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ASTM D 6259 : 2023

Current

Current

The latest, up-to-date edition.

Standard Practice for Determination of a Pooled Limit of Quantitation for a Test Method

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

09-05-2023

1.1This practice covers the use of standard regression techniques and data from an interlaboratory study to determine a lower quantitative limit for a test method. This determined lower limit represents the numerical limit at or above which the test results are considered to be quantitatively meaningful for commerce or regulatory activities by this practice. It is defined by this standard as the pooled limit of quantitation (PLOQ) for the test method.

1.2This practice is applicable to test methods that are capable of producing numerical test results close to zero. Examples are those test methods that determine quantitatively the concentration of analyte(s) near zero.

1.3This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Committee
D 02
DocumentType
Standard Practice
Pages
4
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

ASTM D 4294 : 2021 Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry
ASTM D 8056 : 2018 Standard Guide for Elemental Analysis of Crude Oil
ASTM D 8146 : 2022 Standard Guide for Evaluating Test Method Capability and Fitness for Use
ASTM D 8252 : 2019 : EDT 1 Standard Test Method for Vanadium and Nickel in Crude and Residual Oil by X-ray Spectrometry
ASTM D 7372 : 2021 Standard Guide for Analysis and Interpretation of Proficiency Test Program Results
ASTM D 2622 : 2021 Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry
ASTM D 7039 : 2015 : REV A : R2020 Standard Test Method for Sulfur in Gasoline, Diesel Fuel, Jet Fuel, Kerosine, Biodiesel, Biodiesel Blends, and Gasoline-Ethanol Blends by Monochromatic Wavelength Dispersive X-ray Fluorescence Spectrometry

ASTM E 456 : 2013 : REV A : R2022 Standard Terminology Relating to Quality and Statistics
ASTM E 456 : 2013 : REV A : R2022 : EDT 1 Standard Terminology Relating to Quality and Statistics
ASTM D 6300 : 2021 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 6300 : 2023 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 6300 : 2023 : REV A Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 6300 : 2024 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants

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