• ASTM D 7371 : 2014

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

    Standard Test Method for Determination of Biodiesel (Fatty Acid Methyl Esters) Content in Diesel Fuel Oil Using Mid Infrared Spectroscopy (FTIR-ATR-PLS Method)

    Available format(s):  Hardcopy, PDF

    Superseded date:  23-08-2022

    Language(s):  English

    Published date:  17-10-2014

    Publisher:  American Society for Testing and Materials

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    Abstract - (Show below) - (Hide below)

    This test method covers the determination of the content of fatty acid methyl esters (FAME) biodiesel in diesel fuel oils.

    Scope - (Show below) - (Hide below)

    1.1This test method covers the determination of the content of fatty acid methyl esters (FAME) biodiesel in diesel fuel oils. It is applicable to concentrations from 1.00 to 20 volume % (see Note 1). This procedure is applicable only to FAME. Biodiesel in the form of fatty acid ethyl esters (FAEE) will cause a negative bias.

    Note 1:Using the proper ATR sample accessory, the range maybe expanded from 1 to 100 volume %, however precision data is not available above 20 volume %.

    1.2The values stated in SI units of measurement are to be regarded as the standard. The values given in parentheses are for information only.

    1.3This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

    General Product Information - (Show below) - (Hide below)

    Committee D 02
    Document Type Test Method
    Publisher American Society for Testing and Materials
    Status Superseded
    Superseded By
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM D 8274 : 2020 : REV A Standard Test Method for Determination of Biodiesel (Fatty Acid Methyl Esters) Content in Diesel Fuel Oil by Portable Rapid Mid-Infrared Analyzer
    ASTM D 396 : 2021 Standard Specification for Fuel Oils
    ASTM D 975 : 2021 Standard Specification for Diesel Fuel
    ASTM D 7467 : 2020 : REV A Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 396 : 2019 Standard Specification for Fuel Oils
    ASTM D 7861 : 2014 : R2019 Standard Test Method for Determination of Fatty Acid Methyl Esters (FAME) in Diesel Fuel by Linear Variable Filter (LVF) Array Based Mid-Infrared Spectroscopy
    ASTM D 7467 : 2019 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM D 4057 : 2019 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 4057 : 1995 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2010 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 7467 : 2018 : REV A Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 1298 : 2012 : REV A Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 6299 : 2013 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4177 : 2016 : EDT 1 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2017 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2017 : REV B Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4052 : 1996 : R2002 : EDT 1 Standard Test Method for Density and Relative Density of Liquids by Digital Density Meter
    ASTM D 7467 : 2009 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 6299 : 2009 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 1298 : 2012 : REV B Standard Test Method for Density, Relative Density, or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 4177 : 1995 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 6751 : 2006 : REV A Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 4057 : 2012 : R2018 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 4052 : 2018 : REV A Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
    ASTM D 6751 : 2007 : REV B Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6751 : 2006 : EDT 1 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6299 : 2013 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2021 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6751 : 2018 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6751 : 2009 : REV A Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6751 : 2007 : REV B : EDT 1 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM E 2056 : 2004 Standard Practice for Qualifying Spectrometers and Spectrophotometers for Use in Multivariate Analyses, Calibrated Using Surrogate Mixtures
    ASTM D 975 : 2019 : REV B Standard Specification for Diesel Fuel
    ASTM D 5854 : 1996 : R2010 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
    ASTM D 6299 : 2010 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 7467 : 2010 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 4737 : 2009 Standard Test Method for Calculated Cetane Index by Four Variable Equation
    ASTM D 7467 : 2008 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 6751 : 2007 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 1298 : 1999 : R2005 Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 4052 : 2009 Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
    ASTM D 4057 : 1981 : EDT 2 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 1298 : 2012 : REV B : R2017 Standard Test Method for Density, Relative Density, or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 7467 : 2017 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 1298 : 2012 Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 5854 : 2019 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
    ASTM D 6751 : 2012 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM E 1655 : 2004 Standard Practices for Infrared Multivariate Quantitative Analysis
    ASTM D 975 : 2021 Standard Specification for Diesel Fuel
    ASTM D 7467 : 2015 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 1298 : 1999 : EDT 2 Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 6751 : 2014 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 5854 : 1996 : R2005 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
    ASTM D 7467 : 2015 : REV A Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 4307 : 1999 : R2004 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
    ASTM D 976 : 2021 Standard Test Method for Calculated Cetane Index of Distillate Fuels
    ASTM D 6299 : 2000 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2010 : EDT 2 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 1298 : 1999 Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 6751 : 2011 : REV B Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 975 : 2020 : REV C Standard Specification for Diesel Fuel
    ASTM D 6299 : 2016 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6751 : 2015 : REV B Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 4057 : 2006 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 7467 : 2015 : EDT 1 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 4177 : 2015 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 7467 : 2015 : REV C Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 6751 : 2015 : REV C Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 4052 : 2011 Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
    ASTM D 6299 : 2019 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4052 : 2016 Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
    ASTM D 6751 : 2015 : REV A Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 4057 : 2012 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2000 : REV A Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4307 : 1999 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
    ASTM D 4737 : 2009 : REV A Standard Test Method for Calculated Cetane Index by Four Variable Equation
    ASTM D 4737 : 2021 Standard Test Method for Calculated Cetane Index by Four Variable Equation
    ASTM D 7467 : 2014 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 6751 : 2002 Standard Specification for Biodiesel Fuel (B100) Blend Stock for Distillate Fuels
    ASTM D 6751 : 2003 : REV A Standard Specification for Biodiesel Fuel (B100) Blend Stock for Distillate Fuels
    ASTM D 1298 : 1999 : EDT 1 Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 4737 : 2010 : R2016 Standard Test Method for Calculated Cetane Index by Four Variable Equation
    ASTM D 6751 : 2020 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6299 : 2020 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4177 : 1995 : R2010 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4307 : 2017 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
    ASTM D 4737 : 2003 Standard Test Method for Calculated Cetane Index by Four Variable Equation
    ASTM D 6299 : 2008 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6751 : 2003 Standard Specification for Biodiesel Fuel (B100) Blend Stock for Distillate Fuels
    ASTM E 1655 : 2017 Standard Practices for Infrared Multivariate Quantitative Analysis
    ASTM D 6751 : 2008 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6751 : 2019 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 4177 : 1995 : R2000 Standard Practice for Automatic Sampling of Peroleum and Petroleum Products
    ASTM D 5854 : 1996 : R2000 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
    ASTM D 7467 : 2020 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 6299 : 2002 : EDT 1 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4052 : 1996 Standard Test Method for Density and Relative Density of Liquids by Digital Density Meter
    ASTM D 7467 : 2018 : REV B Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 4307 : 2017 : R2021 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
    ASTM E 1655 : 2000 Standard Practices for Infrared Multivariate Quantitative Analysis
    ASTM D 6751 : 2015 : REV C : EDT 1 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 7467 : 2009 : REV A Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 4307 : 1999 : R2010 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
    ASTM D 4737 : 1996 : REV A Standard Test Method for Calculated Cetane Index by Four Variable Equation
    ASTM D 6299 : 2022 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6751 : 2007 : REV A Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM E 1655 : 2005 Standard Practices for Infrared Multivariate Quantitative Analysis
    ASTM D 7467 : 2015 : REV C : EDT 1 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 4057 : 2022 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 976 : 2006 : R2016 Standard Test Method for Calculated Cetane Index of Distillate Fuels
    ASTM D 7467 : 2019 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 6751 : 2011 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 4177 : 2016 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 7467 : 2015 : REV B Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 4052 : 2022 Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
    ASTM D 4177 : 1995 : R2005 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4737 : 2004 Standard Test Method for Calculated Cetane Index by Four Variable Equation
    ASTM D 1298 : 1985 : R1990 : EDT 1 Standard Practice for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 6751 : 2011 : REV A Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6751 : 2015 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 5854 : 2019 : REV A Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
    ASTM D 6299 : 2007 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 7467 : 2013 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 4052 : 2015 Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
    ASTM E 2056 : 2004 : R2016 Standard Practice for Qualifying Spectrometers and Spectrophotometers for Use in Multivariate Analyses, Calibrated Using Surrogate Mixtures
    ASTM D 6299 : 2007 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM E 2056 : 2004 : R2010 Standard Practice for Qualifying Spectrometers and Spectrophotometers for Use in Multivariate Analyses, Calibrated Using Surrogate Mixtures
    ASTM D 4057 : 1995 : R2000 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2020 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM E 1655 : 2005 : R2012 Standard Practices for Infrared Multivariate Quantitative Analysis
    ASTM D 7467 : 2018 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 6299 : 2017 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6751 : 2009 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 4177 : 2015 : REV A Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4307 : 1999 : R2015 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
    ASTM D 4057 : 2006 : R2011 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM E 2056 : 2000 Standard Practice for Qualifying Spectrometers and Spectrophotometers for Use in Multivariate Analyses, Calibrated Using Surrogate Mixtures
    ASTM D 6751 : 2010 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 5854 : 1996 : R2015 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
    ASTM D 4052 : 2018 Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
    ASTM D 4737 : 2010 Standard Test Method for Calculated Cetane Index by Four Variable Equation
    ASTM D 6751 : 2002 : REV A Standard Specification for Biodiesel Fuel (B100) Blend Stock for Distillate Fuels
    ASTM D 6299 : 2002 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
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