimetry
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