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ASTM D 5236 : 2018 : REV A

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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Standard Test Method for Distillation of Heavy Hydrocarbon Mixtures (Vacuum Potstill Method)

Available format(s)

Hardcopy , PDF

Superseded date

22-11-2023

Superseded by

ASTM D 5236 : 2023

Language(s)

English

Published date

24-07-2018

€74.48
Excluding VAT

Committee
D 02
DocumentType
Test Method
Pages
18
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1This test method covers the procedure for distillation of heavy hydrocarbon mixtures having initial boiling points greater than 150 °C (300 °F), such as heavy crude oils, petroleum distillates, residues, and synthetic mixtures. It employs a potstill with a low pressure drop entrainment separator operated under total takeoff conditions. Distillation conditions and equipment performance criteria are specified and typical apparatus is illustrated.

1.2This test method details the procedures for the production of distillate fractions of standardized quality in the gas oil and lubricating oil range as well as the production of standard residue. In addition, it provides for the determination of standard distillation curves to the highest atmospheric equivalent temperature possible by conventional distillation.

1.3The maximum achievable atmospheric equivalent temperature (AET) is dependent upon the heat tolerance of the charge. For most samples, a temperature up to 565 °C (1050 °F) can be attained. This maximum will be significantly lower for heat sensitive samples (for example, heavy residues) and might be somewhat higher for nonheat sensitive samples.

1.4The recommended distillation method for crude oils up to cutpoint 400 °C (752 °F) AET is Test Method D2892. This test method can be used for heavy crude oils with initial boiling points greater than 150 °C (302 °F). However, distillation curves and fraction qualities obtained by these methods are not comparable.

1.5This test method contains the following annexes:

1.5.1Annex A1Test Method for Determination of Temperature Response Time,

1.5.2Annex A2Practice for Calibration of Sensors,

1.5.3Annex A3Test Method for Dehydration of a Wet Sample of Oil,

1.5.4Annex A4Practice for Conversion of Observed Vapor Temperature to Atmospheric Equivalent Temperature (AET), and

1.5.5Annex A5Test Method for Determination of Wettage.

1.6The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.

1.7This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warnings, see 6.5.4.2, 6.5.6.3, 6.9.3, 9.5, 9.7, and A2.3.1.3.

1.8WARNING—Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use Caution when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location.

1.9This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D 1250 : 1980 : R1997 : EDT 1 Standard Guide for Petroleum Measurement Tables
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ASTM D 4177 : 2020 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 1298 : 1985 : R1990 : EDT 1 Standard Practice for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
ASTM D 4177 : 2022 : EDT 1 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D 5002 : 2022 Standard Test Method for Density, Relative Density, and API Gravity of Crude Oils by Digital Density Analyzer
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ASTM D 5002 : 1999 Standard Test Method for Density and Relative Density of Crude Oils by Digital Density Analyzer

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