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ASTM D 4310 : 2020 : REV A

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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Standard Test Method for Determination of Sludging and Corrosion Tendencies of Inhibited Mineral Oils

Available format(s)

Hardcopy , PDF

Superseded date

14-07-2022

Superseded by

ASTM D 4310 : 2022

Language(s)

English

Published date

15-07-2020

€74.48
Excluding VAT

Committee
D 02
DocumentType
Test Method
Pages
13
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1This test method covers and is used to evaluate the tendency of inhibited mineral oil based steam turbine lubricants and mineral oil based anti-wear hydraulic oils to corrode copper catalyst metal and to form sludge during oxidation in the presence of oxygen, water, and copper and iron metals at an elevated temperature. The test method is also used for testing circulating oils having a specific gravity less than that of water and containing rust and oxidation inhibitors.

Note 1:During round robin testing copper and iron in the oil, water and sludge phases were measured. However, the values for the total iron were found to be so low (that is, below 0.8 mg), that statistical analysis was inappropriate. The results of the cooperative test program are available (see Section 16).

1.2This test method is a modification of Test Method D943 where the oxidation stability of the same kinds of oils is determined by following the acid number of oil. The number of test hours required for the oil to reach an acid number of 2.0 mg KOH/g is the oxidation lifetime.

1.3Procedure A of this test method requires the determination and report of the weight of the sludge and the total amount of copper in the oil, water, and sludge phases. Procedure B requires the sludge determination only. The acid number determination is optional for both procedures.

1.4The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5WARNING—Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use Caution when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location.

1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Section 7 and X1.1.5.

1.7This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D 4304 : 2017 Standard Specification for Mineral and Synthetic Lubricating Oil Used in Steam or Gas Turbines
ASTM D 7873 : 2020 Standard Test Method for Determination of Oxidation Stability and Insolubles Formation of Inhibited Turbine Oils at 120 °C Without the Inclusion of Water (Dry TOST Method)
ASTM D 8029 : 2018 Standard Specification for Biodegradable, Low Aquatic Toxicity Hydraulic Fluids
ASTM D 8324 : 2021 Standard Guide for Selection of Environmentally Acceptable Lubricants for the U.S. Environmental Protection Agency (EPA) Vessel General Permit
ASTM D 943 : 2020 Standard Test Method for Oxidation Characteristics of Inhibited Mineral Oils
ASTM D 6158 : 2018 Standard Specification for Mineral Hydraulic Oils
ASTM D 7155 : 2020 Standard Practice for Evaluating Compatibility of Mixtures of Turbine Lubricating Oils

ASTM D 4057 : 2019 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 3339 : 1995 : EDT 2 Standard Test Method for Acid Number of Petroleum Products by Semi-Micro Color Indicator Titration
ASTM B 1 : 1995 Standard Specification for Hard-Drawn Copper Wire
ASTM D 3339 : 2012 : R2017 Standard Test Method for Acid Number of Petroleum Products by Semi-Micro Color Indicator Titration
ASTM D 664 : 1995 Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
ASTM D 943 : 2018 Standard Test Method for Oxidation Characteristics of Inhibited Mineral Oils
ASTM D 4057 : 2022 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 943 : 1999 Standard Test Method for Oxidation Characteristics of Inhibited Mineral Oils
ASTM D 3339 : 2021 Standard Test Method for Acid Number of Petroleum Products by Semi-Micro Color Indicator Titration

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