Standard Test Method for Determination of Residue Composition in Liquefied Petroleum Gas (LPG) Using Automated Thermal Desorption/Gas Chromatography (ATD/GC) (Withdrawn 2021)

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Withdrawn date

21-01-2021

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English

Published date

21-03-2013

Publisher

American Society for Testing and Materials

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CONTAINED IN VOL. 05.05, 2018 Defines the determination of residue in LPG by automated thermal desorption/gas chromatography (ATD/GC) using flame ionization detection (FID).

Committee	D 02
DocumentType	Test Method
Pages	15
PublisherName	American Society for Testing and Materials
Status	Withdrawn

1.1This test method covers the determination of residue in LPG by automated thermal desorption/gas chromatography (ATD/GC) using flame ionization detection (FID).

1.2The quantitation of residue covers a component boiling point range from 69°C to 522°C, equivalent to the boiling points of C₆ through C₄₀ n-paraffins.

1.2.1The boiling range covers possible LPG contaminants such as gasoline, diesel fuel, phthalates and compressor oil. Qualitative information on the nature of the residue can be obtained from this test method.

1.2.2Materials insoluble in LPG and components which do not elute from the gas chromatograph or which have no response in a flame ionization detector are not determined.

1.2.3The reporting limit (or limit of quantitation) for total residue is 6.7 µg/g.

1.2.4The dynamic range of residue quantitation is 6.7 to 3300 µg/g.

1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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ASTM D 6299 : 2010	Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 2158 : 2005	Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
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ASTM D 3700 : 2001	Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
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ASTM D 6299 : 2009	Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 1835 : 1997	Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 2158 : 2004	Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
ASTM D 6299 : 2013	Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 3700 : 2014	Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
ASTM D 6299 : 2010 : EDT 1	Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 2158 : 2011	Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
ASTM D 2158 : 1989	Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
ASTM D 3700 : 1994	Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
ASTM D 1835 : 2018 : REV A	Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 1835 : 2012	Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 6299 : 2000	Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2010 : EDT 2	Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2016	Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2019	Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 1835 : 2003 : REV A	Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 6299 : 2000 : REV A	Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
ASTM D 1835 : 2003	Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 1835 : 2013	Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 1835 : 2020	Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 6299 : 2020	Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2008	Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 1835 : 2018	Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 2158 : 2002	Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
ASTM D 1265 : 2004	Standard Practice for Sampling Liquefied Petroleum (LP) Gases (Manual Method)
ASTM D 3700 : 2012	Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
ASTM D 6299 : 2002 : EDT 1	Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
ASTM D 2158 : 2016 : REV A	Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
ASTM D 3700 : 2007	Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
ASTM D 1835 : 2016	Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 1265 : 2011 : R2017 : EDT 1	Standard Practice for Sampling Liquefied Petroleum (LP) Gases, Manual Method
ASTM D 2158 : 1997 : EDT 1	Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
ASTM D 1835 : 2011	Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 1265 : 2005	Standard Practice for Sampling Liquefied Petroleum (LP) Gases (Manual Method)
ASTM D 1265 : 2004 : REV A	Standard Practice for Sampling Liquefied Petroleum (LP) Gases (Manual Method)
ASTM D 1265 : 2011	Standard Practice for Sampling Liquefied Petroleum (LP) Gases, Manual Method
ASTM D 2158 : 2016 : REV A : EDT 1	Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
ASTM D 3700 : 2016	Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder
ASTM D 6299 : 2007	Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2007 : EDT 1	Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 6299 : 2017	Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
ASTM D 1835 : 2005	Standard Specification for Liquefied Petroleum (LP) Gases
ASTM D 6299 : 2002	Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance

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ASTM D 7828 : 2012

Standard Test Method for Determination of Residue Composition in Liquefied Petroleum Gas (LPG) Using Automated Thermal Desorption/Gas Chromatography (ATD/GC) (Withdrawn 2021)

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