ASTM D 5394 : 2002 : R2012
Withdrawn
A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.
Standard Specification for Reclaimed 1,1,1-Trichloroethane (Withdrawn 2017)
Hardcopy , PDF
08-12-2017
English
01-03-2012
Important note : Users cannot be edited or removed once added to your Multi user PDF.CONTAINED IN VOL. 15.05, 2015 Provides definition for Type I (high quality reclaimed 1,1,1 trichloroethane, approximating MIL Specification), Type II (good quality reclaimed solvent), Type III (minimal acceptable reclaimed solvent).
| Committee |
D 26
|
| DocumentType |
Standard
|
| Pages |
2
|
| ProductNote |
Reconfirmed 2012
|
| PublisherName |
American Society for Testing and Materials
|
| Status |
Withdrawn
|
| Supersedes |
1.1 This specification defines Type I (high quality reclaimed 1,1,1-trichloroethane, approximating MIL Specification), Type II (good quality reclaimed solvent), Type III (minimal acceptable reclaimed solvent).
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For a specific hazards statement see Section 4.
1.3 1,1,1-trichloroethane also is known commercially as methyl chloroform.
TABLE 1 Properties, Type I
| Property | Specification | Test Method |
|---|---|---|
| Appearance | Free of turbidity and suspended matter | D3741 |
| 1,1,1-trichloroethane, weight %, min | 92 | D6806 |
| Nonvolatile residue, weight %, max | 0.0040 | D2109 |
| Color, Pt-Co, max | 25 | D2108 |
| Water, weight %, max | 0.015 | D3401 |
| Acid acceptance as NaOH, weight %, min | 0.20 | D2942 |
| Aluminum scratch test | PassesA | D2943 |
| Acidity as HCl, weight %, max | 0.001 | D2989 |
| Alkalinity as NaOH, weight %, max | 0.020 | D2106 |
| Halide as Cl, weight %, max | 0.0005 | D2988 |
A Distill 100 mL solvent, collect 50 mL distillate, and conduct scratch test on distillate and portion remaining in distillation flask.
TABLE 2 Properties, Type II
| Property | Specification | Test Method |
|---|---|---|
| Appearance | Free of turbidity and suspended matter | D3741 |
| 1,1,1-trichloroethane, weight %, min | 90 | D6806 |
| Nonvolatile residue (NVR), weight %, max | 0.010 | D2109 |
| Color, Pt-Co, max | 30 | D2108 |
| Water, weight %, max | 0.015 | D3401 |
| Acid acceptance as NaOH, weight %, min | 0.20 | D2942 |
| Aluminum scratch test | PassesA | D2943 |
| Acidity as HCl, weight %, max | 0.001 | D2989 |
| Alkalinity as NaOH, weight %, max | 0.020 | D2106 |
| Halide as Cl, weight %, max | 0.0005 | D2988 |
A Distill 100 mL solvent, collect 50 mL distillate, and conduct scratch test on distillate and portion remaining in distillation flask.
TABLE 3 Properties, Type IIIA
| Property | Specification | Test Method |
|---|---|---|
| Appearance | Free of turbidity and suspended matter | D3741 |
| 1,1,1-trichloroethane, weight %, min | 88 | D6806 |
| Nonvolatile residue, weight %, max | 0.020 | D2109 |
| Color, Pt-Co, max | 50 | D2108 |
| Water, weight %, max | 0.020 | D3401 |
| Acid acceptance as NaOH, weight %, min | 0.20 | D2942 |
| Aluminum scratch test | PassesB | D2943 |
| Acidity as HCl, weight %, max | 0.002 | D2989 |
| Alkalinity as NaOH, weight %, max | 0.020 | D2106 |
A Type III reclaimed 1,1,1-trichloroethane is not recommended for use in precision cleaning or vapor degreasing applications.
B Distill 100 mL solvent, collect 50 mL distillate, and conduct scratch test on distillate and portion remaining in distillation flask.
| ASTM D 3742 : 1998 | Standard Test Method for 1,1,1-Trichloroethane Content (Withdrawn 2003) |
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