ASTM D 4547 : 2020

1.1This guide describes recommended procedures for the collection, handling, and preparation of solid waste, soil, and sediment samples for subsequent determination of volatile organic compounds (VOCs). This class of compounds includes low molecular weight aromatics, hydrocarbons, halogenated hydrocarbons, ketones, acetates, nitriles, acrylates, ethers, and sulfides with boiling points below 200° Celsius (C) that are insoluble or slightly soluble in water.

1.2Methods of sample collection, handling, storage, and preparation for analysis are described.

1.3This guide does not cover the details of sampling design, laboratory preparation of containers, and the analysis of the samples.

1.4It is recommended that this guide be used in conjunction with Guide D4687.

1.5This guide offers an organized collection of information or a series of options and does not recommend a specific course of action. This document cannot replace education or experience and should be used in conjunction with professional judgment. Not all aspects of this guide may be applicable in all circumstances. This ASTM standard is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a project’s many unique aspects. The word “standard” in the title of this document means only that the document has been approved through the ASTM consensus process.

1.6The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. Reporting of test results in units other than SI shall not be regarded as nonconformance with this standard.

1.7This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.8This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.