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ASTM D 7417 : 2017

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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Standard Test Method for Analysis of In-Service Lubricants Using Particular Four-Part Integrated Tester (Atomic Emission Spectroscopy, Infrared Spectroscopy, Viscosity, and Laser Particle Counter)

Available format(s)

Hardcopy , PDF

Superseded date

18-07-2024

Superseded by

ASTM D 7417 : 2024

Language(s)

English

Published date

01-10-2017

€67.30
Excluding VAT

Committee
D 02
DocumentType
Test Method
Pages
9
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1This test method covers the quantitative analysis of in-service lubricants using an automatic testing device that integrates these varied technologies: atomic emission spectroscopy, infrared spectroscopy, viscosity, and particle counting.

1.2This is suited for in-service lubricating oils having viscosities in the range between ISO 10 and ISO 320 and properties in the ranges given in Tables 1 and 2.

TABLE 1 Element Test Parameters Measured, Calculated, and Reported

Element

Low Range, mg/kg

High Range, mg/kg

Element

Low Range, mg/kg

High Range, mg/kg

Aluminum

5 to 100

NA

Molybdenum

10 to 1000

NA

Barium

25 to 150

150 to 2000

Nickel

5 to 100

NA

Boron

5 to 100

100 to 1000

Phosphorous

100 to 600

600 to 4000

Calcium

25 to 500

500 to 9000

Potassium

10 to 1000

1000 to 4000

Chromium

8 to 100

NA

Silicon

5 to 150

150 to 3000

Copper

5 to 500

500 to 1000

Sodium

10 to 1000

NA

Iron

6 to 1000

1000 to 3000

Tin

6 to 100

NA

Lead

6 to 150

NA

Titanium

8 to 100

NA

Magnesium

5 to 100

100 to 3000

Vanadium

7 to 100

NA

Manganese

5 to 100

NA

Zinc

8 to 100

100 to 4000

TABLE 2 Physical Properties Parameters Measured, Calculated, and Reported

Note 1:Review Test Method D4739 and D2896 for particular lubricating oil applications.

Physical Property

Range

Water,  % by mass

0.1 to 3

Glycol,  % by mass

0.1 to 2

Soot,  % by mass

0.1 to 4

Fuel Dilution,  % by mass

0.1 to 15

Oxidation, abs.

0.1 to 50

Nitration, abs.

0.1 to 35

Calculated Viscosity - IR

4 to 35 (100° cSt)

Viscosity 40 °C, cSt (optional)

30 to 320

Viscosity 100 °C, cSt (optional)

5 to 25

Viscosity Index

5 to 150

Base Number, mg/g KOH

1.0 to 17

1.3This test method may be used to establish trends in wear and contamination of in-service lubricants and may not give equivalent numerical results to current ASTM test methods.

1.4This test method is not intended for use with crude oil.

1.5The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (Specific hazard statements are given in Section 9 and 11.3.)

1.7This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D 4057 : 2019 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 2896 : 1998 Standard Test Method for Base Number of Petroleum Products by Potentiometric Perchloric Acid Titration
ASTM E 2412 : 2023 Standard Practice for Condition Monitoring of In-Service Lubricants by Trend Analysis Using Fourier Transform Infrared (FT-IR) Spectrometry
ASTM E 2412 : 2010 : R2018 Standard Practice for Condition Monitoring of In-Service Lubricants by Trend Analysis Using Fourier Transform Infrared (FT-IR) Spectrometry
ASTM D 445 : 2021 : EDT 2 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 445 : 2017 : REV A Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 445 : 1988 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and the Calculation of Dynamic Viscosity)
ASTM D 4739 : 2017 Standard Test Method for Base Number Determination by Potentiometric Hydrochloric Acid Titration
ASTM D 4739 : 1996 Standard Test Method for Base Number Determination by Potentiometric Titration
ASTM D 7042 : 2021 Standard Test Method for Dynamic Viscosity and Density of Liquids by Stabinger Viscometer (and the Calculation of Kinematic Viscosity)
ASTM D 445 : 2019 : REV A Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 2270 : 2010 : R2016 Standard Practice for Calculating Viscosity Index from Kinematic Viscosity at 40 °C and 100 °C
ASTM D 6595 : 2022 Standard Test Method for Determination of Wear Metals and Contaminants in Used Lubricating Oils or Used Hydraulic Fluids by Rotating Disc Electrode Atomic Emission Spectrometry
ASTM D 2270 : 2024 Standard Practice for Calculating Viscosity Index from Kinematic Viscosity at 40 °C and 100 °C
ASTM D 445 : 2019 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 445 : 2001 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (the Calculation of Dynamic Viscosity)
ASTM D 445 : 2024 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 445 : 2021 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 2896 : 2015 Standard Test Method for Base Number of Petroleum Products by Potentiometric Perchloric Acid Titration
ASTM D 6595 : 2017 Standard Test Method for Determination of Wear Metals and Contaminants in Used Lubricating Oils or Used Hydraulic Fluids by Rotating Disc Electrode Atomic Emission Spectrometry
ASTM D 4739 : 2023 Standard Test Method for Base Number Determination by Potentiometric Hydrochloric Acid Titration
ASTM D 4057 : 2022 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 7042 : 2021 : REV A Standard Test Method for Dynamic Viscosity and Density of Liquids by Stabinger Viscometer (and the Calculation of Kinematic Viscosity)
ASTM E 2412 : 2023 : REV A Standard Practice for Condition Monitoring of In-Service Lubricants by Trend Analysis Using Fourier Transform Infrared (FT-IR) Spectrometry
ASTM D 445 : 2018 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 445 : 2021 : EDT 1 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 2896 : 2021 Standard Test Method for Base Number of Petroleum Products by Potentiometric Perchloric Acid Titration
ASTM D 445 : 2023 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)

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