ASTM D 7510 : 2010 : R2016 : EDT 1
Current
The latest, up-to-date edition.
Standard Practice for Performing Detection and Quantitation Estimation and Data Assessment Utilizing DQCALC Software, based on ASTM Practices D6091 and D6512 of Committee D19 on Water
Hardcopy , PDF
English
15-12-2016
Important note : Users cannot be edited or removed once added to your Multi user PDF.CONTAINED IN VOL. 11.01, 2017 Defines detection estimates (DE) and quantitation estimates (QE) for the constant, straight-line, exponential, and hybrid (Rocke-Lorenzato) models of the variation of [inter or intra] laboratory standard deviation (ILSD) with concentration.
| Committee |
D 19
|
| DocumentType |
Standard Practice
|
| Pages |
2
|
| ProductNote |
Reconfirmed EDT 1
|
| PublisherName |
American Society for Testing and Materials
|
| Status |
Current
|
| Supersedes |
1.1This software was developed to automate calculations within three ASTM standards: Practices D2777 (outlier removal section), D6091, and D6512.
1.2The program calculates detection estimates (DE) and quantitation estimates (QE) for the constant, straight-line, exponential, and hybrid (Rocke-Lorenzato) models of the variation of [inter or intra] laboratory standard deviation (ILSD) with concentration. Calculations are shown in the DE_QE worksheet and results are shown in the DLs & QLs worksheet. Several plots are generated showing how well each model fits the data. The least complex model to fit the data with adequate confidence must be used by the ASTM standards.
Note 1:Modeling techniques automated in this practice and with this software have been shown to work well with most data sets. Users of this software are cautioned that with some, rare data sets, anomalous results may be obtained, and manual forcing of a different model may be required. It has been noted that for some data sets when an exponential model is selected, there may be a lack of convergence on a result or there may be a convergence on two separate results.
1.3Users of DQCALC should refer to Practices D2777, D6091, and D6512 for the specifics of the scope and application of the Practices.
1.4The IDE Practice (D6091) and the IQE Practice (D6512) are concerned with estimates of limits of detection and limits of quantitation based on inter-laboratory data. DQCALC may also be employed to calculate detection and quantitation estimates based on single laboratory data.
1.5The DQCALC Software consists of a Microsoft Excel3 workbook spreadsheet and associated macros and a user manual in Microsoft Word.3
| ASTM D 7783 : 2013 | Standard Practice for Within-laboratory Quantitation Estimation (WQE) |
| ASTM D 7782 : 2013 | Standard Practice for Determination of the 99 %/95 % Critical Level (WCL) and a Reliable Detection Estimate (WDE) Based on Within-laboratory Data (Withdrawn 2022) |
| ASTM D 7729 : 2012 : R2018 : EDT 1 | Standard Practice for Determining and Expressing Precision of Measurement Results, in the Analysis of Water, as Relative Standard Deviation, Utilizing DQCALC Software |
| ASTM D 6091 : 2007 | Standard Practice for 99 %/95 % Interlaboratory Detection Estimate (IDE) for Analytical Methods with Negligible Calibration Error |
| ASTM D 2777 : 2013 : REDLINE | Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water |
| ASTM D 2777 : 2012 | Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water |
| ASTM D 2777 : 2003 | Standard Practice for Determination of Precision and Bias of Applicable Methods of Committee D-19 on Water |
| ASTM D 2777 : 2021 | Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water |
| ASTM D 2777 : 2013 | Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water |
| ASTM D 2777 : 1998 | Standard Practice for Determination of Precision and Bias of Applicable Methods of Committee D-19 on Water |
| ASTM D 6512 : 2003 | Standard Practice for Interlaboratory Quantitation Estimate |
| ASTM D 2777 : 2008 | Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water |
| ASTM D 2777 : 2006 | Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water |
| ASTM D 6091 : 2003 | Standard Practice for 99 %/95 % Interlaboratory Detection Estimate (IDE) for Analytical Methods with Negligible Calibration Error |
| ASTM D 6091 : 2007 : R2014 | Standard Practice for 99 %/95 % Interlaboratory Detection Estimate (IDE) for Analytical Methods with Negligible Calibration Error (Withdrawn 2023) |
| ASTM D 6512 : 2007 | Standard Practice for Interlaboratory Quantitation Estimate |
| ASTM D 2777 : 2008 : EDT 1 | Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water |
| ASTM D 6512 : 2000 | Standard Practice for Interlaboratory Quantitation Estimate |
| ASTM D 6091 : 1997 | Standard Practice for 99 %/95 % Interlaboratory Detection Estimate (IDE) for Analytical Methods with Negligible Calibration Error |
| ASTM D 6512 : 2007 : R2014 | Standard Practice for Interlaboratory Quantitation Estimate (Withdrawn 2023) |
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