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ASTM D 6481 : 2024

Current

Current

The latest, up-to-date edition.

Standard Test Method for Determination of Phosphorus, Sulfur, Calcium, and Zinc in Lubrication Oils by Energy Dispersive X-ray Fluorescence Spectroscopy

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

15-03-2024

1.1This test method covers the quantitative determination of additive elements in unused lubricating oils, as shown in Table 1.

1.2This test method is limited to the use of energy dispersive X-ray fluorescence (EDXRF) spectrometers employing an X-ray tube for excitation in conjunction with the ability to separate the signals of adjacent elements.

1.3This test method uses interelement correction factors calculated from empirical calibration data.

1.4This test method is not suitable for the determination of magnesium and copper at the concentrations present in lubricating oils.

1.5This test method excludes lubricating oils that contain chlorine or barium as an additive element.

1.6This test method can be used by persons who are not skilled in X-ray spectrometry. It is intended to be used as a routine test method for production control analysis.

1.7This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations to use.

1.8This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Committee
D 02
DocumentType
Test Method
Pages
5
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

ASTM D 7578 : 2020 Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants
ASTM D 7455 : 2019 Standard Practice for Sample Preparation of Petroleum and Lubricant Products for Elemental Analysis
ASTM D 6074 : 2015 : R2022 Standard Guide for Characterizing Hydrocarbon Lubricant Base Oils
ASTM D 7343 : 2020 Standard Practice for Optimization, Sample Handling, Calibration, and Validation of X-ray Fluorescence Spectrometry Methods for Elemental Analysis of Petroleum Products and Lubricants

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