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ASTM D 7455 : 2024

Current

Current

The latest, up-to-date edition.

Standard Practice for Sample Preparation of Petroleum and Lubricant Products for Elemental Analysis

Available format(s)

PDF

Language(s)

English

Published date

01-07-2024

€57.50
Excluding VAT

Committee
D 02
DocumentType
Standard Practice
Pages
9
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

1.1This practice covers different means by which petroleum product and lubricant samples may be prepared before the measurement of their elemental content using different analytical techniques.

1.2This practice includes only the basic steps for generally encountered sample types. Anything out of the ordinary may require special procedures. See individual test methods for instructions to handle such situations.

1.3This practice is not a substitute for a thorough understanding of the actual test method to be used, caveats the test method contains, and additional sample preparation that may be required.

1.4The user should not expand the scope of the test methods to materials or concentrations outside the scope of the test methods being used without thoroughly understanding the implications of such deviations.

1.5This practice may also be applicable to sample preparation of non-petroleum based bio-fuels for elemental analysis. Currently, work is ongoing in ASTM Subcommittee D02.03; as information becomes available, it will be added to this standard.

1.6The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.7This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.8This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D 8056 : 2024 Standard Guide for Elemental Analysis of Crude Oil
ASTM D 7578 : 2020 Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants
ASTM D 7876 : 2013 : R2018 Standard Practice for Practice for Sample Decomposition Using Microwave Heating (With or Without Prior Ashing) for Atomic Spectroscopic Elemental Determination in Petroleum Products and Lubricants
ASTM D 7740 : 2020 Standard Practice for Optimization, Calibration, and Validation of Atomic Absorption Spectrometry for Metal Analysis of Petroleum Products and Lubricants

ASTM D 4929 : 2024 Standard Test Method for Determination of Organic Chloride Content in Crude Oil
ASTM D 482 : 2019 Standard Test Method for Ash from Petroleum Products
ASTM D 3231 : 2025 Standard Test Method for Phosphorus in Gasoline
ASTM C 1234 : 2011 : R2019 Standard Practice for Preparation of Oils and Oily Waste Samples by High-Pressure, High-Temperature Digestion for Trace Element Determinations
ASTM D 7039 : 2024 Standard Test Method for Sulfur in Gasoline, Diesel Fuel, Jet Fuel, Kerosine, Biodiesel, Biodiesel Blends, and Gasoline-Ethanol Blends by Monochromatic Wavelength Dispersive X-ray Fluorescence Spectrometry
ASTM D 4047 : 2025 Standard Test Method for Phosphorus in Lubricating Oils and Additives by Quinoline Phosphomolybdate Method<rangeref></rangeref >
ASTM D 5762 : 2024 Standard Test Method for Nitrogen in Liquid Hydrocarbons, Petroleum and Petroleum Products by Boat-Inlet Chemiluminescence
ASTM C 1234 : 2024 Standard Practice for Preparation of Oils and Oily Waste Samples by High-Pressure, High-Temperature Digestion for Trace Element Determinations
ASTM D 6728 : 2016 : R2021 Standard Test Method for Determination of Contaminants in Gas Turbine and Diesel Engine Fuel by Rotating Disc Electrode Atomic Emission Spectrometry
ASTM D 7260 : 2020 Standard Practice for Optimization, Calibration, and Validation of Inductively Coupled Plasma-Atomic Emission Spectrometry (ICP-AES) for Elemental Analysis of Petroleum Products and Lubricants
ASTM D 86 : 2023 : REV A : EDT 1 Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure
ASTM D 7318 : 2019 : EDT 1 Standard Test Method for Existent Inorganic Sulfate in Ethanol by Potentiometric Titration
ASTM D 7111 : 2016 : R2025 Standard Test Method for Determination of Trace Elements in Middle Distillate Fuels by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM D 4175 : 2024 : EDT 1 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4929 : 2022 Standard Test Method for Determination of Organic Chloride Content in Crude Oil
ASTM D 3120 : 2025 Standard Test Method for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry
ASTM D 3231 : 2024 Standard Test Method for Phosphorus in Gasoline
ASTM D 7620 : 2010 : R2020 Standard Test Method for Determination of Total Sulfur in Liquid Hydrocarbon Based Fuels by Continuous Injection, Air Oxidation and Ultraviolet Fluorescence Detection (Withdrawn 2025)
ASTM D 482 : 2019 : EDT 1 Standard Test Method for Ash from Petroleum Products
ASTM D 3120 : 2008 : R2019 Standard Test Method for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry
ASTM D 7318 : 2025 Standard Test Method for Existent Inorganic Sulfate in Ethanol by Potentiometric Titration
ASTM D 2622 : 2024 : REV A Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry
ASTM D 7622 : 2020 : R2025 Standard Test Method for Total Mercury in Crude Oil Using Combustion and Direct Cold Vapor Atomic Absorption Method with Zeeman Background Correction
ASTM D 5384 : 2014 : R2019 Standard Test Methods for Chlorine in Used Petroleum Products (Field Test Kit Method)
ASTM D 2622 : 2024 Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry
ASTM D 7039 : 2015 : REV A : R2020 Standard Test Method for Sulfur in Gasoline, Diesel Fuel, Jet Fuel, Kerosine, Biodiesel, Biodiesel Blends, and Gasoline-Ethanol Blends by Monochromatic Wavelength Dispersive X-ray Fluorescence Spectrometry
ASTM D 8110 : 2017 Standard Test Method for Elemental Analysis of Distillate Products by Inductively Coupled Plasma Mass Spectrometry (ICP-MS)
ASTM D 7260 : 2025 Standard Practice for Optimization, Calibration, and Validation of Inductively Coupled Plasma-Atomic Emission Spectrometry (ICP-AES) for Elemental Analysis of Petroleum Products and Lubricants
ASTM D 6728 : 2016 : R2025 Standard Test Method for Determination of Contaminants in Gas Turbine and Diesel Engine Fuel by Rotating Disc Electrode Atomic Emission Spectrometry
ASTM D 482 : 2025 Standard Test Method for Ash from Petroleum Products
ASTM D 4045 : 2025 Standard Test Method for Sulfur in Petroleum Products by Hydrogenolysis and Rateometric Colorimetry
ASTM D 4629 : 2017 Standard Test Method for Trace Nitrogen in Liquid Hydrocarbons by Syringe/Inlet Oxidative Combustion and Chemiluminescence Detection
ASTM D 4294 : 2021 Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry
ASTM D 7622 : 2020 Standard Test Method for Total Mercury in Crude Oil Using Combustion and Direct Cold Vapor Atomic Absorption Method with Zeeman Background Correction
ASTM D 5453 : 2019 : REV A Standard Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence
ASTM D 5384 : 2025 Standard Test Methods for Chlorine in Used Petroleum Products (Field Test Kit Method)
ASTM D 86 : 2023 : REV A : EDT 2 Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure
ASTM D 4175 : 2024 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
ASTM D 4629 : 2024 Standard Test Method for Trace Nitrogen in Liquid Hydrocarbons by Syringe/Inlet Oxidative Combustion and Chemiluminescence Detection
ASTM D 4047 : 2018 Standard Test Method for Phosphorus in Lubricating Oils and Additives by Quinoline Phosphomolybdate Method
ASTM D 5453 : 2025 Standard Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence
ASTM D 8110 : 2025 Standard Test Method for Elemental Analysis of Distillate Products by Inductively Coupled Plasma Mass Spectrometry (ICP-MS)
ASTM D 4294 : 2024 Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry
ASTM D 4045 : 2019 Standard Test Method for Sulfur in Petroleum Products by Hydrogenolysis and Rateometric Colorimetry
ASTM D 7111 : 2016 : R2021 Standard Test Method for Determination of Trace Elements in Middle Distillate Fuels by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM D 5453 : 2024 Standard Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence
ASTM D 1266 : 2018 Standard Test Method for Sulfur in Petroleum Products (Lamp Method) (Withdrawn 2025)

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€57.50
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