ASTM D 4821 : 2020
Current
The latest, up-to-date edition.
Standard Guide for Carbon Black—Validation of Test Method Precision and Bias
Hardcopy , PDF
English
26-11-2020
Committee |
D 24
|
DocumentType |
Guide
|
Pages |
14
|
PublisherName |
American Society for Testing and Materials
|
Status |
Current
|
Supersedes |
1.1This guide covers procedures for using the ASTM Standard Reference Blacks2 (SRBs) and the HT and INR Iodine Number Standards to continuously monitor the precision of those carbon black test methods for which reference values have been established. It also offers guidelines for troubleshooting various test methods.
1.2This guide defines the environmental conditions that are required for laboratories that perform carbon black testing activities for those test methods under D24’s jurisdiction.
1.3This guide establishes procedures for the use of x-charts to continuously monitor those tests listed in Section 2 for within-lab precision (repeatability) and between-lab accuracy (reproducibility).
1.4This guide provides a statistical procedure for improving test reproducibility when a laboratory cannot physically calibrate its apparatus to obtain the reference values of the ASTM reference blacks, within the ranges given in this guide.
1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
ASTM E 177 : 1990 : REV A : R1996 | Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods |
ASTM D 3324 : 2001 : REV A | Standard Practice for Carbon Black—Improving Test Reproducibility Using ASTM Standard Reference Blacks (Withdrawn 2002) |
ASTM D 2414 : 2022 | Standard Test Method for Carbon Black—Oil Absorption Number (OAN) |
ASTM E 2586 : 2019 : R2024 | Standard Practice for Calculating and Using Basic Statistics |
ASTM D 3493 : 2020 | Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample (COAN) |
ASTM D 3493 : 2021 | Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample (COAN) |
ASTM D 3265 : 2024 : REV A | Standard Test Method for Carbon Black—Tint Strength |
ASTM D 1765 : 2023 : REV A | Standard Classification System for Carbon Blacks Used in Rubber Products |
ASTM D 1510 : 2019 : REV A | Standard Test Method for Carbon Black—Iodine Adsorption Number |
ASTM D 2414 : 2023 | Standard Test Method for Carbon Black—Oil Absorption Number (OAN) |
ASTM D 1510 : 2024 | Standard Test Method for Carbon Black—Iodine Adsorption Number |
ASTM D 3265 : 2023 | Standard Test Method for Carbon Black—Tint Strength |
ASTM D 1510 : 2024 : REV A | Standard Test Method for Carbon Black—Iodine Adsorption Number |
ASTM D 1765 : 2019 | Standard Classification System for Carbon Blacks Used in Rubber Products |
ASTM D 2414 : 2019 | Standard Test Method for Carbon Black—Oil Absorption Number (OAN) |
ASTM E 2282 : 2023 | Standard Guide for Defining the Test Result of a Test Method |
ASTM D 1765 : 2001 | Standard Classification System for Carbon Blacks Used in Rubber Products |
ASTM D 3265 : 2024 | Standard Test Method for Carbon Black—Tint Strength |
ASTM E 2282 : 2014 : R2019 | Standard Guide for Defining the Test Result of a Test Method |
ASTM D 3265 : 2019 : REV B | Standard Test Method for Carbon Black—Tint Strength |
ASTM D 7854 : 2018 : REV C : EDT 1 | Standard Test Method for Carbon Black-Void Volume at Mean Pressure |
ASTM E 2282 : 2014 : R2023 | Standard Guide for Defining the Test Result of a Test Method |
ASTM E 2586 : 2019 : EDT 1 | Standard Practice for Calculating and Using Basic Statistics |
ASTM D 1510 : 2021 | Standard Test Method for Carbon Black—Iodine Adsorption Number |
ASTM D 3265 : 2021 | Standard Test Method for Carbon Black—Tint Strength |
ASTM D 3265 : 2023 : REV A | Standard Test Method for Carbon Black—Tint Strength |
ASTM D 2414 : 2001 | Standard Test Method for Carbon Black—Oil Absorption Number |
ASTM D 6556 : 2019 : REV A | Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption |
ASTM D 1765 : 2021 | Standard Classification System for Carbon Blacks Used in Rubber Products |
ASTM D 6556 : 2021 | Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption |
ASTM D 2414 : 2023 : REV A | Standard Test Method for Carbon Black—Oil Absorption Number (OAN) |
ASTM D 1513 : 2005 : R2017 | Standard Test Method for Carbon Black, Pelleted—Pour Density |
ASTM D 1765 : 2023 : REV B | Standard Classification System for Carbon Blacks Used in Rubber Products |
ASTM D 1765 : 2023 | Standard Classification System for Carbon Blacks Used in Rubber Products |
ASTM D 1513 : 2005 : R2023 | Standard Test Method for Carbon Black, Pelleted—Pour Density |
ASTM D 2414 : 2021 | Standard Test Method for Carbon Black—Oil Absorption Number (OAN) |
ASTM D 1510 : 2024 : REV B | Standard Test Method for Carbon Black—Iodine Adsorption Number |
ASTM D 7854 : 2021 | Standard Test Method for Carbon Black-Void Volume at Mean Pressure |
ASTM D 1510 : 2023 | Standard Test Method for Carbon Black—Iodine Adsorption Number |
ASTM D 1510 : 2023 : REV A | Standard Test Method for Carbon Black—Iodine Adsorption Number |
ASTM D 1765 : 2022 | Standard Classification System for Carbon Blacks Used in Rubber Products |
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