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ASTM E 1382 : 1997 : R2023

Current

Current

The latest, up-to-date edition.

Standard Test Methods for Determining Average Grain Size Using Semiautomatic and Automatic Image Analysis

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

04-05-2023

€80.76
Excluding VAT

Committee
E 04
DocumentType
Test Method
Pages
24
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

1.1These test methods are used to determine grain size from measurements of grain intercept lengths, intercept counts, intersection counts, grain boundary length, and grain areas.

1.2These measurements are made with a semiautomatic digitizing tablet or by automatic image analysis using an image of the grain structure produced by a microscope.

1.3These test methods are applicable to any type of grain structure or grain size distribution as long as the grain boundaries can be clearly delineated by etching and subsequent image processing, if necessary.

1.4These test methods are applicable to measurement of other grain-like microstructures, such as cell structures.

1.5This standard deals only with the recommended test methods and nothing in it should be construed as defining or establishing limits of acceptability or fitness for purpose of the materials tested.

1.6The sections appear in the following order:

Section

Section

Scope

1

Referenced Documents

2

Terminology

3

 Definitions

3.1

 Definitions of Terms Specific to This Standard

3.2

 Symbols

3.3

Summary of Test Method

4

Significance and Use

5

Interferences

6

Apparatus

7

Sampling

8

Test Specimens

9

Specimen Preparation

10

Calibration

11

Procedure:

 Semiautomatic Digitizing Tablet

12

 Intercept Lengths

12.3

 Intercept and Intersection Counts

12.4

 Grain Counts

12.5

 Grain Areas

12.6

 ALA Grain Size

12.6.1

 Two-Phase Grain Structures

12.7

Procedure:

 Automatic Image Analysis

13

 Grain Boundary Length

13.5

 Intersection Counts

13.6

 Mean Chord (Intercept) Length/Field

13.7.2

 Individual Chord (Intercept) Lengths

13.7.4

 Grain Counts

13.8

 Mean Grain Area/Field

13.9

 Individual Grain Areas

13.9.4

 ALA Grain Size

13.9.8

 Two-Phase Grain Structures

13.10

Calculation of Results

14

Test Report

15

Precision and Bias

16

Grain Size of Non-Equiaxed Grain Structure Specimens

Annex A1

Examples of Proper and Improper Grain Boundary Delineation

Annex A2

1.7This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.8This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM E 112 : 2013 : R2021 Standard Test Methods for Determining Average Grain Size
ASTM F 1376 : 1992 : R2020 Standard Guide for Metallurgical Analysis for Gas Distribution System Components (Withdrawn 2023)
ASTM E 2627 : 2013 : R2019 Standard Practice for Determining Average Grain Size Using Electron Backscatter Diffraction (EBSD) in Fully Recrystallized Polycrystalline Materials
ASTM F 3160 : 2021 Standard Guide for Metallurgical Characterization of Absorbable Metallic Materials for Medical Implants
ASTM C 1557 : 2020 Standard Test Method for Tensile Strength and Young's Modulus of Fibers

ASTM E 1181 : 2002 : R2023 Standard Test Methods for Characterizing Duplex Grain Sizes
ASTM E 883 : 2011 : R2017 Standard Guide for Reflected–Light Photomicrography
ASTM E 1181 : 2002 : R2015 Standard Test Methods for Characterizing Duplex Grain Sizes
ASTM E 3 : 2011 : R2017 Standard Guide for Preparation of Metallographic Specimens
ASTM E 883 : 2011 : R2024 Standard Guide for Reflected–Light Photomicrography
ASTM E 407 : 2007 : R2015 : EDT 1 Standard Practice for Microetching Metals and Alloys
ASTM E 407 : 2023 Standard Practice for Microetching Metals and Alloys
ASTM E 112 : 2024 Standard Test Methods for Determining Average Grain Size

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