• ASTM D 8127 : 2017 : EDT 1

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

    Standard Test Method for Coupled Particulate and Elemental Analysis using X-ray Fluorescence (XRF) for In-Service Lubricants

    Available format(s):  Hardcopy, PDF

    Superseded date:  25-05-2023

    Language(s):  English

    Published date:  01-05-2018

    Publisher:  American Society for Testing and Materials

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    Abstract - (Show below) - (Hide below)

    CONTAINED IN VOL. 05.05, 2018 Defines particle analysis2 test method for in-service lubricants describes using a combination of pore blockage particle counting and energy dispersive X-ray fluorescence (EDXRF) spectrometry for the quantitative determination of solid particle counts larger than four (4) micrometres, and elemental content of suspended particulate of iron (Fe) and copper (Cu) in such lubricants.

    Scope - (Show below) - (Hide below)

    1.1This automatic wear particle analysis2 test method for in-service lubricants describes using a combination of pore blockage particle counting and energy dispersive X-ray fluorescence (EDXRF) spectrometry for the quantitative determination of solid particle counts larger than four (4) micrometres, and elemental content of suspended particulate of iron (Fe) and copper (Cu) in such lubricants.

    1.2This test method provides for the determination of the elemental content of suspended particulate of Fe greater than 4 μm in the range of 6 mg/kg to 223 mg/kg. Suspended particulate of copper greater than 4 μm is determined in the range of 3.5 mg/kg to 92.4 mg/kg in the lubricant. Total particle count greater than 4 μm is determined in the range of 11 495 particles/mL greater than 4 μm to 2 169 500 particles/mL greater than 4 μm in the lubricant.

    1.3This test method is applicable to all known in-service lubricants (API Groups I-V) at any stage of degradation.

    1.4This test method uses an empirical inter-element correction methodology.

    1.5The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

    1.7This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

    General Product Information - (Show below) - (Hide below)

    Committee D 02
    Document Type Test Method
    Publisher American Society for Testing and Materials
    Status Superseded
    Superseded By
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM D 7343 : 2018 Standard Practice for Optimization, Sample Handling, Calibration, and Validation of X-ray Fluorescence Spectrometry Methods for Elemental Analysis of Petroleum Products and Lubricants
    ASTM D 7343 : 2020 Standard Practice for Optimization, Sample Handling, Calibration, and Validation of X-ray Fluorescence Spectrometry Methods for Elemental Analysis of Petroleum Products and Lubricants
    ASTM D 7578 : 2020 Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants
    ASTM D 7455 : 2019 Standard Practice for Sample Preparation of Petroleum and Lubricant Products for Elemental Analysis
    ASTM D 7578 : 2018 Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM D 4057 : 2019 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 7751 : 2014 Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis
    ASTM D 4057 : 1995 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 7669 : 2011 Standard Guide for Practical Lubricant Condition Data Trend Analysis
    ASTM D 7720:2011 Standard Guide for Statistically Evaluating Measurand Alarm Limits when Using Oil Analysis to Monitor Equipment and Oil for Fitness and Contamination
    ASTM D 4177 : 2016 : EDT 1 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 7874 : 2013 : R2018 Standard Guide for Applying Failure Mode and Effect Analysis (FMEA) to In-Service Lubricant Testing
    ASTM E 1621 : 2013 Standard Guide for Elemental Analysis by Wavelength Dispersive X-Ray Fluorescence Spectrometry
    ASTM D 4177 : 1995 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4057 : 2012 : R2018 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 7720 : 2021 Standard Guide for Statistically Evaluating Measurand Alarm Limits when Using Oil Analysis to Monitor Equipment and Oil for Fitness and Contamination
    ASTM D 5854 : 1996 : R2010 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
    ASTM D 7874 : 2013 : R2022 Standard Guide for Applying Failure Mode and Effect Analysis (FMEA) to In-Service Lubricant Testing
    ASTM D 4057 : 1981 : EDT 2 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM E 1621 : 2005 Standard Guide for X-Ray Emission Spectrometric Analysis
    ASTM D 5854 : 2019 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
    ASTM D 7751 : 2014 : EDT 1 Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis
    ASTM D 5854 : 1996 : R2005 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
    ASTM D 7874 : 2013 Standard Guide for Applying Failure Mode and Effect Analysis (FMEA) to In-Service Lubricant Testing
    ASTM D 7751 : 2012 Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis
    ASTM D 4057 : 2006 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM E 1621 : 2022 Standard Guide for Elemental Analysis by Wavelength Dispersive X-Ray Fluorescence Spectrometry
    ASTM D 4177 : 2015 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4057 : 2012 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 7669 : 2015 Standard Guide for Practical Lubricant Condition Data Trend Analysis
    ASTM E 1621 : 2021 Standard Guide for Elemental Analysis by Wavelength Dispersive X-Ray Fluorescence Spectrometry
    ASTM D 7751 : 2011 : EDT 1 Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis
    ASTM D 4177 : 2022 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4177 : 1995 : R2010 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4177 : 1995 : R2000 Standard Practice for Automatic Sampling of Peroleum and Petroleum Products
    ASTM D 5854 : 1996 : R2000 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
    ASTM E 1621 : 2013 : REDLINE Standard Guide for Elemental Analysis by Wavelength Dispersive X-Ray Fluorescence Spectrometry
    ISO 21018-3:2008 Hydraulic fluid power — Monitoring the level of particulate contamination of the fluid — Part 3: Use of the filter blockage technique
    ASTM D 7669 : 2015 : REDLINE Standard Guide for Practical Lubricant Condition Data Trend Analysis
    ASTM D 7751 : 2011 Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis
    ASTM D 7751 : 2016 Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis
    ASTM D 4057 : 2022 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 4177 : 2016 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4177 : 2020 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4177 : 1995 : R2005 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 7720 : 2011 : R2017 Standard Guide for Statistically Evaluating Measurand Alarm Limits when Using Oil Analysis to Monitor Equipment and Oil for Fitness and Contamination
    ASTM D 5854 : 2019 : REV A Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
    ASTM E 1621 : 1994 : R1999 Standard Guide for X-Ray Emission Spectrometric Analysis
    ASTM D 4057 : 1995 : R2000 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 7751 : 2016 : REDLINE Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis
    ASTM D 4177 : 2022 : EDT 1 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4177 : 2015 : REV A Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4057 : 2006 : R2011 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 7751 : 2016 : R2021 Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis
    ASTM D 5854 : 1996 : R2015 Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
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