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ASTM E 2594 : 2020

Current

Current

The latest, up-to-date edition.

Standard Test Method for Analysis of Nickel Alloys by Inductively Coupled Plasma Atomic Emission Spectrometry (Performance-Based)

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

02-03-2020

€56.53
Excluding VAT

Committee
E 01
DocumentType
Test Method
Pages
10
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

1.1This test method describes the inductively coupled plasma atomic emission spectrometric analysis of nickel alloys, such as specified by Committee B02, and having chemical compositions within the following limits:

Element

Application Range (%)

Aluminum

0.01–1.00

Boron

0.001–0.050

Calcium

0.001–0.05

Carbon

0.10–0.20

Chromium

0.01–33.0

Cobalt

0.10–20.0

Copper

0.01–3.00

Iron

0.01–50.0

Lead

0.001–0.01

Magnesium

0.0001–0.100

Manganese

0.01–3.0

Molybdenum

0.01–30.0

Niobium

0.01–6.0

Nickel

25.0–80.0

Nitrogen

0.001–0.20

Oxygen

0.0001–0.003

Phosphorous

0.001–0.030

Sulfur

0.0001–0.010

Silicon

0.01–1.50

Tantalum

0.005–0.10

Tin

0.001–0.020

Titanium

0.001–6.0

Tungsten

0.01–5.0

Vanadium

0.01–1.0

Zirconium

0.01–0.10

1.2The following elements may be determined using this test method. The test method user should carefully evaluate the precision and bias statements of this test method to determine applicability of the test method for the intended use.

Element

Quantification Range (%)

Aluminum

0.060–1.40

Boron

0.002–0.020

Calcium

0.001–0.003

Copper

0.010–0.52

Magnesium

0.001–0.10

Manganese

0.002–0.65

Niobium

0.020–5.5

Phosphorous

0.004–0.030

Tantalum

0.010–0.050

Tin

0.002–0.018

Titanium

0.020–3.1

Tungsten

0.007–0.11

Vanadium

0.010–0.50

Zirconium

0.002–0.10

1.3This test method has only been interlaboratory tested for the elements and ranges specified. It may be possible to extend this test method to other elements or different quantification ranges provided that method validation is performed that includes evaluation of method sensitivity, precision, and bias as described in this document. Additionally, the validation study must evaluate the acceptability of sample preparation methodology using reference materials or spike recoveries, or both. The user is cautioned to carefully evaluate the validation data against the laboratory’s data quality objectives. Method validation of scope extensions is also a requirement of ISO/IEC 17025.

1.4The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given in 8.2.6.3 and safety hazard statements are given in Section 9.

1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM E 1473 : 2016 Standard Test Methods for Chemical Analysis of Nickel, Cobalt and High-Temperature Alloys
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ASTM D 1193 : 2024 Standard Specification for Reagent Water
ASTM E 1479 : 2016 Standard Practice for Describing and Specifying Inductively Coupled Plasma Atomic Emission Spectrometers
ASTM E 29 : 2013 : R2019 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
ASTM E 135 : 2023 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 135 : 2024 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 29 : 2002 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
ASTM E 135 : 2021 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 135 : 2003 : REV B Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 135 : 2023 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 1601 : 1998 Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
ASTM E 135 : 2002 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 135 : 2022 : REV B Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 50 : 2017 Standard Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials
ASTM E 135 : 2022 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 50 : 2024 Standard Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials
ASTM E 135 : 2021 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 135 : 2003 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 135 : 2003 : REV C Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 55 : 2023 Standard Practice for Sampling Wrought Nonferrous Metals and Alloys for Determination of Chemical Composition
ASTM E 135 : 2022 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 50 : 1982 : R1986 Standard Practices for Apparatus, Reagents, and Safety Precautions for Chemical Analysis of Metals
ASTM E 135 : 2020 : REV B Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 55 : 2011 : R2017 Standard Practice for Sampling Wrought Nonferrous Metals and Alloys for Determination of Chemical Composition
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
ASTM E 1479 : 2024 Standard Practice for Describing and Specifying Inductively Coupled Plasma Atomic Emission Spectrometers
ASTM E 55 : 2011 : R2022 : EDT 1 Standard Practice for Sampling Wrought Nonferrous Metals and Alloys for Determination of Chemical Composition
ASTM E 29 : 2022 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

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