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ASTM D 6331 : 2016

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by

Standard Test Method for Determination of Mass Concentration of Particulate Matter from Stationary Sources at Low Concentrations (Manual Gravimetric Method)

Available format(s)

Hardcopy , PDF

Superseded date

12-11-2024

Superseded by

ASTM D 6331 : 2024

Language(s)

English

Published date

01-10-2016

€74.48
Excluding VAT

Committee
D 22
DocumentType
Test Method
Pages
15
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1This test method2 covers a method for the measurement of particulate matter (dust) concentration in emission gases in the concentrations below 20 mg/m3 standard conditions, with special emphasis around 5 mg/m3.

1.2To meet the requirements of this test method, the particulate sample is weighed to a specified level of accuracy. At low dust concentrations, this is achieved by:

1.2.1Precise and repeatable weighing procedures,

1.2.2Using low tare weight weighing dishes,

1.2.3Extending the sampling time at conventional sampling rates, or

1.2.4Sampling at higher rates at conventional sampling times (high-volume sampling).

1.3This test method differs from Test Method D3685/D3685M by requiring the mass measurement of filter blanks, specifying weighing procedures, and requiring monitoring of the flue gas flow variability over the testing period. It requires that the particulate matter collected on the sample filter have a mass at least five times a positive mass difference on the filter blank. High volume sampling techniques or an extension of the sampling time may be employed to satisfy this requirement. This test method has tightened requirements on sampling temperature fluctuations and isokinetic sampling deviation. This test method has eliminated the in-stack filtration technique.

1.4This test method may be used for calibration of automated monitoring systems (AMS). If the emission gas contains unstable, reactive, or semi-volatile substances, the measurement will depend on the filtration temperature.

1.5The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

ASTM D 6831 : 2011 : R2018 Standard Test Method for Sampling and Determining Particulate Matter in Stack Gases Using an In-Stack, Inertial Microbalance

ASTM D 3796 : 1990 : R1998 Standard Practice for Calibration of Type S Pitot Tubes
ASTM D 3670 : 1991 : R1996 : EDT 1 Standard Guide for Determination of Precision and Bias of Methods of Committee D22
ASTM D 2986 : 1995 Standard Method for Evaluation of Air Assay Media by the Monodisperse DOP (Dioctyl Phthalate) Smoke Test
ASTM D 1356 : 2015 Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 3154 : 2000 : R2006 Standard Test Method for Average Velocity in a Duct (Pitot Tube Method)
ASTM E 2251 : 2007 Standard Specification for Liquid-in-Glass ASTM Thermometers with Low-Hazard Precision Liquids
ASTM D 3670 : 1991 : R2022 Standard Guide for Determination of Precision and Bias of Methods of Committee D22
ASTM D 3154 : 2000 Standard Test Method for Average Velocity in a Duct (Pitot Tube Method)
ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
ASTM E 2251 : 2003 : REV A Standard Specification for Liquid-in-Glass ASTM Thermometers with Low-Hazard Precision Liquids
ASTM D 1356 : 2017 Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 2986 : 1995 : REV A Standard Method for Evaluation of Air Assay Media by the Monodisperse DOP (Dioctyl Phthalate) Smoke Test
ASTM D 3796 : 1990 : R2004 Standard Practice for Calibration of Type S Pitot Tubes
ASTM D 3631 : 1999 : R2004 Standard Test Methods for Measuring Surface Atmospheric Pressure
ASTM D 3154 : 2014 : R2023 Standard Test Method for Average Velocity in a Duct (Pitot Tube Method)
ASTM E 2251 : 2003 Standard Specification for Liquid-in-Glass ASTM Thermometers with Low-Hazard Precision Liquids
ASTM D 1356 : 2015 : REV B Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM E 2251 : 2014 : R2021 Standard Specification for Liquid-in-Glass ASTM Thermometers with Low-Hazard Precision Liquids
ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
ASTM D 3670 : 1991 : R2014 Standard Guide for Determination of Precision and Bias of Methods of Committee D22
ASTM D 3154 : 2014 Standard Test Method for Average Velocity in a Duct (Pitot Tube Method)
ASTM E 2251 : 2010 Standard Specification for Liquid-in-Glass ASTM Thermometers with Low-Hazard Precision Liquids
ASTM D 1356 : 2014 : REV A Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM E 2251 : 2011 Standard Specification for Liquid-in-Glass ASTM Thermometers with Low-Hazard Precision Liquids
ASTM D 3796 : 2009 : R2016 Standard Practice for Calibration of Type S Pitot Tubes
ASTM E 2251 : 2014 Standard Specification for Liquid-in-Glass ASTM Thermometers with Low-Hazard Precision Liquids
ASTM D 3631 : 1999 : R2007 Standard Test Methods for Measuring Surface Atmospheric Pressure
ASTM D 3670 : 1991 : R2001 Standard Guide for Determination of Precision and Bias of Methods of Committee D22
ASTM D 3796 : 2009 : R2024 Standard Practice for Calibration of Type S Pitot Tubes
ASTM D 3685/D3685M : 2013 Standard Test Methods for Sampling and Determination of Particulate Matter in Stack Gases
ASTM D 1193 : 1991 Standard Specification for Reagent Water
ASTM D 3631 : 1999 : R2011 Standard Test Methods for Measuring Surface Atmospheric Pressure
ASTM D 2986 : 1995 : REV A : R1999 Standard Practice for Evaluation of Air Assay Media by the Monodisperse DOP (Dioctyl Phthalate) Smoke Test (Withdrawn 2004)
ASTM D 1356 : 2015 : REV A Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 1356 : 2005 : R2010 Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 3670 : 1991 : R2007 Standard Guide for Determination of Precision and Bias of Methods of Committee D22
ASTM E 1 : 2014 : R2020 Standard Specification for ASTM Liquid-in-Glass Thermometers
ASTM D 1356 : 2020 Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 1356 : 2000 : REV A Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 2986 : 1971 Standard Method For Evaluation Of Air Assay Media By The Monodisperse Dop (Dioctyl Phthalate) Smoke Test
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM D 1356 : 2014 : REV B Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 1356 : 2014 Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 1193 : 2006 Standard Specification for Reagent Water
ASTM D 1193 : 1999 Standard Specification for Reagent Water
ASTM D 3685/D3685M : 2013 : R2021 Standard Test Methods for Sampling and Determination of Particulate Matter in Stack Gases
ASTM D 1356 : 2005 Standard Terminology Relating to Sampling and Analysis of Atmospheres
ASTM D 3796 : 2009 : R2024 : EDT 1 Standard Practice for Calibration of Type S Pitot Tubes
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
ASTM D 3796 : 2009 Standard Practice for Calibration of Type S Pitot Tubes
ASTM D 3631 : 1999 Standard Test Methods for Measuring Surface Atmospheric Pressure
ASTM D 3631 : 1999 : R2017 Standard Test Methods for Measuring Surface Atmospheric Pressure

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