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ASTM E 2371 : 2021 : REV A

Current

Current

The latest, up-to-date edition.

Standard Test Method for Analysis of Titanium and Titanium Alloys by Direct Current Plasma and Inductively Coupled Plasma Atomic Emission Spectrometry (Performance-Based Test Methodology)

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

06-01-2022

€61.92
Excluding VAT

Committee
E 01
DocumentType
Test Method
Pages
14
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

1.1This method describes the analysis of titanium and titanium alloys, such as specified by committee B10, by inductively coupled plasma atomic emission spectrometry (ICP-AES) and direct current plasma atomic emission spectrometry (DCP-AES) for the following elements:

Element

Application
Range (wt.%)

Quantitative
Range (wt.%)

Aluminum

0–8

0.009 to 8.0

Boron

0–0.04

0.0008 to 0.01

Cobalt

0-1

0.006 to 0.1

Chromium

0–5

0.005 to 4.0

Copper

0–0.6

0.004 to 0.5

Iron

0–3

0.004 to 3.0

Manganese

0–0.04

0.003 to 0.01

Molybdenum

0–8

0.004 to 6.0

Nickel

0–1

0.001 to 1.0

Niobium

0-6

0.008 to 0.1

Palladium

0-0.3

0.02 to 0.20

Ruthenium

0-0.5

0.004 to 0.10

Silicon

0–0.5

0.02 to 0.4

Tantalum

0-1

0.01 to 0.10

Tin

0–4

0.02 to 3.0

Tungsten

0-5

0.01 to 0.10

Vanadium

0–15

0.01 to 15.0

Yttrium

0–0.04

0.001 to 0.004

Zirconium

0–5

0.003 to 4.0

1.2This test method has been interlaboratory tested for the elements and ranges specified in the quantitative range part of the table in 1.1. It may be possible to extend this test method to other elements or broader mass fraction ranges as shown in the application range part of the table above provided that test method validation is performed that includes evaluation of method sensitivity, precision, and bias. Additionally, the validation study shall evaluate the acceptability of sample preparation methodology using reference materials or spike recoveries, or both. Guide E2857 provides information on validation of analytical methods for alloy analysis.

1.3Because of the lack of certified reference materials (CRMs) containing bismuth, hafnium, and magnesium, these elements were not included in the scope or the interlaboratory study (ILS). It may be possible to extend the scope of this test method to include these elements provided that method validation includes the evaluation of method sensitivity, precision, and bias during the development of the testing method.

1.4Units—The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific safety hazards statements are given in Section 9.

1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM F 2885 : 2017 Standard Specification for Metal Injection Molded Titanium-6Aluminum-4Vanadium Components for Surgical Implant Applications
ASTM B 299/B299M : 2018 Standard Specification for Titanium Sponge
ASTM B 1009 : 2020 Standard Specification for Titanium Alloy Bars for Near Surface Mounts in Civil Structures
ASTM E 1004 : 2017 Standard Test Method for Determining Electrical Conductivity Using the Electromagnetic (Eddy Current) Method
ASTM F 136 : 2013 : R2021 : EDT 1 Standard Specification for Wrought Titanium-6Aluminum-4Vanadium ELI (Extra Low Interstitial) Alloy for Surgical Implant Applications (UNS R56401)
ASTM B 367 : 2013 : R2017 Standard Specification for Titanium and Titanium Alloy Castings
ASTM B 348/B348M : 2021 Standard Specification for Titanium and Titanium Alloy Bars and Billets
ASTM B 988 : 2018 Standard Specification for Powder Metallurgy (PM) Titanium and Titanium Alloy Structural Components
ASTM F 620 : 2020 Standard Specification for Titanium Alloy Forgings for Surgical Implants in the Alpha Plus Beta Condition
ASTM F 1295 : 2016 Standard Specification for Wrought Titanium-6Aluminum-7Niobium Alloy for Surgical Implant Applications (UNS R56700)
ASTM F 1580 : 2018 Standard Specification for Titanium and Titanium-6 Aluminum-4 Vanadium Alloy Powders for Coatings of Surgical Implants
ASTM B 863 : 2019 Standard Specification for Titanium and Titanium Alloy Wire
ASTM B 861 : 2019 Standard Specification for Titanium and Titanium Alloy Seamless Pipe
ASTM B 862 : 2019 Standard Specification for Titanium and Titanium Alloy Welded Pipe
ASTM B 381 : 2021 Standard Specification for Titanium and Titanium Alloy Forgings
ASTM B 338 : 2017 : R2021 Standard Specification for Seamless and Welded Titanium and Titanium Alloy Tubes for Condensers and Heat Exchangers
ASTM F 2146 : 2013 Standard Specification for Wrought Titanium-3Aluminum-2.5Vanadium Alloy Seamless Tubing for Surgical Implant Applications (UNS R56320)
ASTM F 3046 : 2021 Standard Specification for Wrought Titanium-3Aluminum-2.5Vanadium Alloy for Surgical Implant Applications (UNS R56320)
ASTM F 2924 : 2014 : R2021 Standard Specification for Additive Manufacturing Titanium-6 Aluminum-4 Vanadium with Powder Bed Fusion
ASTM F 3001 : 2014 : R2021 Standard Specification for Additive Manufacturing Titanium-6 Aluminum-4 Vanadium ELI (Extra Low Interstitial) with Powder Bed Fusion
ASTM F 1813 : 2021 Standard Specification for Wrought Titanium-12Molybdenum-6Zirconium-2Iron Alloy for Surgical Implant (UNS R58120)
ASTM F 67 : 2013 : R2017 Standard Specification for Unalloyed Titanium, for Surgical Implant Applications (UNS R50250, UNS R50400, UNS R50550, UNS R50700)
ASTM F 2066 : 2018 Standard Specification for Wrought Titanium-15 Molybdenum Alloy for Surgical Implant Applications (UNS R58150)
ASTM B 265 : 2020 : REV A Standard Specification for Titanium and Titanium Alloy Strip, Sheet, and Plate
ASTM F 3049 : 2014 : R2021 Standard Guide for Characterizing Properties of Metal Powders Used for Additive Manufacturing Processes
ASTM F 3302 : 2018 Standard for Additive Manufacturing – Finished Part Properties – Standard Specification for Titanium Alloys via Powder Bed Fusion
ASTM F 1472 : 2020 : REV A Standard Specification for Wrought Titanium-6Aluminum-4Vanadium Alloy for Surgical Implant Applications (UNS R56400)
ASTM F 2989 : 2021 Standard Specification for Metal Injection Molded Unalloyed Titanium Components for Surgical Implant Applications
ASTM F 1713 : 2008 : R2021 : EDT 1 Standard Specification for Wrought Titanium-13Niobium-13Zirconium Alloy for Surgical Implant Applications (UNS R58130)
SAE AMS6952A Titanium Alloy, Forgings 5.8Al - 4.0Sn - 3.5Zr - 2.8Mo - 0.7Nb - 0.35Si - 0.06C Solution and Precipitation Heat Treated
SAE AMS4918R Titanium Alloy, Sheet, Strip, and Plate 6Al - 6V - 2Sn Annealed
SAE AMS4934J Titanium Alloy, Extrusions and Flash Welded Rings, 6Al - 4V, Solution Heat Treated and Aged
SAE AMS6901D Titanium Alloy Bars, Forgings, and Forging Stock, 5Al - 2.5Sn, Extra Low Interstitial, Annealed
SAE AMS6949B Titanium Alloy, Sheet and Strip, 4Al - 2.5V - 1.5Fe, Electron Beam Single Melted. Annealed

ASTM E 2027 : 2017 : EDT 1 Standard Practice for Conducting Proficiency Tests in the Chemical Analysis of Metals, Ores, and Related Materials (Withdrawn 2022)
ASTM D 1193 : 2024 Standard Specification for Reagent Water
ASTM E 1479 : 2016 Standard Practice for Describing and Specifying Inductively Coupled Plasma Atomic Emission Spectrometers
ASTM E 2857 : 2021 Standard Guide for Validating Analytical Methods
ASTM E 135 : 2023 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 135 : 2024 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 135 : 2021 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 1832 : 2008 : R2017 Standard Practice for Describing and Specifying a Direct Current Plasma Atomic Emission Spectrometer
ASTM E 691 : 2023 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 135 : 2023 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 1832 : 2008 : R2024 Standard Practice for Describing and Specifying a Direct Current Plasma Atomic Emission Spectrometer
ASTM E 2857 : 2022 Standard Guide for Validating Analytical Methods
ASTM E 691 : 2022 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 135 : 2022 : REV B Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 2857 : 2011 : R2021 : EDT 1 Standard Guide for Validating Analytical Methods
ASTM E 691 : 2021 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 50 : 2017 Standard Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials
ASTM E 135 : 2022 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 50 : 2024 Standard Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials
ASTM E 135 : 2022 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
ASTM E 1479 : 2024 Standard Practice for Describing and Specifying Inductively Coupled Plasma Atomic Emission Spectrometers

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