ASTM E 2787 : 2011 : R2016
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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Standard Test Method for Determination of Thiodiglycol in Soil Using Pressurized Fluid Extraction Followed by Single Reaction Monitoring Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS)
Hardcopy , PDF
14-05-2021
English
25-09-2017
Important note : Users cannot be edited or removed once added to your Multi user PDF.CONTAINED IN VOL. 15.08, 2017 Defines the determination of thiodiglycol (TDG) in soil using pressurized fluid extraction (PFE). A commercially available PFE system was used, followed by analysis using liquid chromatography (LC), and detected with tandem mass spectrometry (MS/MS).
| Committee |
D 34
|
| DocumentType |
Test Method
|
| Pages |
9
|
| ProductNote |
Reconfirmed 2016
|
| PublisherName |
American Society for Testing and Materials
|
| Status |
Superseded
|
| SupersededBy | |
| Supersedes |
1.1This procedure covers the determination of thiodiglycol (TDG) in soil using pressurized fluid extraction (PFE). A commercially available PFE system2 was used, followed by analysis using liquid chromatography (LC), and detected with tandem mass spectrometry (MS/MS). TDG is qualitatively and quantitatively determined by this method. This method adheres to single reaction monitoring (SRM) mass spectrometry.
1.2The Method Detection Limit (MDL) and Reporting Range for TDG are listed in Table 1.
1.2.1The MDL is determined following the Code of Federal Regulations, 40 CFR Part 136, Appendix B.
1.2.2The reporting limit (RL) is calculated from the concentration of the Level 1 calibration standard as shown in Table 4. The RL for this method is 200 ppb. Reporting range concentrations are calculated from Table 4 concentrations assuming a 5 μL injection of the lowest level calibration standard, 5 g sample, and a 2 mL final extract volume.
1.3Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
| CFR 40(PTS100-149) : JUL 94 | PROTECTION OF ENVIRONMENT - ENVIRONMENTAL PROTECTION AGENCY |
| ASTM D 653 : 2007 | Standard Terminology Relating to Soil, Rock, and Contained Fluids |
| ASTM D 3740 : 2012-06 | PRACTICE FOR MINIMUM REQUIREMENTS FOR AGENCIES ENGAGED IN TESTING AND/OR INSPECTION OF SOIL AND ROCK AS USED IN ENGINEERING DESIGN AND CONSTRUCTION |
| ASTM D 653 : 2020 : EDT 1 | Standard Terminology Relating to Soil, Rock, and Contained Fluids |
| ASTM D 653 : 2021 | Standard Terminology Relating to Soil, Rock, and Contained Fluids |
| ASTM E 2554 : 2013-05 | PRACTICE FOR ESTIMATING AND MONITORING THE UNCERTAINTY OF TEST RESULTS OF A TEST METHOD USING CONTROL CHART TECHNIQUES |
| ASTM D 653 : 2014 : REDLINE | Standard Terminology Relating to Soil, Rock, and Contained Fluids |
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