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  • ASTM D 4821 : 2016

    View superseded by
    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
    View superseded by

    Standard Guide for Carbon Black—Validation of Test Method Precision and Bias

    Available format(s):  Hardcopy, PDF

    Superseded date:  16-09-2019

    Language(s):  English

    Published date:  15-08-2016

    Publisher:  American Society for Testing and Materials

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    1.1This guide covers procedures for using the ASTM Standard Reference Blacks2 (SRBs) and the HT and INR Iodine Number Standards to continuously monitor the precision of those carbon black test methods for which reference values have been established. It also offers guidelines for troubleshooting various test methods.

    1.2This guide defines the environmental conditions that are required for laboratories that perform carbon black testing activities for those test methods under D24’s jurisdiction.

    1.3This guide establishes procedures for the use of x-charts to continuously monitor those tests listed in Section 2 for within-lab precision (repeatability) and between-lab accuracy (reproducibility).

    1.4This guide provides a statistical procedure for improving test reproducibility when a laboratory cannot physically calibrate its apparatus to obtain the reference values of the ASTM reference blacks, within the ranges given in this guide.

    General Product Information - (Show below) - (Hide below)

    Committee D 24
    Document Type Guide
    Publisher American Society for Testing and Materials
    Status Superseded
    Superseded By
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM D 2414 : 2018 : REV A Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
    ASTM D 8043 : 2016 Standard Guide for Carbon Black—Shelf Life
    ASTM D 1510 : 2019 Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM D 3493 : 2018 : REV A Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample (COAN)
    ASTM D 3265 : 2019 Standard Test Method for Carbon Black—Tint Strength
    ASTM D 6915 : 2017 : EDT 1 Standard Practice for Carbon Black—Evaluation of Standard Reference Blacks

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM D 3493 : 2001 Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample
    ASTM E 2586 : 2012 Standard Practice for Calculating and Using Basic Statistics
    ASTM D 2414 : 2008 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
    ASTM D 3493 : 2009 Standard Test Method for Carbon Black-Oil Absorption Number of Compressed Sample (COAN)
    ASTM D 3493 : 2006 : EDT 1 Standard Test Method for Carbon Black-Oil Absorption Number of Compressed Sample (COAN)
    ASTM D 2414 : 2008 : REV A Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
    ASTM D 1765 : 2005 : REV A : EDT 1 Standard Classification System for Carbon Blacks Used in Rubber Products
    ASTM D 3493 : 2006 Standard Test Method for Carbon Black-Oil Absorption Number of Compressed Sample (COAN)
    ASTM D 1513 : 2004 Standard Test Method for Carbon Black, Pelleted—Pour Density
    ASTM D 3265 : 2011 Standard Test Method for Carbon Black-Tint Strength
    ASTM D 3493 : 2004 Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample (COAN)
    ASTM D 1765 : 2003 Standard Classification System for Carbon Blacks Used in Rubber Products
    ASTM D 2414 : 2000 : REV A Standard Test Method for Carbon Black—Oil Absorption Number
    ASTM D 1510 : 2007 Standard Test Method for Carbon Black-Iodine Adsorption Number
    ASTM D 1510 : 2019 Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM D 2414 : 2003 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
    ASTM D 1765 : 2004 : EDT 1 Standard Classification System for Carbon Blacks Used in Rubber Products
    ASTM D 2414 : 2016 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
    ASTM D 1510 : 2008 : REV B Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM D 6556 : 2009 Standard Test Method for Carbon Black-Total and External Surface Area by Nitrogen Adsorption
    ASTM D 1765 : 2017 Standard Classification System for Carbon Blacks Used in Rubber Products
    ASTM D 3265 : 2017 : EDT 1 Standard Test Method for Carbon Black—Tint Strength
    ASTM D 2414 : 2006 : REV A Standard Test Method for Carbon Black-Oil Absorption Number (OAN)
    ASTM D 6556 : 2007 Standard Test Method for Carbon Black-Total and External Surface Area by Nitrogen Adsorption
    ASTM D 3493 : 2003 Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample
    ASTM D 2414 : 2013 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
    ASTM D 1510 : 2011 Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM D 6556 : 2002 : REV A Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption
    ASTM D 3265 : 2015 : REV A Standard Test Method for Carbon Black—Tint Strength
    ASTM D 1510 : 2008 Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM D 1510 : 2016 : REV A Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM D 1765 : 2014 Standard Classification System for Carbon Blacks Used in Rubber Products
    ASTM D 6556 : 2003 Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption
    ASTM D 1765 : 2000 : REV A Standard Classification System for Carbon Blacks Used in Rubber Products
    ASTM D 2414 : 2011 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
    ASTM E 2586 : 2014 Standard Practice for Calculating and Using Basic Statistics
    ASTM D 1510 : 2003 Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM D 2414 : 2005 : REV A Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
    ASTM D 3493 : 2007 Standard Test Method for Carbon Black-Oil Absorption Number of Compressed Sample (COAN)
    ASTM D 3493 : 2014 Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample (COAN)
    ASTM D 1513 : 2005 : EDT 1 Standard Test Method for Carbon Black, Pelleted—Pour Density
    ASTM D 3265 : 2015 Standard Test Method for Carbon Black—Tint Strength
    ASTM D 2414 : 2005 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
    ASTM D 3265 : 2003 Standard Test Method for Carbon Black—Tint Strength
    ASTM D 1510 : 2017 Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM D 6556 : 2019 Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption
    ASTM D 1765 : 2018 Standard Classification System for Carbon Blacks Used in Rubber Products
    ASTM D 3493 : 2000 : REV A Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample
    ASTM D 1765 : 2001 : EDT 1 Standard Classification System for Carbon Blacks Used in Rubber Products
    ASTM D 2414 : 2012 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
    ASTM D 3265 : 2006 Standard Test Method for Carbon Black-Tint Strength
    ASTM D 1765 : 2004 : REV A Standard Classification System for Carbon Blacks Used in Rubber Products
    ASTM E 2586 : 2010 : REV A Standard Practice for Calculating and Using Basic Statistics
    ASTM D 3265 : 2013 : REV A Standard Test Method for Carbon Black—Tint Strength
    ASTM D 3265 : 2005 Standard Test Method for Carbon Black—Tint Strength
    ASTM D 1513 : 2005 : R2012 Standard Test Method for Carbon Black, Pelleted—Pour Density
    ASTM E 2282 : 2013 Standard Guide for Defining the Test Result of a Test Method
    ASTM D 1510 : 2005 : REV A Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM E 2586 : 2019 Standard Practice for Calculating and Using Basic Statistics
    ASTM D 1765 : 2001 Standard Classification System for Carbon Blacks Used in Rubber Products
    ASTM D 3265 : 2007 Standard Test Method for Carbon Black-Tint Strength
    ASTM D 1510 : 2013 Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM D 1765 : 2016 Standard Classification System for Carbon Blacks Used in Rubber Products
    ASTM D 3493 : 2016 Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample (COAN)
    ASTM D 2414 : 2002 Standard Test Method for Carbon Black—Oil Absorption Number
    ASTM D 2414 : 2016 : EDT 1 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
    ASTM D 3493 : 2018 Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample (COAN)
    ASTM D 6556 : 2002 Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption
    ASTM E 2586 : 2012 : REV A Standard Practice for Calculating and Using Basic Statistics
    ASTM D 6556 : 2017 Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption
    ASTM D 1510 : 1999 Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM D 1765 : 2005 : REV A Standard Classification System for Carbon Blacks Used in Rubber Products
    ASTM D 1765 : 2013 Standard Classification System for Carbon Blacks Used in Rubber Products
    ASTM D 1513 : 2005 : EDT 2 Standard Test Method for Carbon Black, Pelleted—Pour Density
    ASTM D 2414 : 2009 : REV A Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
    ASTM D 1510 : 2009 Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM D 1510 : 2012 Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM E 2282 : 2003 Standard Guide for Defining the Test Result of a Test Method
    ASTM D 1513 : 1999 : REV A : EDT 1 Standard Test Method for Carbon Black, Pelleted-Pour Density
    ASTM E 2586 : 2007 Standard Practice for Calculating and Using Basic Statistics
    ASTM D 3493 : 2004 : REV A Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample (COAN)
    ASTM D 2414 : 2006 Standard Test Method for Carbon Black-Oil Absorption Number (OAN)
    ASTM D 3265 : 2017 Standard Test Method for Carbon Black—Tint Strength
    ASTM E 2586 : 2016 Standard Practice for Calculating and Using Basic Statistics
    ASTM D 1765 : 2006 Standard Classification System for Carbon Blacks Used in Rubber Products
    ASTM D 1510 : 2008 : REV C Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM D 1510 : 2007 : REV A Standard Test Method for Carbon Black-Iodine Adsorption Number
    ASTM D 2414 : 2018 : REV A Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
    ASTM D 2414 : 2017 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
    ASTM E 2586 : 2018 Standard Practice for Calculating and Using Basic Statistics
    ASTM D 3265 : 2013 Standard Test Method for Carbon Black—Tint Strength
    ASTM D 2414 : 2014 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
    ASTM D 2414 : 2006 : REV A : EDT 1 Standard Test Method for Carbon Black-Oil Absorption Number (OAN)
    ASTM D 6556 : 2001 Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption
    ASTM D 6556 : 2000 : REV A Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption
    ASTM D 2414 : 2002 : REV A Standard Test Method for Carbon Black—Oil Absorption Number
    ASTM D 6556 : 2014 Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption
    ASTM E 2586 : 2012 : REV B Standard Practice for Calculating and Using Basic Statistics
    ASTM D 6556 : 2001 : REV A Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption
    ASTM D 1510 : 2006 : REV A Standard Test Method for Carbon Black-Iodine Adsorption Number
    ASTM D 2414 : 2001 Standard Test Method for Carbon Black—Oil Absorption Number
    ASTM E 2282 : 2014 Standard Guide for Defining the Test Result of a Test Method
    ASTM D 1510 : 2002 : REV A Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM D 3324 : 2001 Standard Practice for Carbon Black—Improving Test Reproducibility Using ASTM Standard Reference Blacks
    ASTM D 3493 : 2018 : REV A Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample (COAN)
    ASTM D 1510 : 2006 Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM D 3493 : 2013 Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample (COAN)
    ASTM D 2414 : 2004 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
    ASTM D 3265 : 2002 Standard Test Method for Carbon Black—Tint Strength
    ASTM D 1510 : 2016 Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM D 1765 : 2010 Standard Classification System for Carbon Blacks Used in Rubber Products
    ASTM D 1510 : 2005 Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM E 2586 : 2010 Standard Practice for Calculating and Using Basic Statistics
    ASTM D 1510 : 2010 Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM D 1765 : 2004 Standard Classification System for Carbon Blacks Used in Rubber Products
    ASTM D 1513 : 2005 : R2017 Standard Test Method for Carbon Black, Pelleted—Pour Density
    ASTM D 6556 : 2004 Standard Test Method for Carbon Black-Total and External Surface Area by Nitrogen Adsorption
    ASTM D 1510 : 2001 : REV A Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM D 1510 : 2002 Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM E 2282 : 2009 Standard Guide for Defining the Test Result of a Test Method
    ASTM D 3324 : 1999 Standard Practice for Carbon Black—Improving Test Reproducibility Using ASTM Standard Reference Blacks
    ASTM D 2414 : 2018 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
    ASTM D 1513 : 1999 : REV A : R2004 Standard Test Method for Carbon Black, Pelleted—Pour Density
    ASTM D 6556 : 2016 Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption
    ASTM D 1510 : 2009 : REV B Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM D 3265 : 2019 Standard Test Method for Carbon Black—Tint Strength
    ASTM D 3265 : 2001 Standard Test Method for Carbon Black—Tint Strength
    ASTM E 2586 : 2013 Standard Practice for Calculating and Using Basic Statistics
    ASTM D 1510 : 2011 : REV A Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM D 1510 : 2008 : REV A Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM D 1510 : 2009 : REV A Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM D 2414 : 2009 Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
    ASTM D 3265 : 2014 Standard Test Method for Carbon Black—Tint Strength
    ASTM D 3265 : 2000 Standard Test Method for Carbon Black—Tint Strength
    ASTM D 2414 : 2013 : REV A Standard Test Method for Carbon Black—Oil Absorption Number (OAN)
    ASTM D 1510 : 2001 Standard Test Method for Carbon Black—Iodine Adsorption Number
    ASTM D 3265 : 2017 : REV A Standard Test Method for Carbon Black—Tint Strength
    ASTM D 1765 : 2005 Standard Classification System for Carbon Blacks Used in Rubber Products
    ASTM D 1513 : 2005 Standard Test Method for Carbon Black, Pelleted—Pour Density
    ASTM D 6556 : 2010 Standard Test Method for Carbon Black-Total and External Surface Area by Nitrogen Adsorption
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