ASTM E 2823 : 2017 : REDLINE
Current
The latest, up-to-date edition.
Standard Test Method for Analysis of Nickel Alloys by Inductively Coupled Plasma Mass Spectrometry (Performance-Based)
Hardcopy Redline , PDF Redline
English
01-01-2017
CONTAINED IN VOL. 03.05, 2017 Specifies the inductively coupled plasma mass spectrometric analysis of nickel and nickel allys, as specified by Committee B 02, and having chemical compositions.
Committee |
E 01
|
DocumentType |
Redline
|
Pages |
10
|
PublisherName |
American Society for Testing and Materials
|
Status |
Current
|
1.1This test method describes the inductively coupled plasma mass spectrometric analysis of nickel and nickel allys, as specified by Committee B02, and having chemical compositions within the following limits:
Element | Application Range (Mass Fraction %) |
Aluminum | 0. 01–6.00 |
Boron | 0. 01–0.10 |
Carbon | 0. 01–0.15 |
Chromium | 0. 01–33.00 |
Copper | 0.01–35.00 |
Cobalt | 0. 01–20.00 |
Iron | 0.05–50.00 |
Magnesium | 0. 01–0.020 |
Molybdenum | 0. 01–30.0 |
Niobium | 0. 01–6.0 |
Nickel | 25.00–100.0 |
Phosphorous | 0.001–0.025 |
Silicon | 0.01–1.50 |
Sulfur | 0.0001–0.01 |
Titanium | 0.0001–6.0 |
Tungsten | 0.01–5.0 |
Vanadium | 0.0005–1.0 |
1.2The following elements may be determined using this method.
Element | Quantification Range (μg/g) |
Antimony | 0.5–50 |
Bismuth | 0.1–11 |
Gallium | 2.9–54 |
Lead | 0.4–21 |
Silver | 1–35 |
Tin | 2.2–97 |
Thallium | 0.5–3.0 |
1.3This method has only been interlaboratory tested for the elements and ranges specified. It may be possible to extend this method to other elements or different composition ranges provided that method validation that includes evaluation of method sensitivity, precision, and bias as described in this document is performed. Additionally, the validation study must evaluate the acceptability of sample preparation methodology using reference materials and/or spike recoveries. The user is cautioned to carefully evaluate the validation data as to the intended purpose of the analytical results. Guide E2857 provides additional guidance on method validation.
1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific safety hazard statements are given in Section 9.
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SAE AMS 7001 : 2018 | NICKEL ALLOY, CORROSION AND HEAT-RESISTANT, POWDER FOR ADDITIVE MANUFACTURING, 62NI - 21.5CR - 9.0MO - 3.65NB |
ISO/IEC 17025:2005 | General requirements for the competence of testing and calibration laboratories |
ASTM E 177 : 2014 : REDLINE | Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods |
ASTM E 50 : 2017 : REDLINE | Standard Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials |
ASTM E 2165 : 2001 | Standard Practice for Establishing an Uncertainty Budget for the Chemical Analysis of Metals, Ores, and Related Materials (Withdrawn 2007) |
ASTM E 1479 : 2016 : REDLINE | Standard Practice for Describing and Specifying Inductively Coupled Plasma Atomic Emission Spectrometers |
ASTM E 2972 : 2015 | Standard Guide for Production, Testing, and Value Assignment of In-House Reference Materials for Metals, Ores, and Other Related Materials |
ASTM E 1601 : 2012 : REDLINE | Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method |
ISO/IEC Guide 98-3:2008 | Uncertainty of measurement — Part 3: Guide to the expression of uncertainty in measurement (GUM:1995) |
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