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ASTM D 5863 : 2000 : REV A : R2005

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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Standard Test Methods for Determination of Nickel, Vanadium, Iron, and Sodium in Crude Oils and Residual Fuels by Flame Atomic Absorption Spectrometry

Available format(s)

Hardcopy , PDF

Superseded date

11-11-2014

Language(s)

English

Published date

01-05-2005

€67.30
Excluding VAT

CONTAINED IN VOL. 05.03, 2016 Defines the determination of nickel, vanadium, iron and sodium in crude oils and residual fuels by flame atomic absorption spectrometry (AAS).

Committee
D 02
DocumentType
Test Method
Pages
7
ProductNote
Reconfirmed 2005
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1 These test methods cover the determination of nickel, vanadium, iron, and sodium in crude oils and residual fuels by flame atomic absorption spectrometry (AAS). Two different test methods are presented.

1.2 Test Method A, Sections -Flame AAS is used to analyze a sample that is decomposed with acid for the determination of total Ni, V, and Fe.

1.3 Test Method B, Sections -Flame AAS is used to analyze a sample diluted with an organic solvent for the determination of Ni, V, and Na. This test method uses oil-soluble metals for calibration to determine dissolved metals and does not purport to quantitatively determine nor detect insoluble particulates. Hence, this test method may underestimate the metal content, especially sodium, present as inorganic sodium salts.

1.4 The concentration ranges covered by these test methods are determined by the sensitivity of the instruments, the amount of sample taken for analysis, and the dilution volume. A specific statement is given in Note 0.

1.5 For each element, each test method has its own unique precision. The user can select the appropriate test method based on the precision required for the specific analysis.

1.6 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given in 7.1, 8.2, 8.5, 10 2, 10.4, and 15.1 .

ASTM D 7740 : 2011 : R2016 Standard Practice for Optimization, Calibration, and Validation of Atomic Absorption Spectrometry for Metal Analysis of Petroleum Products and Lubricants
ASTM D 7578 : 2018 Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants
ASTM D 8056 : 2018 Standard Guide for Elemental Analysis of Crude Oil
ASTM D 4057 : 2012 : R2018 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 7455 : 2019 Standard Practice for Sample Preparation of Petroleum and Lubricant Products for Elemental Analysis

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